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Tytuł:
Kinetics and mechanism of one-step reductive leaching of manganese oxide ores by EDTA/EDTA-2Na
Autorzy:
Zhang, C.
Wang, S.
Cao, Z.
Zhong, H.
Powiązania:
https://bibliotekanauki.pl/articles/109834.pdf
Data publikacji:
2018
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
kinetics
EDTA
reductive leaching
manganese oxide ores
EDTA-2Na
Opis:
In this research, the kinetics and mechanism of one-step reductive leaching of manganese oxide ores by ethylenediaminetetraacetic acid (EDTA) or its disodium salt (EDTA-2Na) in an aqueous medium have been investigated. The kinetic data of this reductive leaching process may be described by the Avrami model, and the apparent activation energy was determined to be 15.8 kJ·mol-1/7.9 kJ·mol-1 for leaching by EDTA/EDTA-2Na with a reaction order of -1.7/2.0. The EDTA/EDTA-2Na leach liquor characterized and analyzed by X-ray photoelectron spectra (XPS), Fourier transform infrared spectra (FTIR), and total organic carbon (TOC) determination denoted that the oxidation-reduction reaction happened between manganese(IV) and EDTA/EDTA-2Na, and a coordination complex, EDTA-manganese(II/III) formed. This new process can be easily used to leach manganese from manganese oxide ores in a moderate environment with the pH range of 5–8.
Źródło:
Physicochemical Problems of Mineral Processing; 2018, 54, 3; 858-867
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Study on a novel hydroxamic acid as the collector of rhodochrosite
Autorzy:
Zhao, G.
Dai, T.
Wang, S.
Zhong, H.
Powiązania:
https://bibliotekanauki.pl/articles/110816.pdf
Data publikacji:
2018
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
flotation
rhodochrosite
hydroxamic acid
DFT
Opis:
A novel collector, tert-butyl benzohydroxamic acid (TBHA), was first introduced in rhodochrosite flotation. The performance of TBHA was investigated by the density functional theory (DFT) calculation along with the micro flotation test, zeta potential determination and XPS analysis, compared with benzohydroxamic acid (BHA). TBHA has stronger affinity to the mineral than BHA in terms of frontier molecular orbital, atomic net charge and bond population. The substitution of tert-butyl group on the benzene ring improves the affinity of the hydroxamic acid to the mineral. TBHA exhibits excellent collecting ability to rhodochrosite with a recovery of about 99% at a concentration of 3.89×10-4 mol/dm3 and pH 6.5. The hydroxamic acid molecules are adhered on mineral surfaces by chemical adsorption, resulting in negative shifts for the zeta potential of rhodochrosite with the presence of the collector. Chemical adsorption can be also confirmed from XPS analyses that the atomic concentration ratios of C and O to Mn on the treated mineral surfaces were increased and the binding energy of Mn3s was decreased. The experimental data achieve excellent agreement with the computational analyses.
Źródło:
Physicochemical Problems of Mineral Processing; 2018, 54, 2; 428-439
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
A novel method to extract vanadium from high-grade vanadium slag: non-salt roasting and alkaline leaching
Autorzy:
Liu, B.
Meng, L.
Zheng, S.
Li, M.
Wang, S.
Powiązania:
https://bibliotekanauki.pl/articles/110480.pdf
Data publikacji:
2018
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
high-grade vanadium slag
cleaner production
non-salt roasting
alkaline leaching
mechanisms
Opis:
A new method using non-salt roasting-alkaline leaching to treat vanadium slag was proposed in this study. The V(III) in vanadium slag is oxidized to V(V) by roasting and the latter can be effectively leached out as vanadate by alkaline leaching. This method possesses distinct advantage of being able to treat high-grade vanadium slag. For the South Africa high-grade vanadium slag, the maximum vanadium recovery of 98% was achieved when the reaction conditions were roasting temperature of 850 °C, roasting time of 2 h, alkali concentration of 30 wt.%, leaching temperature of 210 °C, and leaching time of 2 h. The roasting and leaching mechanisms have been well elucidated based on the XRD and SEM analysis results. The phases transitions of vanadium slag were clearly presented. This work has laid the foundation for the industrial application of non-salt roasting-alkaline leaching and provided new insights into effective extraction of high-grade vanadium slag.
Źródło:
Physicochemical Problems of Mineral Processing; 2018, 54, 3; 657-667
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Adsorption behavior of surfactants on lignite particles with different densities in aqueous medium
Autorzy:
Wang, J.
He, Y.
Wen, B.
Ling, X.
Xie, W.
Wang, S.
Powiązania:
https://bibliotekanauki.pl/articles/110538.pdf
Data publikacji:
2017
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
interfacial surface free energy
adsorption
lignite
surfactant
Washburn equation
Opis:
Lignite is well known for its strong hydrophilicity and hard-to-float properties. However, the surface free energy of the solid is made up of two components, that is the Lifshitz-van der Waals and acid-base interaction energy. Differences in these two components between the low ash (lower density) and high ash fraction (higher density) provide a benefit for improving the separation efficiency through introducing surfactants in flotation. In this paper, thermodynamic characterization of three density lignite fractions was measured by a Washburn dynamic method. Combining the Washburn equation and Van Oss-Chaudhury-Good theory, the surface free energy components of three samples were calculated according to the wetting process by n-hexane, diiodomethane, deionized water and ethylene glycol. The Lifshitz-van der Waals part of surface free energy reduced with the coal density increase, especially between fractions of -1.45 g/cm3 and 1.45-1.80 g/cm3, while the Lewis base part increased slightly. The interfacial interaction free energies between the surfactant and lignite in aqueous medium indicated that the low hydrophilic index benefited for the stronger adsorption intensity. Increase of the surfactant Lifshitz-van der Waals component increases the adsorptive intensity on lower density lignite and the repulsive intensity on higher density lignite, which is beneficial for separation.
Źródło:
Physicochemical Problems of Mineral Processing; 2017, 53, 2; 996-1008
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Simultaneous extraction of vanadium and chromium from vanadium slag using low-pressure liquid phase oxidation method
Autorzy:
Xia, J.-P.
Zheng, S.-L.
Wang, S.-N.
Liu, B.
Zou, X.
Powiązania:
https://bibliotekanauki.pl/articles/110818.pdf
Data publikacji:
2018
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
vanadium slag
low pressure leaching
liquid phase oxidation
kinetics
Opis:
A low-pressure liquid oxidation method was proposed and proven to be effective to extract vanadium and chromium simultaneously from the vanadium slag in concentrated NaOH aqueous solutions. The effect of temperature, NaOH mass concentration, liquid-to-solid mass ratio, stirring speed and pressure on the extraction of vanadium and chromium in NaOH aqueous solutions were systematically investigated. Under the optimal reaction conditions (temperature of 473 K, liquid-to-solid mass ratio of 6:1, stirring speed of 700 rpm, NaOH mass concentration of 50%, pressure of 1 MPa and reaction time of 180 min), the vanadium and chromium recovery reached 95% and 90%, respectively. It was found that the reaction temperature and NaOH concentration were important factors for the extraction of vanadium and chromium. The kinetics of the decomposition of vanadium slag in concentrated NaOH aqueous under low pressure was analyzed using the shrinking core model, and the results indicated that the extraction of vanadium and chromium were both governed by the internal diffusion step, with apparent activation energies calculated to be 26.22 and 32.79 kJ/mol, respectively.
Źródło:
Physicochemical Problems of Mineral Processing; 2018, 54, 2; 609-619
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Response of energy-size reduction to the control of circulating load in vertical spindle pulverizer
Autorzy:
Li, H.
He, Y.
Zhang, Y.
Ge, Z.
Xie, W.
Wang, S.
Li, K.
Powiązania:
https://bibliotekanauki.pl/articles/110803.pdf
Data publikacji:
2017
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
circulating load control
response of energy-size reduction
mixture grinding
energy efficiency
Opis:
In the vertical spindle pulverizer (VSP), the large circulation ratio and high ash and sulfur contents in circulating load would result in intensive energy consumption and low grinding efficiency. Although the control of circulating load would help increase the energy efficiency, no quantitative study has been conducted due to the high temperature and pressure in the closed VSP. In this study, response of energy-size reduction to the control of circulating load was studied by the experimental simulation method. Coal mixtures with fine/coarse ratio of 11:1, 8:1 and 6:1 were ground by a lab-scale roller mill. Energy-size reductions of the coarse coal were compared to evaluate the influence of circulating load control. Results showed that the product with the coarse coal increased by 30% when the specific breakage energy was 1.0 kWht–1 as the circulation ratio decreased from 11 to 6. Meanwhile, a breakage characteristic index of the coarse coal was two times higher due to the cushioning effect of fines. Besides, decrease of circulation ratio led to increase of the breakage rate of coarse coal, and the energy saving improved by 57%. With the same energy input of 2.0 kWht-1, the yield of –0.09 mm pulverized fuel (PF) increased from 22 to 43%. Therefore, controlling the circulating load is an effective method to improve the breakage rate of coarse coal and energy efficiency for PF generation.
Źródło:
Physicochemical Problems of Mineral Processing; 2017, 53, 2; 793-801
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Modifying effect of electron beam irradiation on magnetic property of iron-bearing minerals
Autorzy:
Wang, H.
Lu, S.
Powiązania:
https://bibliotekanauki.pl/articles/109818.pdf
Data publikacji:
2014
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
magnetic susceptibility
iron bearing mineral
sulfide
electron beam irradiation
Opis:
The effect of electron beam irradiation on magnetic property of iron bearing minerals was investigated by susceptibility measurements. The results show that the magnetic susceptibility of iron bearing sulfide minerals can be enhanced remarkably by strong beam current irradiation, while the magnetic susceptibility of oxidized iron minerals keeps unchanged and even is slightly reduced. The magnetic susceptibility of arsenopyrite can reach the ferromagnetic level. The particle size of irradiated minerals makes notable effects on magnetic susceptibility. The magnetic susceptibility of irradiated minerals is enhanced greatly with reduction of particle size, and the irradiation dose corresponding to the maximum magnetic susceptibility is decreased simultaneously. Exposure of pyrite to small beam current electron irradiation can only enhance its magnetic susceptibility from 4 to 5-fold. Enhancement of magnetic property by radiation induced defects and excitation in minerals is limited. Strong beam current electron irradiation provides a novel approach to enlarge the magnetic property differences between iron bearing minerals.
Źródło:
Physicochemical Problems of Mineral Processing; 2014, 50, 1; 79-86
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Flotation separation of cervantite from quartz
Autorzy:
Wang, J.
Hua, Y.
Yu, S.
Xiao, J.
Xu, L.
Wang, Z.
Powiązania:
https://bibliotekanauki.pl/articles/110941.pdf
Data publikacji:
2017
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
cervantite
quartz
dodecylamine
flotation
density functional theory
Opis:
Flotation separation of cervantite (Sb2O4) from quartz was investigated using dodecylamine (DDA) as a collector. Experiments were conducted on single minerals and on a synthetic mixture of quartz and cervantite. Flotation separation mechanisms were investigated using the zeta potential technique, solution chemistry principles, density functional calculations and Fourier Transform Infrared (FT-IR) spectroscopy. The results indicated that DDA, primarily in the form of molecules, exhibited excellent performance in flotation of cervantite and quartz at pH 10.5. The adsorption energy of the DDA molecules on the cervantite surface was greater than the adsorption energy of water molecules, while the adsorption energy of DDA on the quartz surface was less than the adsorption energy of water molecules. DDA molecules can be adsorbed on the quartz surface to a certain extent, but it was difficult for the same molecule to be adsorbed on the cervantite surface in the pulp. This resulted in flotation of quartz. DDA molecules were adsorbed on quartz not only through physical adsorption but also by hydrogen bonding. However, cervantite could not be floated at pH 10.5 since adsorption of DDA molecules occurred through weak physical bonds on cervantite.
Źródło:
Physicochemical Problems of Mineral Processing; 2017, 53, 2; 1119-1132
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of two-stage stirred pulp-mixing on coal flotation
Autorzy:
Gui, X.
Wang, Y.
Zhang, H.
Li, S.
Powiązania:
https://bibliotekanauki.pl/articles/110764.pdf
Data publikacji:
2014
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
mixing
stirred
two stage
fine coal
flotation
Opis:
Stirred pulp-mixing is performed before coal flotation. In this study, a two-stage stirred pulpmixing tank was designed based on the single-stirred process to intensify the mixing effect of pulp and flotation reagents. A tank has a pitched-impeller opening-type turbine. Stirred pulp-mixing and flotation experiments were conducted on a sample of anthracite fine coal (-0.5mm) from the Xuehu Coal Preparation Plant in Henan Province, China. The results of the two-stage stirred pulp-mixing were compared with those of a single-stage stirred pulp-mixing in terms of flotation performance. Compared with the single-stage stirred pulp-mixing, two mixing areas and double-layer impeller were able to strengthen the energy input to the stirred system, thereby improving the mixing efficiency of flotation reagents and coal particles in the pulp. The two-stage stirred pulp-mixing significantly increased the flotation feed rate of the cyclone-static micro-bubble flotation column and concentrate yield, enhanced the combustible matter recovery effect of coarse particles at a suitable flotation feed rate, and ensured the recovery effect of fine particles at high flotation feed rate.
Źródło:
Physicochemical Problems of Mineral Processing; 2014, 50, 1; 299-310
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Pretreatment of coking wastewater by an adsorption process using fine coking coal
Autorzy:
Gao, L.
Li, S.
Wang, Y.
Gui, X.
Xu, H.
Powiązania:
https://bibliotekanauki.pl/articles/110417.pdf
Data publikacji:
2016
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
coking coal
coking wastewater
adsorption
COD
phenol
Opis:
A new technique for pretreatment of coking wastewater is introduced based on the concept of circular economy. Coal is fed into a coking system after adsorption. This study validates the feasibility of using coking coal to adsorb organic pollutants in coking wastewater. The sorption kinetics and equilibrium sorption isotherms of coking coal for removal of chemical oxygen demand (COD) and phenol from coking wastewater was also discussed in this paper. Gas chromatograph/mass spectroscopy (GC/MS) was used to detect changes in the quality of coking wastewater. The results showed that when coking coal dosage was 120 g/dm3, 65% of COD and 34% of phenol in waste water can be removed after 40 min of agitation. The surface functional groups of coking coal before and after adsorption were observed with a Fourier transform infrared spectrometer. The kinetics of COD and phenol adsorption from coking wastewater by coking coal fitted the pseudo second-order model. The adsorption process of coking coal can be classified into two categories, namely, rapid and slow. The Freundlich isotherm provided a better fit with all adsorption isotherms than the Langmuir isotherm. Coking coal could be a suitable low-cost adsorbent for recalcitrant organic pollutants.
Źródło:
Physicochemical Problems of Mineral Processing; 2016, 52, 1; 422-436
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Features of distribution of uranium and thorium in red mud
Autorzy:
Gu, H.
Wang, N.
Yang, Y.
Zhao, C.
Cui, S.
Powiązania:
https://bibliotekanauki.pl/articles/110444.pdf
Data publikacji:
2017
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
red mud
uranium
thorium
distribution
perovskite
Opis:
Natural radioactive elements such as uranium and thorium restrict the use of red mud as building materials or additives, and may cause environmental problems. The distribution features of U and Th in red mud was studied from micro and macro analysis, using EPMA, LA-ICP-MS, and methods of mineralogy and beneficiation. Based on the micro-area scanning analysis, main chemical compositions in red mud, such as Ca, Al, Si, Na, and K are dispersive while Fe and Ti mainly tend to concentrate in granular phases. Based on the in-situ analysis, the distribution of main elements and most trace elements in micro-zone of red mud was homogeneous. In micro-zone area, the variation tendency of thorium content was similar with Y in red mud samples. By means of the methods of mineralogy and beneficiation, red mud samples were separated into different fractions. U and Th tend to be enriched in the low density fraction of the red mud. Th presented a high concentration in the finest particle size fractions of the red mud. Neither U or Th was regularly distributed in various magnetic red mud fractions. Thorium fingerprint peaks were determined in perovskite by EDX under TEM, which is proposed to be one of the radioactivity sources in Bayer red mud.
Źródło:
Physicochemical Problems of Mineral Processing; 2017, 53, 1; 110-120
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Investigation of leaching kinetics of cerussite in sodium hydroxide solutions
Autorzy:
Feng, Q.
Wen, S.
Wang, Y.
Zhao, W.
Deng, J.
Powiązania:
https://bibliotekanauki.pl/articles/110621.pdf
Data publikacji:
2015
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
cerussite
sodium hydroxide
leaching
kinetics
activation energy
Opis:
The leaching kinetics of cerussite in alkaline medium was investigated with respect to experimental variables such as sodium hydroxide concentration, temperature, particle size and stirring speed. The results showed that leaching reagent concentration and reaction temperature exerted significant effects on the extraction of lead, whereas particle size and stirring speed exhibited a relatively moderate effect on the leaching rate. The leaching process followed the kinetic law of the shrinking core model, and the dissolution rates were controlled by the surface chemical reaction with an apparent activation energy value of 43.79 kJ/mol. A corresponding dissolution kinetic equation was also proposed to describe the dissolution reaction. The results indicated that sodium hydroxide could be used as an effective leaching reagent for extracting lead from cerussite.
Źródło:
Physicochemical Problems of Mineral Processing; 2015, 51, 2; 491-500
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Copper adsorption reaction rate and ion exchange ratio during the copper activation of sphalerite
Autorzy:
Liu, J.
Luo, D.
Huang, L.
Wang, Y.
Wen, S.
Powiązania:
https://bibliotekanauki.pl/articles/110651.pdf
Data publikacji:
2018
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
sphalerite
copper activation
solution chemistry
ion exchange ratio
reaction rate
Opis:
A theoretical analysis method of the solution chemistry characteristic of Cu(II) at various pH values was developed. Using such method, the existence form of Cu species and their proportions in aqueous solution can be clearly determined. After that, the copper adsorption and ion exchange ratio (E) during the copper activation of sphalerite were investigated. The results indicated that the copper activation of sphalerite can be divided into two stages, i.e., the fast activation stage (t ≤4 min) and slow activation stage (t >4 min). The general form of the copper adsorption rate was determined as ΓCu=K1ln(t) +Γ1, which is confirmed by the data fitting of the fast activation stage. The lower activation pH results in higher ion exchange efficiency for Cu substituting Zn. For a strong acid pH of 4.1, the E maintains about 1:1 in the entire activation time range and is not dependent on the activation time. However, the value of E is greater than 1 under weak acidic (pH=6.2) and alkaline (pH=9.1) pH conditions and it significantly depends on the activation time. For such conditions, E decreases with increase in the activation time, which supports the ion exchange mechanism, but within short activation time, it is not a 1:1 ion exchange process.
Źródło:
Physicochemical Problems of Mineral Processing; 2018, 54, 2; 377-385
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Flotation behaviour and surface characteristic of anosovite in a sodium oleate solution
Autorzy:
Wang, Y.
Wen, S.
Zhang, J.
Wu, D.
Xian, Y.
Shen, H.
Powiązania:
https://bibliotekanauki.pl/articles/110766.pdf
Data publikacji:
2017
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
anosovite
sodium oleate
flotation
adsorption
Opis:
Properties of anosovite in titanium slag, anosovite flotation response in a collector solution of sodium oleate, and adsorption behaviour of sodium oleate on the mineral surface were studied in the present work using XRD, Raman spectra, flotation tests, zeta potential analysis, FTIR and XPS. The results show that the anosovite crystal contains magnesium, and its chemical composition is Mg0.09Ti2.91O5. The chemical bonds on the anosovite surface mainly comprise Ti-O bonds. Micro-flotation tests indicate that anosovite has better floatability at a wide pH range and the recovery reaches 88% at pH=6, when the dosage of sodium oleate is only 4·10−6 mol/dm3. The point of zero charge of anosovite was determined near pH 3.2 by the zeta potential measurement. In the flotation process, chemical adsorption occurs between the carboxyl of sodium oleate and the titanium sites on the anosovite surface.
Źródło:
Physicochemical Problems of Mineral Processing; 2017, 53, 2; 714-723
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Efficient sulfidization of lead oxide at high temperature using pyrite as vulcanizing reagent
Autorzy:
Zheng, Y.-X.
Lv, J.-F.
Wang, H.
Wen, S.-M.
Huang, L.
Powiązania:
https://bibliotekanauki.pl/articles/110351.pdf
Data publikacji:
2018
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
lead oxide
sulfidization roasting
pyrite
reaction mechanism
TG
Opis:
A sulfidization roasting-flotation process was usually viewed to be effective in treating the refractory oxide ore. In this paper, pyrite was proposed to be applied as a potential vulcanizing reagent to transform PbO or its surface to PbS based on feasibilities of technology and economy. The evolution process, phase and characteristics of crystal growth were investigated by TG, XRD and SEM-EDS, respectively, to interpret the interaction mechanism of lead oxide and pyrite at high temperature. It was found that the decomposition process of pyrite under argon atmosphere was a slow process of sulfur released from FeS2 to FexS, which made the process easier to be controlled. When PbO was introduced into the system, the initial solid-solid (PbO-FeS2) reaction and prevailing solid-gas (PbO-S2(g)) reaction occurred at about 500 °C and 700 °C, respectively. Combined with the SEM-EDS analyses results, the optimal temperature for the sulfidization of PbO should be in the range of 700-750 °C.
Źródło:
Physicochemical Problems of Mineral Processing; 2018, 54, 2; 270-277
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
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