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    Wyświetlanie 1-7 z 7
    Tytuł:
    Flotation of antimony ores with high arsenic content
    Autorzy:
    Özer, Mustafa
    Powiązania:
    https://bibliotekanauki.pl/articles/2146881.pdf
    Data publikacji:
    2022
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    antimony
    arsenic
    flotation
    rougher
    clearing
    Opis:
    Efficient evaluation of antimony ores, which are on the critical raw materials list due to the supply risk by the European Union, is an important necessity. In this context, ore preparation and enrichment processes are very important during the process from ore to metal. Especially for sulfide antimony ores, the most common beneficiation method is flotation. Therefore, antimony ore consisting of stibnite mineral obtained from Tokat-Turkey region was used in this study. Due to the low antimony (5.06%Sb) and the high Arsenic (1.38%As) content, it is an important requirement to increase the Sb content of this ore by flotation, as well as to reduce the As content to certain levels. Stibnite as an antimony mineral and arsenopyrite as arsenic mineral, are minerals that have a sulphurous structure in mineralization and their flotation properties are quite close to each other. Therefore, in this study, it is aimed to selectively separate the bulk concentrate taken from rougher flotation by cleaning steps. A bulk sulfur concentrate with 24.54% Sb and 3.69% As content obtained as a result of the rougher flotation was obtained with a recovery of 98.9%. This product was subjected to 6 stages of cleaning flotation and a concentrate with a content of 63.8% Sb and 0.31% As was produced with an antimony recovery of 83% Sb.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2022, 58, 5; art. no. 152865
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Development of characterization methods for adherent anode slimes in copper electrorefining
    Autorzy:
    Kiviluoma, M.
    Aaltonen, M.
    Aromaa, J.
    Lundstrom, M.
    Forsen, O.
    Powiązania:
    https://bibliotekanauki.pl/articles/110440.pdf
    Data publikacji:
    2016
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    anode
    slime
    copper
    electrorefining
    nickel
    lead
    arsenic
    Opis:
    Adherent anode slimes can cause anode passivation in copper electrorefining and lower the efficiency of copper electrorefining. Declining concentrate grades cause larger impurity levels in anodes, thus creating larger quantities of slimes in the refining process. In order to investigate the characterization methods for adherent anode slimes in copper electrorefining, experiments were conducted for the Boliden Harjavalta Pori refinery material. Methods such as particle size determination, chemical (ICP) analysis, settling rate determination, XRD, SEM-SE, SEM-BSE and SEM-EDS were applied. In addition, adherent anode slime samples were compared to optical micrograph and SEM-BSE images of respective anode copper samples. It was shown that SEM-EDS and SEM-BSE provided precise information about phases formed during electrorefining. The settling rate and particle size had a correlation only with a copper content of anode slime. The main phases in the anode slime were copper and lead sulphates as well as copper-silver selenides. NiO was shown to be the major Ni-bearing phase in the adherent slime. Nickel, tellurium and lead had the strongest, whereas arsenic, selenium and antimony had the weakest tendency to report to the anode slime.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2016, 52, 1; 295-302
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effect of pyrite type on the electrochemistry of chalcopyrite/pyrite interactions
    Autorzy:
    Forbes, E.
    Smith, L.
    Vepsalainen, M.
    Powiązania:
    https://bibliotekanauki.pl/articles/110218.pdf
    Data publikacji:
    2018
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    flotation
    arsenic
    pyrite
    galvanic interaction
    Surface oxidation
    Opis:
    Pyrite is the most common sulphide gangue mineral occurring in base metal sulphide ores around the world. Pyrite is known to galvanically interact with valuable minerals such as chalcopyrite, altering their electrochemical and flotation behaviour. Different types of pyrite are known to vary in texture, chemical composition and electrochemical activity. However, the effect that these differences have on the degree of pyrite interaction with chalcopyrite are not well studied. This work examines two distinct types of pyrite from different deposits that have a similar chemical composition, but vary greatly in texture. It investigates the way in which these pyrites interact with chalcopyrite surfaces, affecting both its electrochemical behaviour and floatability. It was found that the Renison pyrite was characterised by a much higher level of surface activity than the Huanzala pyrite. This was attributed to the elevated levels of arsenic within the mineral’s crystalline matrix.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2018, 54, 4; 1117-1129
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Beneficiation of arsenic bearing complex sulphide ore by flotation
    Autorzy:
    Gul, A.
    Bulut, G.
    Sirkeci, A. A.
    Powiązania:
    https://bibliotekanauki.pl/articles/110834.pdf
    Data publikacji:
    2013
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    arsenic
    non-toxic depressants
    sulphide minerals
    flotation
    Opis:
    In this study beneficiation of a sulphide ore from the Gümüşhane-Black Sea Region of Turkey was investigated. Detailed flotation studies were carried out with the ore sample which contained 2.95% Pb, 6.72% Zn and 0.32% Cu. Mineralogical analyses showed that the sample includes pyrite, galena, sphalerite, chalcopyrite, tennantite, cerussite, anglesite and smithsonite. On the other hand, hematite, goethite, limonite, calcite and quartz were determined as gangue minerals. Selective sulphide concentrates with low arsenic content were tried to be produced by froth flotation. Individual concentrates of Pb, Zn and Cu assayed 67.54% Pb, and 61.49% Zn and 23.31% Cu where corresponding recoveries were 73.0% and 77.1% and 38.7%, respectively. Arsenic contents were less than 2000 ppm in the lead and zinc con-centrates. Copper concentrate assayed 5.03% As since the major copper minerals were in tennantite form (copper arsenic sulphide mineral). In flotation tests, non-toxic reagents such as metabisulphite, caustified starch, and activated carbon were used to depress minerals in relevant circuits.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2013, 49, 1; 203-212
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    The effect of CaO and MgO addition and cooling rate on stability of slag obtained after jarosite and neutral leaching residue treatment in the Waelz process
    Autorzy:
    Radovanovic, D.
    Kamberovic, Z.
    Andjic, Z.
    Ranitovic, M.
    Markovic, B.
    Powiązania:
    https://bibliotekanauki.pl/articles/109711.pdf
    Data publikacji:
    2018
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    Jarosite
    Waelz slag
    arsenic
    antimony
    leaching test
    microstructure
    Opis:
    Jarosite and neutral leaching residue (NLR) are the greatest environmental problems of hydrometallurgical zinc production due to their high quantity and hazardous content. Pyrometallur-gical processes, such as the Waelz process, could be applied to recover valuable metals present in this waste. The paper investigates the possibility of forming environmentally stable Waelz slag after the Waelz process of jarosite and NLR. Waelz slag, obtained using CaO as a conventional alkaline additive in the Waelz process, showed high As and Sb release after the EN 12457-4 standard leaching test. Multiphase equilibrium composition calculations indicated that As and Sb were present as volatile and migratory species in the slag. In order to obtain Waelz slag with more stable matrices that would encapsulate and immobilize pollutants, MgO additions to CaO and different cooling conditions of the slag were further investigated. The efficiency of modification in additives composition and cooling conditions was assessed by EN 12457-4 leaching test and chemical and microstructural characterization (XRF and SEM-EDS analyses) of the Waelz slags. The results show that addition of MgO does not reduce the efficiency of the process, even more it increases leaching resistance of the slags. Concentrations of all investigated metals (As, Ba, Cu, Mo, Pb, Sb, Zn) after the leaching test were below defined limits for non-hazardous waste. Microstructural analyses revealed that MgO remained inert during Waelz process, and thus favoring the formation of amorphous stable structure, which was enhanced by increased cooling rate. All investigated Waelz slags with MgO additions are suitable for further use or safe disposal.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2018, 54, 2; 484-495
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Arsenate removal on the ion exchanger modified with cerium(III) ions
    Autorzy:
    Dudek, Sebastian
    Kołodyńska, Dorota
    Powiązania:
    https://bibliotekanauki.pl/articles/2146888.pdf
    Data publikacji:
    2022
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    arsenic
    adsorption
    cerium
    iron oxides
    Ferrix A33E
    Opis:
    The iron oxide ion exchanger Ferrix A33E was successfully modified with cerium(III) ions to obtain Ferrix A33E-Ce(III) providing much better sorption properties in relation to the As(V) species. The new material has been characterized using a number of techniques including scanning electron microscopy SEM, nitrogen adsorption/desorption isotherms, Fourier transform infrared spectroscopy FTIR and X-ray photoelectron spectroscopy XPS. At optimal pH 6 the main mechanism of arsenate adsorption on A33E-Ce(III) was electrostatic attraction and formation of monodentate and bidentate surface complexes. The process was exothermic and spontaneous. Unlike the unmodified ion exchanger, A33E-Ce(III) could completely remove arsenic from the arsenate solution at a concentration of 50 mg/dm3 in 60 minutes. Furthermore, the maximum sorption capacity for As(V) was determined to be 60.41 mg/g which almost doubled after modification with cerium(III) ions. It is also worth noting that even after three cycles of sorption/desorption A33E-Ce(III) exhibited a higher sorption capacity than unmodified A33E before the arsenate adsorption. It can be concluded that modifying the sorbent with a small amount of cerium(III) ions boosts its sorption properties significantly, improves effectiveness of water purification and reduces the overall operation cost
    Źródło:
    Physicochemical Problems of Mineral Processing; 2022, 58, 2 (Special issue - selected papers conference: Physicochemistry of interfaces - instrumental methods); art. no. 147412
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Adsorption behaviour of As(III) onto synthetic iron-based minerals: a comparative study of akaganeite, goethite and magnetite
    Autorzy:
    Ulatowska, Justyna.
    Powiązania:
    https://bibliotekanauki.pl/articles/2146953.pdf
    Data publikacji:
    2022
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    iron-based minerals
    arsenic
    adsorption
    FTIR analysis
    kinetic study
    Opis:
    The present study compares the adsorption capacity of iron-based minerals in removing As(III) from aqueous solutions. The work contains the results of studies carried out on a laboratory scale. The synthetic material was used in three forms as akaganeite, goethite and magnetite. To characterise the minerals before and after adsorption of As(III), specific surface area, particle size distribution, density, and zeta potential were determined. Additionally, digital and optical micrographs, SEM, and FTIR analyses were performed. In the experimental part, the influence of the main parameters on the adsorption efficiency was investigated (pH, initial concentration, contact time, and amount of adsorbent). Adsorption isotherms were fitted by Freundlich, Langmuir, and DubininRadushkevich models. Pseudo-first-order (PFO), pseudo-second-order (PSO), and intraparticle diffusion (IPD) models were used to fit the kinetics data. Linear regression was used to estimate the parameters of isotherm and kinetic models. FTIR measurements gave helpful information on the synthesised minerals and the As(III) removal process. Results show that As(III) adsorption is related to the iron-based adsorbents, and adsorption efficiency increases in the following order: goethite < magnetite < akaganeite.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2022, 58, 2; art. no. 144818
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-7 z 7

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