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    Wyświetlanie 1-11 z 11
    Tytuł:
    Experimental investigation of a high temperature resistant and low friction fracturing fluid
    Autorzy:
    Xiao, B.
    Zhang, S.
    Zhang, J.
    Hou, T.
    Guo, T.
    Powiązania:
    https://bibliotekanauki.pl/articles/109339.pdf
    Data publikacji:
    2015
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    high temperature fracturing fluid
    resistance to shearing
    hydroxypropyl guar
    low friction
    delayed crosslinking
    Opis:
    The performance of a hydraulic fracturing fluid (HFF) system directly determines the efficiency of stimulation. Since the targeted formations of most oil fields in China are characterized by large depth (~5000 m), high temperature (160 to 180 °C) and tight lithology, newer and suitable HFFs have to be developed. Based on a newly synthetized organo-boron/-zirconium cross-linking agent (Gh-g), a composite temperature stabilizer (WJ-6) and other optimized additives via indoor evaluation, this study introduced a novel HFF, which is thermally stable at high temperature (HT) up to 180 °C and exerted low friction pressures. The performance of HFF was evaluated in the laboratory. The experimental results showed that the HFF system performed well at HTs. It maintained a viscosity of 100 mPa•s or more after 90 min of shearing (170 s−1) at 180 °C. Furthermore, the system exhibited delayed cross-linking. It took 120 s for the cross-linking reaction to complete; therefore, the tube friction was reduced to a large extent. Another characteristic feature of the formulated HFF system was the low friction pressures, where the drag reduction percentage was in the range from 35% to 70%. Moreover, only minor damage was caused by the fluid to the formation core samples. The average core permeability damage was 19.6%. All these qualities ensure that this fluid system is in full compliance with the requirements of the fracturing treatment.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2015, 51, 1; 37-47
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effect of two-stage stirred pulp-mixing on coal flotation
    Autorzy:
    Gui, X.
    Wang, Y.
    Zhang, H.
    Li, S.
    Powiązania:
    https://bibliotekanauki.pl/articles/110764.pdf
    Data publikacji:
    2014
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    mixing
    stirred
    two stage
    fine coal
    flotation
    Opis:
    Stirred pulp-mixing is performed before coal flotation. In this study, a two-stage stirred pulpmixing tank was designed based on the single-stirred process to intensify the mixing effect of pulp and flotation reagents. A tank has a pitched-impeller opening-type turbine. Stirred pulp-mixing and flotation experiments were conducted on a sample of anthracite fine coal (-0.5mm) from the Xuehu Coal Preparation Plant in Henan Province, China. The results of the two-stage stirred pulp-mixing were compared with those of a single-stage stirred pulp-mixing in terms of flotation performance. Compared with the single-stage stirred pulp-mixing, two mixing areas and double-layer impeller were able to strengthen the energy input to the stirred system, thereby improving the mixing efficiency of flotation reagents and coal particles in the pulp. The two-stage stirred pulp-mixing significantly increased the flotation feed rate of the cyclone-static micro-bubble flotation column and concentrate yield, enhanced the combustible matter recovery effect of coarse particles at a suitable flotation feed rate, and ensured the recovery effect of fine particles at high flotation feed rate.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2014, 50, 1; 299-310
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Pre-concentration of vanadium-bearing mica from stone coal by roasting-flotation
    Autorzy:
    Tang, J.
    Zhang, Y.
    Bao, S.
    Liu, C.
    Powiązania:
    https://bibliotekanauki.pl/articles/109373.pdf
    Data publikacji:
    2017
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    roasting
    flotation
    vanadium bearing mica
    stone coal
    Opis:
    In China, stone coal is an important source of vanadium. The use of roasting–floatation for the pre-concentration of vanadium bearing mica from vanadium bearing stone coal was investigated based on its mineralogical characteristics. The results showed that the vanadium occurred in mica minerals and the main gangue minerals were coal, calcite, and quartz. The pre-concentration process comprises three key steps: roasting, desliming, and flotation. The coal was completely removed by roasting at 700 °C for an hour. Slime was concentrated and the subsequent flotation pulp was improved by desliming. Calcite was removed by reverse flotation and mica was concentrated by positive floatation. During the process, the grade of V2O5 was increased from 0.71% to 1.14%, and 46.18% of the tailings were rejected. The leaching rate of vanadium was increased from 30.49% of raw ore to 69.15% of the concentrate which was an increase of about 40% at the same leaching process. This technique may promote the efficient utilization of stone coal resources.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2017, 53, 1; 402-412
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Depression effect of corn starch on muscovite mica at different pH values
    Autorzy:
    Peng, W.
    Zhang, L.
    Qiu, Y.
    Song, S.
    Powiązania:
    https://bibliotekanauki.pl/articles/110573.pdf
    Data publikacji:
    2016
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    muscovite mica
    corn starch
    pulp pH
    depression effect
    Opis:
    The depression effect of corn starch on the surface of muscovite mica powder at different pulp pH value was investigated. The experiments were performed on single mineral, and its flotation performance was studied by flotation tests, adsorption quantity measurement, zeta-potential technique and Fourier transform infrared (FT-IR). The results indicated that the depression effect was varied with the pulp pH value when dodecylamine chloride (DDA) was used as collector, the strongest inhibitory effect appeared at pH 2 and the zeta-potential of muscovite mica increased overall after conditioned with corn starch solution. It was confirmed by the FT-IR spectra that the corn starch indeed adsorbed on the surface of muscovite mica powder and physical adsorption was occurred between muscovite mica and corn starch. This study leads to a better understanding of the depression effect of corn starch on the surface of muscovite mica powder.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2016, 52, 2; 780-788
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Flotation behaviour and surface characteristic of anosovite in a sodium oleate solution
    Autorzy:
    Wang, Y.
    Wen, S.
    Zhang, J.
    Wu, D.
    Xian, Y.
    Shen, H.
    Powiązania:
    https://bibliotekanauki.pl/articles/110766.pdf
    Data publikacji:
    2017
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    anosovite
    sodium oleate
    flotation
    adsorption
    Opis:
    Properties of anosovite in titanium slag, anosovite flotation response in a collector solution of sodium oleate, and adsorption behaviour of sodium oleate on the mineral surface were studied in the present work using XRD, Raman spectra, flotation tests, zeta potential analysis, FTIR and XPS. The results show that the anosovite crystal contains magnesium, and its chemical composition is Mg0.09Ti2.91O5. The chemical bonds on the anosovite surface mainly comprise Ti-O bonds. Micro-flotation tests indicate that anosovite has better floatability at a wide pH range and the recovery reaches 88% at pH=6, when the dosage of sodium oleate is only 4·10−6 mol/dm3. The point of zero charge of anosovite was determined near pH 3.2 by the zeta potential measurement. In the flotation process, chemical adsorption occurs between the carboxyl of sodium oleate and the titanium sites on the anosovite surface.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2017, 53, 2; 714-723
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Flotation behavior of hard-to-separate and high-ash fine coal
    Autorzy:
    Xing, Y.
    Gui, X.
    Liu, J.
    Cao, Y.
    Zhang, Y.
    Li, S.
    Powiązania:
    https://bibliotekanauki.pl/articles/110585.pdf
    Data publikacji:
    2016
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    flotation behavior
    fine coal
    Fuerstenau upgrading curve
    energy input
    selectivity
    Opis:
    The flotation behavior of hard-to-separate and high-ash fine coal was investigated using conventional flotation with constant power input. A new flotation process, based on energy input and distribution, was designed to lower the ash content of concentrate. The results obtained using Fourier transform infrared (FTIR) analysis show that the coal samples have good floatability because of many hydrophobic and few hydrophilic functional groups. Under a constant power input, a large number of ash-forming materials floated into a froth product at the start of flotation. Based on the Fuerstenau upgrading curves, it was determined that the 0.25-0.074 mm size fraction range showed the worst selectivity when compared with 0.50-0.25 mm and -0.074 mm size fractions. The desired concentrate with an ash content of 13.98%, 27.59% of ash recovery, and 80.01% combustible matter recovery could be obtained by transferring the excess energy of the flotation-conditioning stage to the pre-conditioning stage and increasing the power input step-by-step in the flotation-conditioning stage at equal total energy consumption.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2016, 52, 2; 703-717
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Role of dissolved mineral species in quartz flotation and siderite solubility simulation
    Autorzy:
    Luo, X.
    Wang, Y.
    Ma, M.
    Song, S.
    Zhang, Y.
    Deng, J.
    Liu, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/109459.pdf
    Data publikacji:
    2017
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    quartz
    solubility
    siderite
    calcium ion
    temperature
    flotation
    Opis:
    Quartz is, in most cases, the major gangue mineral found in the iron ores. Although it can be activated by calcium at strong alkaline pH, quartz nevertheless, reports to the concentrate with Fe when the iron ores contain siderite. It causes a poor concentrate grade and separation between quartz and iron minerals. The effect of siderite on reverse anionic flotation of quartz from hematite was studied in our previous investigations. In this work, the effect of siderite dissolution on the quartz recovery in the froth product and the effect of pH, ions and temperature on siderite dissolution were investigated. Microflotation, PHREEQC simulation, solution chemistry calculation and Fourier transform infrared spectroscopy (FTIR) measurements were conducted. It was observed that the dissolved species of siderite exhibited negative impact on quartz flotation. This influence became weak to some extent by either stripping the dissolved species or shortening dissolution time. Siderite was easily dissolved in the presence of calcium ion under strong alkaline conditions and its solubility increased with increasing the calcium ion concentrate and temperature. When the calcium ion was added as an activator of quartz under strong alkaline conditions (pH>9.96), calcium existed mainly in the CaCO3 precipitation form according to the solubility rule in the presence of siderite. This form could adsorb onto quartz surfaces and further the chemical reaction between starch and quartz was monitored by FTIR measurements. This study provides a further supplement for previous study. A potential strategy is suggested that finding a collector used at low temperature or flotation under neutral (or weak alkaline) medium is helpful to the reverse flotation of iron ores containing siderite.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2017, 53, 2; 1241-1254
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Kinetics and mechanism of one-step reductive leaching of manganese oxide ores by EDTA/EDTA-2Na
    Autorzy:
    Zhang, C.
    Wang, S.
    Cao, Z.
    Zhong, H.
    Powiązania:
    https://bibliotekanauki.pl/articles/109834.pdf
    Data publikacji:
    2018
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    kinetics
    EDTA
    reductive leaching
    manganese oxide ores
    EDTA-2Na
    Opis:
    In this research, the kinetics and mechanism of one-step reductive leaching of manganese oxide ores by ethylenediaminetetraacetic acid (EDTA) or its disodium salt (EDTA-2Na) in an aqueous medium have been investigated. The kinetic data of this reductive leaching process may be described by the Avrami model, and the apparent activation energy was determined to be 15.8 kJ·mol-1/7.9 kJ·mol-1 for leaching by EDTA/EDTA-2Na with a reaction order of -1.7/2.0. The EDTA/EDTA-2Na leach liquor characterized and analyzed by X-ray photoelectron spectra (XPS), Fourier transform infrared spectra (FTIR), and total organic carbon (TOC) determination denoted that the oxidation-reduction reaction happened between manganese(IV) and EDTA/EDTA-2Na, and a coordination complex, EDTA-manganese(II/III) formed. This new process can be easily used to leach manganese from manganese oxide ores in a moderate environment with the pH range of 5–8.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2018, 54, 3; 858-867
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Ammonium chloride’s weakening effect on the copper activation of pyrite in flotation and the surface regulation mechanism behind it
    Autorzy:
    Zhang, Shengdong
    Chen, Yumeng
    Tong, Xiong
    Xie, Xian
    Lu, Yalin
    Powiązania:
    https://bibliotekanauki.pl/articles/110323.pdf
    Data publikacji:
    2019
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    pyrite
    depression
    cuprammonium solution
    pH buffering property
    flotation
    Opis:
    The traditional separation process of pyrite and marmatite is carried out under highly alkaline conditions. Therefore, a large amount of lime is demanded and the zinc recovery cannot be guaranteed. However, under weakly alkaline conditions, copper-activated pyrite has good floatability, which is difficult to separate from marmatite. In this paper, ammonium chloride (NH4Cl) is used for depressing the flotation of copper-activated pyrite to achieve the separation of these two minerals under weakly alkaline environment. The flotation tests show that NH4Cl can significantly reduce the floatability of pyrite in weakly alkaline conditions. The results of adsorption tests and X-ray photoelectron spectroscopy (XPS) analyses indicate that NH4Cl can obviously change the composition of pyrite surface by increasing the content of iron/copper hydroxide and reducing the content of copper sulfides. Calculation of the solution composition demonstrates that the addition of NH4Cl results in the occurrence of Cu(NH3)n2+ and the pH buffering property. Based on these results, it can be concluded that the depression of NH4Cl on copper activated pyrite is mainly derived from two aspects: 1) the pH buffering property of the conjugated acid-base pair (NH4+/NH3) can impede the decline of OH- concentration, which results in more hydroxide adsorbed on pyrite; 2) NH3 (aq) competes with the pyrite surface to consume Cu2+through complexation, which causes a reduction in the amount of copper sulfides formed on the pyrite surface.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2019, 55, 5; 1070-1081
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Response of energy-size reduction to the control of circulating load in vertical spindle pulverizer
    Autorzy:
    Li, H.
    He, Y.
    Zhang, Y.
    Ge, Z.
    Xie, W.
    Wang, S.
    Li, K.
    Powiązania:
    https://bibliotekanauki.pl/articles/110803.pdf
    Data publikacji:
    2017
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    circulating load control
    response of energy-size reduction
    mixture grinding
    energy efficiency
    Opis:
    In the vertical spindle pulverizer (VSP), the large circulation ratio and high ash and sulfur contents in circulating load would result in intensive energy consumption and low grinding efficiency. Although the control of circulating load would help increase the energy efficiency, no quantitative study has been conducted due to the high temperature and pressure in the closed VSP. In this study, response of energy-size reduction to the control of circulating load was studied by the experimental simulation method. Coal mixtures with fine/coarse ratio of 11:1, 8:1 and 6:1 were ground by a lab-scale roller mill. Energy-size reductions of the coarse coal were compared to evaluate the influence of circulating load control. Results showed that the product with the coarse coal increased by 30% when the specific breakage energy was 1.0 kWht–1 as the circulation ratio decreased from 11 to 6. Meanwhile, a breakage characteristic index of the coarse coal was two times higher due to the cushioning effect of fines. Besides, decrease of circulation ratio led to increase of the breakage rate of coarse coal, and the energy saving improved by 57%. With the same energy input of 2.0 kWht-1, the yield of –0.09 mm pulverized fuel (PF) increased from 22 to 43%. Therefore, controlling the circulating load is an effective method to improve the breakage rate of coarse coal and energy efficiency for PF generation.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2017, 53, 2; 793-801
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Regional features analysis of plugged holes of dense phase gas-solid separation fluidized bed
    Autorzy:
    Zhang, B.
    Zhao, Y.
    Luo, Z.
    Song, S.
    Duan, C.
    Dong, L.
    Powiązania:
    https://bibliotekanauki.pl/articles/109699.pdf
    Data publikacji:
    2014
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    gas-solid fluidized bed for separation
    pressure fluctuation
    plugged holes regions
    features analysis
    plugged holes sensitivity
    Opis:
    In contrast to traditional coal separation, dry separation does not require water and does not cause water pollution. Dense phase gas–solid fluidized beds are used for dry separation. The plugged holes in the air distributor should be tested to ensure the stability of these beds for particle separation. The pressure fluctuation is sensitive to these plugged holes. This sensitivity can be tested and diagnosed by determining the standard deviation of the pressure fluctuation. In areas with partial blockage, that is the areas with weak fluidization, a decrease in the volume fraction of the particles and in the pressure differences in the transverse of the bed results in an increase of the standard deviation of the pressure fluctuation, thereby stimulating the lateral mixing of medium-sized particles. The standard deviation and the mixing intensity decrease axially. The value of sensitivity of the plugged holes in the air distributor decreases as the height of the bed increases. The features of air distributors affect the surrounding areas. The distribution law determining the influence of plugged holes on the beds is symmetrical. As the blockage of the fluidized bed distributor region increases, the mean square error of the pressure fluctuation in the related regions increases. The intensity of the effect is proportional to the distance to the plugged holes.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2014, 50, 2; 667-679
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-11 z 11

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