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    Tytuł:
    Attachment of 2,2-bipyridine onto a silica gel for application as a sequestering agent for copper, cadmium and lead ions from an aqueous medium
    Autorzy:
    Souza, E. J.
    Cristante, V. M.
    Padilha, P. M.
    Jorge, S. M. A.
    Martines, M. A. U.
    Silva, R. I. V.
    Carmo, D. R.
    Castro, G. R.
    Powiązania:
    https://bibliotekanauki.pl/articles/779827.pdf
    Data publikacji:
    2011
    Wydawca:
    Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
    Tematy:
    2,2-bipirydyna
    żel krzemionkowy
    adsorpcja
    jony metali
    2,2'-bipyridine
    silica gel
    adsorption
    metal ions
    Opis:
    A method was developed to attach 2,2-bipyridine (BP) onto a silica gel surface by a two-step reaction. The fi rst step consisted of a reaction between the matrix and a silylating agent, 3-chloropropyltrimethoxysilane. In the second step of the reaction, a ligand molecule was attached onto Si-CPTS, yielding the product Si-BP. The modified material contained 0.431±0.01 mmol of 2,2-bipyridine per gram of modified silica, as confirmed by FT-IR spectra of the proposed structure. The surface modification was characterized by the BET technique, which revealed a decrease in the surface area from 614 to 450 m2 g-1. The series of adsorption isotherms for the metal ions were adjusted to fit a modified Langmuir equation. The maximum number of moles of copper, cadmium and lead ions adsorbed was 0.64, 0.53, and 0.54 mmol g-1, respectively. The surface saturation was calculated as ¢ fraction and the values obtained, Cu(II) =1.160, Cd(II) = 1.044 and Pb(II) = 0.997, suggest a type 1:1 metal-ligand complex.
    Źródło:
    Polish Journal of Chemical Technology; 2011, 13, 4; 28-33
    1509-8117
    1899-4741
    Pojawia się w:
    Polish Journal of Chemical Technology
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Analysis of the effects of recycling on process control
    Autorzy:
    Silva, Cássio R.A.
    Panuci, Victor C.
    Coutinho, Monica R.
    Conceição, Wagner A.S.
    Andrade, Cid M.G.
    Powiązania:
    https://bibliotekanauki.pl/articles/27315644.pdf
    Data publikacji:
    2023
    Wydawca:
    Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
    Tematy:
    level control
    control structure
    decoupled tanks
    cycle
    Arduino
    Opis:
    The union of different devices in order to obtain a specific response for a process is commonly called a control system. For a control system, it is necessary to have one or more controllers. Among the most used in the industrial sector are the PID and PI controllers. Next to these controllers is the control software. Scilab is a good example of control software. It is characterized as free code software, with no cost for its acquisition, in addition to having a large computational power and integrated tools, such as Xcos, intended for modeling and simulation. For the union with Scilab, there is Arduino. Such a mixture can be used, for example, to control liquid levels in tanks. In this context, the present work aims to study the tank-level control system based on PID and PI controllers through the union between Scilab and Arduino. Phenomenological models were developed based on closed-loop control (feedback control system) of the process with two tanks not coupled with recycle. Furthermore, for comparison purposes, two approaches were used for each process: one considering the saturation of the manipulated variable and the other without the presence of such saturation. At first, there was a need to implement an anti-windup system. For tuning the controller parameters, the ISE method was used, executed through a programming code developed in Scilab. The parameters found for the two systems were tested on a made-up experimental bench. Therefore, using the block diagrams and the method here called “ISE method”, satisfactory values were obtained for the control parameters. These were ratified in the tests carried out in the experimental module. Level control was achieved with greater prominence for the PI controller since there is one less parameter to be tuned and processed by the system. This controller provided results close to the PID controller for cycles up to 50%. In general, the PI controller showed maximum response deviations smaller than the PID, such as deviations of 1.55 cm and 2.40 cm, respectively, for the case with 75% recycle. It was also clear the influence of the saturation of the manipulated variable on the system response, but not on the tuning of the controller parameterseters.
    Źródło:
    Polish Journal of Chemical Technology; 2023, 25, 2; 43--55
    1509-8117
    1899-4741
    Pojawia się w:
    Polish Journal of Chemical Technology
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-2 z 2

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