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    Wyświetlanie 1-12 z 12
    Tytuł:
    Application of uniform test design in optimizing the flotation reagents of iron anionic reverse flotation circuit
    Autorzy:
    Hou, Ying
    Sobhy, Ahmed
    Powiązania:
    https://bibliotekanauki.pl/articles/2146945.pdf
    Data publikacji:
    2022
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    iron oxide
    quartz
    uniform test design
    reverse flotation
    optimization
    flotation reagents
    Opis:
    Most iron reserves are low in grade with quartz as the main gangue mineral, and anionic reverse flotation has become the most crucial separation method in the processing plants of iron ore. Thus, a flotation feed sample that is a mixture of low-intensity and high-gradient magnetic separators concentrates was acquired from a processing plant. The sample characterizations with X-ray diffraction (XRD), X-ray fluorescence (XRF), laser particle size analyzer, and mineral liberation analysis (MLA) confirmed that the sample consists of iron oxide as a valuable mineral and quartz as a gangue mineral with adequate liberation degree. In the anionic reverse flotation, the interaction of the flotation reagents with the constituents of the feed makes the flotation a complex system. Thus, the selection and optimization of regent dosages were performed using a uniform experimental design to estimate the optimum separation efficiency. The optimum reagent system was 1.6 kg/Mg starch depressant, 1.0 kg/Mg calcium oxide (lime) activator, and 0.8 kg/Mg TD-II anionic collector. At the optimum, 68.90% iron grade with 92.62% recovery was produced.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2022, 58, 1; 37--49
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Flotation separation of cassiterite and chlorite using carboxymethyl cellulose as a depressant
    Autorzy:
    Hu, Yang
    Ying, Luo Hong
    Zhang, Ying
    Wei, Lu Kuan
    Hao, Guan Zhen
    Powiązania:
    https://bibliotekanauki.pl/articles/2175422.pdf
    Data publikacji:
    2022
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    cassiterite
    chlorite
    sodium oleate
    carboxymethyl cellulose
    selective inhibition
    Opis:
    The nature and mechanism of interaction between carboxymethyl cellulose (CMC) with cassiterite (and chlorite surfaces) and their effects on the flotation separation process of cassiterite (from chlorite) were investigated by micro-flotation tests, surface adsorption experiments, zeta potential measurements, solution chemical calculation, infrared spectroscopy, and X-ray photo-electron spectroscopy (XPS). The results from single mineral tests revealed that CMC exhibited good selective inhibition effects with cassiterites and chlorites. When the dosage was 12.5 mg/L at pH 8, cassiterite and chlorite recovery was 92.2% and 6.3%, respectively. The artificial mixed ore test revealed that the flotation separation effect was the best when the dosage of CMC was 6.5 mg/L. Cassiterite used during the studies was 75.1% pure. The recovery was 82.8%. The interaction between CMC and the cassiterite surface led to a shift in the zeta potential toward the negative direction. CMC was weakly adsorbed on the cassiterite surface. There was no significant impact on the subsequent collection of sodium oleate. The concentration of C atom increased post interaction, and the potential shifted toward the negative direction. Characteristic CMC peaks were observed at this point. Hydrogen bonds and weak chemisorption interactions between CMC and chlorite affected the interaction between sodium oleate and the chlorite surface. It also affected the flotation results. The cassiterite and chlorite were separated effectively.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2022, 58, 6; art. no. 155141
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Prediction and optimization of tower mill grinding power consumption based on GA-BP neural network
    Autorzy:
    Wang, Ziyang
    Hou, Ying
    Sobhy, Ahmed
    Powiązania:
    https://bibliotekanauki.pl/articles/27323660.pdf
    Data publikacji:
    2023
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    tower mill
    grinding power consumption
    energy saving
    genetic algorithm
    BP neural network
    Opis:
    Grinding is commonly responsible for the liberation of valuable minerals from host rocks but can entail high costs in terms of energy and medium consumption, but a tower mill is a unique power-saving grinding machine over traditional mills. In a tower mill, many operating parameters affect the grinding performance, such as the amount of slurry with a known solid concentration, screw mixer speed, medium filling rate, material-ball ratio, and medium properties. Thus, 25 groups of grinding tests were conducted to establish the relationship between the grinding power consumption and operating parameters. The prediction model was established based on the backpropagation “BP” neural network, further optimized by the genetic algorithm GA to ensure the accuracy of the model, and verified. The test results show that the relative error of the predicted and actual values of the backpropagation “BP” neural network prediction model within 3% was reduced to within 2% by conducting the generic algorithm backpropagation “GA-BP” neural network. The optimum grinding power consumption of 41.069 kWh/t was obtained at the predicted operating parameters of 66.49% grinding concentration, 301.86 r/min screw speed, 20.47% medium filling rate, 96.61% medium ratio, and 0.1394 material-ball ratio. The verifying laboratory test at the optimum conditions, produced a grinding power consumption of 41.85 kWh/t with a relative error of 1.87%, showing the feasibility of using the genetic algorithm and BP neural network to optimize the grinding power consumption of the tower mill.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2023, 59, 6; art. no. 172096
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Significance of reagents addition sequence on iron anionic reverse flotation and their adsorption characteristics using QCM-D
    Autorzy:
    Hou, Ying
    Sobhy, Ahmed
    Wang, Yue
    Powiązania:
    https://bibliotekanauki.pl/articles/1448929.pdf
    Data publikacji:
    2021
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    iron oxide
    adsorption
    pH modifier
    starch
    reverse flotation
    QCM-D
    Opis:
    To explore the influence of reagents addition sequence of the pH regulator and the starch depressant on the anionic reverse flotation of iron oxide, flotation conditional experiments were performed on mixed low-intensity and high-gradient magnetic concentrates which is the flotation feed acquired from the iron processing plant. Besides, quartz crystal micro-balance with dissipative (QCM-D) was conducted to detect the adsorption phenomena of the flotation reagent on iron oxide sensors at different addition orders. The outcomes showed that the flotation performance using the pH regulator prior to the depressant was the best. For example, at 1.6 kg/Mg starch dosage, the recovery and separation efficiencies were improved by 18.3% and 21.2%, respectively, with keeping the concentrate Fe grade as high as 69.5%. Also, QCM-D frequency shifted by -41 Hz from 17 Hz to -24 Hz with increased dissipation from -2.6 x 10-6 to 8.2 x 10-6, indicating an increase in the mass of slightly-rigid starch adsorption layer on the surface of iron oxide under a strong alkaline condition with adsorption density of about 0.46 mg/cm2. On the other hand, under weak alkaline conditions, starch was adsorbed, and then the starch was desorbed upon the addition of the strong alkaline solution. Whereas, adding the pH modifier to create a strong alkaline condition enhanced the starch adsorption significantly with coordination and hydrogen bonds, and prevented the following adsorption of the anionic collector for more efficient reverse flotation of iron oxide minerals.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2021, 57, 1; 284-293
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Dispersion of sodium phytate on muscovite and the implications for arsenopyrite flotation
    Autorzy:
    Zou, Dan
    Wang, Zhen
    Zhao, Kaile
    Xu, Ying
    Powiązania:
    https://bibliotekanauki.pl/articles/2175449.pdf
    Data publikacji:
    2022
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    cassiterite
    chlorite
    sodium oleate
    carboxymethyl cellulose
    selective inhibition
    Opis:
    The effective flotation separation of sulfides and sliming silicate minerals is always a difficult problem. In this paper, the selective flotation of arsenopyrite from muscovite was studied by using sodium phytate (SP) as dispersant, and the mechanism was investigated through SEM/EDS, zeta potential, FTIR and XPS measurements. Single mineral flotation results showed that with the increasing isoamyl xanthate (IAX) dosage the recovery of arsenopyrite increased, until 8×10−5 mol/L IAX (79.40% recovery, pH=7), after that it decreased slightly. While muscovite floated poorly at any IAX concentration. For the mixed minerals, arsenopyrite recovery was only 54.63% while that of muscovite was 42.70%, which was attributed to the coverage of muscovite on arsenopyrite surface. When 6×10−5 mol/L SP was added into the mixed minerals system, the recovery of arsenopyrite recovered to 68.26% while that of muscovite was 8.48% (approximate the value of the single mineral). SEM/EDS results showed that SP could disperse muscovite and prevented its coverage on arsenopyrite surface. Zeta potential results showed that the electrokinetic potential of muscovite and arsenopyrite decrease from -26.60mV to -39.01 mV and from -26.90 mV to -27.84 mV at pH=7, respectively. It was obvious that the negatively charged phytate ions selectively adsorbed on the surface of muscovite. FTIR and XPS resulted co-proved the chemisorption of SP with active sites on muscovite while arsenopyrite spectrum did not change significantly, which was consistent with flotation and zeta potential results. The selective adsorption of SP on muscovite compared to arsenopyrite was responsible for the effective separation of them.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2022, 58, 6; art. no. 154951
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Mechanism of ultrasonic cavitation to improve the effect of siderite on quartz flotation
    Autorzy:
    Yin, Wanzhong
    Cai, Lizheng
    Ma, Yingqiang
    Wang, Ying
    Powiązania:
    https://bibliotekanauki.pl/articles/24085972.pdf
    Data publikacji:
    2023
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    ultrasound treatment
    cover
    fine siderite
    CaCO3 precipitate
    Opis:
    In order to effectively eliminate the effect of fine carbonate minerals on quartz flotation, the influence of fine siderite on quartz flotation was studied as well as the mechanism or role of ultrasonic treatment in the process. The results of adsorption capacity measurement and flotation solution chemical calculation show that fine siderite and its dissolved components have a great influence on the collector consumption and the surface properties of quartz. In addition, SEM, EDS and XPS analysis were used to study the surface morphology and chemical environment changes of quartz with and without ultrasonic treatment. The results of flotation test show that the recovery of quartz increase from 38.79% to 58.38% under the condition that ultrasonic time was 0.5 min and ultrasonic power was200 W. The mechanical effect caused by ultrasonic cavitation can clean the quartz surface to a certain extent and increase its active sites, thus improving the floatability of quartz.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2023, 59, 2; art. no. 165930
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Adsorption of yeast dextran on clinochlore surface and the implications for pyrite/clinochlore separation
    Autorzy:
    Wang, Zhen
    Zou, Dan
    Zhao, Kaile
    Safarov, Sayfidin
    Xu, Ying
    Powiązania:
    https://bibliotekanauki.pl/articles/2146917.pdf
    Data publikacji:
    2022
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    clinochlore
    pyrite
    flotation
    yeast dextran
    adsorption
    Opis:
    Silicate minerals with a certain degree of flotability are often easy to mix into sulfide ore concentrate in mineral processing industry. In this paper, the adsorption of yeast dextran on clinochlore and its application in pyrite/clinochlore separation were investigated. The adsorbed amount and micro polarity measurement results displayed that the yeast dextran molecules selectively adsorbed onto clinochlore surface compared with pyrite. The adsorbed yeast dextran resulted in the increase in the surface polarity of clinochlore surface, and inhibited the further adsorption of xanthate, thus keep it hydrophilic and depressed. Quantum chemical computation results indicated that yeast dextran was mainly adsorbed on mineral surface by the chelation with the surface metal active sites, and the chelating strength of yeast dextran with three ions was in the sequence of Fe3+ > Mg2+ > Fe2+. While Mg2+, Fe2+ and Fe3+ are the main metal ions on the surface of clinochlore, and Fe2+ is the unique metal ions on pyrite surface. This is the reason of the selectivity of the yeast dextran depressant for pyrite/clinochlore flotation system. The flotation results demonstrated that yeast dextran was qualified to selectively depress clinochlore in pyrite flotation.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2022, 58, 4; art. no. 151635
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Selective depression of Escherichia coli on flotation of collophanite and dolomite
    Autorzy:
    Li, JiaXin
    Nie, GuangHua
    Jiang, Ying
    Luo, GuoJv
    Li, Jie
    Powiązania:
    https://bibliotekanauki.pl/articles/2146918.pdf
    Data publikacji:
    2022
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    Escherichia coli
    collophanite
    dolomite
    flotation
    phosphate rock
    Opis:
    The phosphate rock flotatio n test was carried out using Escherichia coli E. coli ) as a depressant of dolomite. The results showed that E. coli had a great selective depression on dolomite during flotation. With E. coli as a depressant of dolomite, a useful beneficiation index of phosphorus concentrate with P2O5 grade of more than 30% and MgO content less than 1.2% can be obtained by closed circuit of one stage roughing and one stage cleaning. Furthermore, the depression mechanism of E. coli was studied by ad sorption experiments, infrared spectrum, and zeta potential. This study shows that the adsorption ability of E. coli onto dolomite is stronger than that of collophanite. When the pH is greater than 6, E. coli are chemically adsorbed on the surface of the c ollophanite and dolomite,which also increases the negative charge on the surface of the two minerals. The selective adsorption of E. coli cells to dolomite was best when the pH value is about 7.8.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2022, 58, 4; art. no. 150604
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effect of particle size on flotation performance of hematite
    Autorzy:
    Luo, Ximei
    Song, Shuixiang
    Ma, Mingze
    Wang, Yunfan
    Zhou, Yongfeng
    Zhang, Ying
    Powiązania:
    https://bibliotekanauki.pl/articles/109891.pdf
    Data publikacji:
    2019
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    particle size
    hematite
    entrainment
    surface bonding site
    reagent adsorption
    Opis:
    The effect of particle size on flotation performance of hematite and quartz was investigated. Microflotation, X-ray photoelectron spectroscopy analysis, reagent adsorption measurements, and collision and attachment probability calculation between particle and bubble were conducted in this investigation. The results showed that the floatability of minerals with different particle size fractions was different, which was mainly related to surface bonding site, reagent adsorption, collision probability and entrainment. The quartz with different particle size had little impact on hematite recovery, but -45 μm fraction negatively affected Fe grade of concentrate both in the direct and reverse flotation of hematite. In the direct flotation, the Fe grade in froth product dropped off due to the fine quartz entrainment. While in the reverse flotation, the Fe grade in sink product dropped off as a result of difficulty in floating fine quartz particles, which was due to lower collision probability. Meanwhile, in the reverse flotation, the presence of hematite fines (-18 μm fraction) also had negative impact on hematite recovery because of fine particle entrainment.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2019, 55, 2; 479-493
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effect of manganese ions addition orders on the flotation behavior of scheelite
    Autorzy:
    Lu, Kuanwei
    Chen, Rong
    Zhang, Ying
    Luo, Hongying
    Yang, Hu
    Cai, Jiaozhong
    Powiązania:
    https://bibliotekanauki.pl/articles/1845215.pdf
    Data publikacji:
    2020
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    manganese ion
    addition order
    scheelite
    sodium silicate
    flotation
    Opis:
    In this study, the effect of MnCl2 on scheelite flotation with sodium oleate (NaOL) as a collector and sodium silicate as a depressant was assessed by a combination of flotation experiments, Fouriertransform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), and solution chemistry. The flotation experiments confirmed that the addition of MnCl2 before sodium silicate showed an adverse effect on flotation and the recovery of scheelite gradually decreased as the amount of MnCl2 was increased. When MnCl2 was added afte r sodium silicate, the recovery of scheelite gradually increased with an increase in the amount of MnCl2. The results of FTIR, XPS, and solution chemistry indicated that MnCl2 acted on the surface of scheelite in the form of manganese ions. When MnCl2 was added before sodium silicate, manganese ions adsorbed on the surface of scheelite reacted with sodium silicate to form a hydrophilic silicate, which covers the surface of scheelite and blocks the adsorption of NaOL. However, when MnCl2 was added after sodium silicate, manganese ions are continued to be adsorbed on the surface of scheelite, which increases the cations on the surface of scheelite, and hence the condition becomes conducive for the interaction between scheelite and NaOL.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2020, 56, 5; 860-873
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Preparation of α-calcium sulfate hemihydrate from industrial by-product gypsum: a review
    Autorzy:
    Guan, Qingjun
    Sui, Ying
    Zhang, Fang
    Yu, Weijian
    Bo, Yongjie
    Wang, Ping
    Peng, Wenqing
    Jin, Jiao
    Powiązania:
    https://bibliotekanauki.pl/articles/1448527.pdf
    Data publikacji:
    2021
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    α-calcium sulfate hemihydrate
    industrial by-product gypsum
    FGD gypsum
    phosphogypsum
    preparation method
    Opis:
    In recent years, the massive accumulation of industrial by-product gypsum, especially flue gas desulfurization (FGD) gypsum and phosphogypsum (PG), not only encroaches on lands but also causes serious environmental pollution. The preparation of α-calcium sulfate hemihydrate (α-HH) from industrial by-product gypsum is an important way to solve the massive accumulation. α-HH possessing larger, dense and well-grown crystals with fewer cracks and pores has high added value and a wide range of application. Hitherto the preparation methods of α-HH from industrial by-product gypsum mainly include the autoclave process, salt/acid solution process, or alcohol-water solution process. Thereinto, the autoclave process is the only method to realize industrialization. In order to solve the high energy consumption and unfavorable continuous operation of the autoclave process, researchers suggested alternative approaches, such as salt/acid solution process and alcohol-water solution process. However, these methods are basically in the laboratory stage or pilot scale test at present. Compared with FGD gypsum, the utilization rate of PG with a larger emission is very low owing to the high impurity content. And combining the preparation of α-HH with the recovery of valuable impurities from PG seems a promising way to solve the bulk deposition of PG.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2021, 57, 1; 168-181
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Preparation of magnesium hydroxide by modifier-directed hydration and its effect on flame retardancy and mechanical properties of polypropylene
    Autorzy:
    Wang, Mei Jia
    Bai, Li Mei
    Zhang, Meng Ting
    Ma, Yu Xin
    Zhao, Liu Cheng
    Li, Shao Ying
    Powiązania:
    https://bibliotekanauki.pl/articles/27323651.pdf
    Data publikacji:
    2023
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    modifier
    hydration preparation
    magnesium hydroxide
    polypropylene
    Opis:
    With the rapid development of the polymer materials industry and the improvement of people's environmental awareness, magnesium hydroxide has been widely used in polymer materials due to its high decomposition temperature, non-toxic smoke suppression, and the advantages of neutralizing harmful gases produced by polymer combustion. However, the conventional preparation methods of magnesium hydroxide exhibit several issues, including high hydrophilicity, elevated polarity, and limited compatibility with polymers. This research proposes an improved method by adding sodium stearate and KH560 modifier, controlling the rate of magnesium oxide and preparing magnesium hydroxide flame retardants using a modifier-directed hydration method. Various characterizations confirmed its morphology, particle size and structure. The magnesium hydroxide exhibits low polarity, small particle size, stable structure and excellent hydrophobicity (with a contact angle of 120.32°, and a free energy of 1.34mN/m). In parallel, the magnesium hydroxide/polypropylene composites demonstrate excellent flame retardancy (LOI of 25%, V-1 grade) and simultaneously enhance the dispersion of magnesium hydroxide within the polypropylene matrix, improving the material's toughness and strength.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2023, 59, 6; art. no. 175706
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-12 z 12

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