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    Wyświetlanie 1-8 z 8
    Tytuł:
    Study of flotation behavior and mechanism of cervantite activation by copper ions
    Autorzy:
    Wang, J.
    Wang, Y.
    Fu, K.
    Xu, L.
    Wang, Z.
    Sun, H.
    Xiao, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/110228.pdf
    Data publikacji:
    2018
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    flotation
    cervantite
    copper ions
    activation mechanism
    Opis:
    Copper-ion activation plays a highly important role in cervantite (Sb2O4) flotation. Without metal-ion activation, cervantite cannot be floated by sodium oleate. In this study, flotation tests were conducted to study the effect of Cu2+ on the flotation behaviours of cervantite and quartz (SiO2) as the main gangue mineral. Metal-ion adsorption capacities, zeta potentials, solution chemistry and X-ray photoelectron spectra were analyzed to study the adsorption behavior and mechanism of copper ions and sodium oleate interaction with the minerals surfaces. The results demonstrate that under weakly acidic conditions, cervantite can be flotated and separated from quartz by the addition of copper ions. The reason is that copper ions can be selectively adsorbed on the cervantite surface under weakly acidic conditions, thereby promoting the adsorption of sodium oleate onto the cervantite surface by chemical adsorption. Conversely, copper ions are weakly adsorbed on quartz surfaces below pH 6.1, and sodium oleate cannot be adsorbed on quartz surfaces by chemical adsorption. The hydroxy copper species are integral to the selective activation of cervantite over quartz.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2018, 54, 3; 814-825
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Flotation separation of cervantite from quartz
    Autorzy:
    Wang, J.
    Hua, Y.
    Yu, S.
    Xiao, J.
    Xu, L.
    Wang, Z.
    Powiązania:
    https://bibliotekanauki.pl/articles/110941.pdf
    Data publikacji:
    2017
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    cervantite
    quartz
    dodecylamine
    flotation
    density functional theory
    Opis:
    Flotation separation of cervantite (Sb2O4) from quartz was investigated using dodecylamine (DDA) as a collector. Experiments were conducted on single minerals and on a synthetic mixture of quartz and cervantite. Flotation separation mechanisms were investigated using the zeta potential technique, solution chemistry principles, density functional calculations and Fourier Transform Infrared (FT-IR) spectroscopy. The results indicated that DDA, primarily in the form of molecules, exhibited excellent performance in flotation of cervantite and quartz at pH 10.5. The adsorption energy of the DDA molecules on the cervantite surface was greater than the adsorption energy of water molecules, while the adsorption energy of DDA on the quartz surface was less than the adsorption energy of water molecules. DDA molecules can be adsorbed on the quartz surface to a certain extent, but it was difficult for the same molecule to be adsorbed on the cervantite surface in the pulp. This resulted in flotation of quartz. DDA molecules were adsorbed on quartz not only through physical adsorption but also by hydrogen bonding. However, cervantite could not be floated at pH 10.5 since adsorption of DDA molecules occurred through weak physical bonds on cervantite.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2017, 53, 2; 1119-1132
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Copper adsorption reaction rate and ion exchange ratio during the copper activation of sphalerite
    Autorzy:
    Liu, J.
    Luo, D.
    Huang, L.
    Wang, Y.
    Wen, S.
    Powiązania:
    https://bibliotekanauki.pl/articles/110651.pdf
    Data publikacji:
    2018
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    sphalerite
    copper activation
    solution chemistry
    ion exchange ratio
    reaction rate
    Opis:
    A theoretical analysis method of the solution chemistry characteristic of Cu(II) at various pH values was developed. Using such method, the existence form of Cu species and their proportions in aqueous solution can be clearly determined. After that, the copper adsorption and ion exchange ratio (E) during the copper activation of sphalerite were investigated. The results indicated that the copper activation of sphalerite can be divided into two stages, i.e., the fast activation stage (t ≤4 min) and slow activation stage (t >4 min). The general form of the copper adsorption rate was determined as ΓCu=K1ln(t) +Γ1, which is confirmed by the data fitting of the fast activation stage. The lower activation pH results in higher ion exchange efficiency for Cu substituting Zn. For a strong acid pH of 4.1, the E maintains about 1:1 in the entire activation time range and is not dependent on the activation time. However, the value of E is greater than 1 under weak acidic (pH=6.2) and alkaline (pH=9.1) pH conditions and it significantly depends on the activation time. For such conditions, E decreases with increase in the activation time, which supports the ion exchange mechanism, but within short activation time, it is not a 1:1 ion exchange process.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2018, 54, 2; 377-385
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Selective agglomeration of magnetite in entlandite-serpentine system and implication for their separation
    Autorzy:
    Lu, J.
    Yuan, Z.
    Liu, J.
    Li, L.
    Wang, N.
    Meng, Q.
    Powiązania:
    https://bibliotekanauki.pl/articles/110411.pdf
    Data publikacji:
    2017
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    serpentine
    pentlandite
    magnetite
    selective magnetic agglomeration
    magnetic separation
    Opis:
    In nickel sulfide processing, magnesium silicates (serpentines) can easily form slime coatings or hetero-aggregation on pentlandite surfaces, and hence decrease the pentlandite flotation rate and recovery. In this work, magnetic separation of pentlandite from serpentine using selective magnetic coating through adding magnetite fines as magnetic seeds was investigated. Interactions of magnetite-pentlandite and magnetite-serpentine were calculated by the DLVO (Derjaguin-Landau-Verwey-Overbeek) theory. The results show that the interaction of magnetite-pentlandite was obviously stronger than that of magnetite-serpentine with an external weak magnetic field (4776 A/m-1). Therefore, fine magnetite fractions selectively adhered to the pentlandite surfaces and enhanced its magnetism, resulting in being separated from serpentine by magnetic separation, which was further verified by magnetic coating-magnetic separation and SEM observations.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2017, 53, 2; 943-955
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Water film structure during rupture as revealed by MDS image analysis
    Autorzy:
    Truong, N. T.
    Dang, L. X.
    Lin, C.-L.
    Wang, X.
    Miller, J. D.
    Powiązania:
    https://bibliotekanauki.pl/articles/110251.pdf
    Data publikacji:
    2018
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    image processing
    molecular dynamics simulation
    film stability
    molecular porosity
    Opis:
    The structure of thin water films during the rupture process was investigated by a new approach, which combines molecular dynamics simulation (MDS) with image processing analysis. The analysis procedure was developed to convert MDS trajectories to readable 3D images. The water films were studied at different thicknesses by MDS to determine the critical thickness at which the film ruptures. The potential energy of each specific film thickness during the simulation time was analyzed, and the results showed that the potential energy of stable films remained unchanged while the potential energy kept decreasing for films which ruptured during the simulation time. By applying the new procedure, the molecular porosity, which is defined as the void fraction between the volume of molecular pores in the water film and the total volume of the water film, was calculated. The results of molecular porosity for different film thicknesses during the simulation time suggested a critical molecular porosity as 49%. In other words, stable films have a molecular porosity of less than 49%. If a water film has a molecular porosity greater than 49%, rupture occurs during the simulation.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2018, 54, 4; 1060-1069
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Efficient sulfidization of lead oxide at high temperature using pyrite as vulcanizing reagent
    Autorzy:
    Zheng, Y.-X.
    Lv, J.-F.
    Wang, H.
    Wen, S.-M.
    Huang, L.
    Powiązania:
    https://bibliotekanauki.pl/articles/110351.pdf
    Data publikacji:
    2018
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    lead oxide
    sulfidization roasting
    pyrite
    reaction mechanism
    TG
    Opis:
    A sulfidization roasting-flotation process was usually viewed to be effective in treating the refractory oxide ore. In this paper, pyrite was proposed to be applied as a potential vulcanizing reagent to transform PbO or its surface to PbS based on feasibilities of technology and economy. The evolution process, phase and characteristics of crystal growth were investigated by TG, XRD and SEM-EDS, respectively, to interpret the interaction mechanism of lead oxide and pyrite at high temperature. It was found that the decomposition process of pyrite under argon atmosphere was a slow process of sulfur released from FeS2 to FexS, which made the process easier to be controlled. When PbO was introduced into the system, the initial solid-solid (PbO-FeS2) reaction and prevailing solid-gas (PbO-S2(g)) reaction occurred at about 500 °C and 700 °C, respectively. Combined with the SEM-EDS analyses results, the optimal temperature for the sulfidization of PbO should be in the range of 700-750 °C.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2018, 54, 2; 270-277
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Simultaneous extraction of vanadium and chromium from vanadium slag using low-pressure liquid phase oxidation method
    Autorzy:
    Xia, J.-P.
    Zheng, S.-L.
    Wang, S.-N.
    Liu, B.
    Zou, X.
    Powiązania:
    https://bibliotekanauki.pl/articles/110818.pdf
    Data publikacji:
    2018
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    vanadium slag
    low pressure leaching
    liquid phase oxidation
    kinetics
    Opis:
    A low-pressure liquid oxidation method was proposed and proven to be effective to extract vanadium and chromium simultaneously from the vanadium slag in concentrated NaOH aqueous solutions. The effect of temperature, NaOH mass concentration, liquid-to-solid mass ratio, stirring speed and pressure on the extraction of vanadium and chromium in NaOH aqueous solutions were systematically investigated. Under the optimal reaction conditions (temperature of 473 K, liquid-to-solid mass ratio of 6:1, stirring speed of 700 rpm, NaOH mass concentration of 50%, pressure of 1 MPa and reaction time of 180 min), the vanadium and chromium recovery reached 95% and 90%, respectively. It was found that the reaction temperature and NaOH concentration were important factors for the extraction of vanadium and chromium. The kinetics of the decomposition of vanadium slag in concentrated NaOH aqueous under low pressure was analyzed using the shrinking core model, and the results indicated that the extraction of vanadium and chromium were both governed by the internal diffusion step, with apparent activation energies calculated to be 26.22 and 32.79 kJ/mol, respectively.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2018, 54, 2; 609-619
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Kinetic research of quinoline, pyridine and phenol adsorption on modified coking coal
    Autorzy:
    Sun, X.
    Xu, H.
    Wang, J.
    Ning, K.
    Huang, G.
    Yu, Y.
    Ma, L.
    Powiązania:
    https://bibliotekanauki.pl/articles/110365.pdf
    Data publikacji:
    2018
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    adsorption kinetics
    modification
    coking coal
    coking wastewater
    Opis:
    Adsorption is widely used in wastewater treatment. In this work, the removal of quinoline, pyridine and phenol from coking wastewater by using modified coking coal, which was treated by four different modification methods i.e. acidification sodium hydroxide (5 mol/dm3), hydrochloric acid (5 mol/dm3) and acetic acid (5 mol/dm3) and low-temperature (105 oC) oxidation, was investigated. The modified coal was characterized by the surface area analysis, SEM, total acidity and basicity and FT-IR. The results showed that the surface area from high to low follows the order: modification with acetic acid, modification with hydrochloric acid, raw coal, modification with sodium hydroxide and modification with low-temperature. Experimental data were fitted to pseudo-first-order, pseudo-second-order and intra-particle diffusion. The adsorption of all followed pseudo-second-order kinetics. The result showed that the removal efficiency of coal modified by hydrochloric acid and acetic acid are higher than raw coal, while modified by sodium hydroxide and low-temperature are lower than raw coal., The coal modified by hydroxide acid had the best adsorption capacity.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2018, 54, 3; 965-974
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-8 z 8

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