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    Wyświetlanie 1-9 z 9
    Tytuł:
    Extraction and separation of zinc, lead, silver, and bismuth from bismuth slag
    Autorzy:
    Xing, Peng
    Ma, Baozhong
    Wang, Chengyan
    Chen, Yongqiang
    Powiązania:
    https://bibliotekanauki.pl/articles/109744.pdf
    Data publikacji:
    2019
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    bismuth
    zinc
    lead
    silver
    extraction
    separation
    Opis:
    The present paper deals with the extraction and separation of zinc, lead, silver, and bismuth from a refractory bismuth refining slag via a hydrometallurgical route. The process consists of a preliminary leaching of zinc with water, followed by the selective leaching of lead and silver with a calcium chloride solution, leading to the crystallization of lead chloride and the cementation of silver. The diagrams of the total concentrations of [Pb]/[Ag] versus [Cl-] and temperature in the Pb/Ag-Cl-H2O system were drawn, respectively, to determine the optimum concentration of leaching agent and leaching temperature. The potential-pH diagram of the Pb/Ag/Bi-H2O system indicates that the preferential leaching of lead and silver could be achieved. Finally, 98.8% of lead and 90.4% of silver were selectively removed by further leaching the water leaching residue with 400 g/dm3 of CaCl2 solution at pH 4.5 and 80 °C, while only 3.7% of bismuth was leached in this stage. Fifty-nine percent of lead in the leach liquor was separated out as PbCl2 by natural cooling. Ninety-five percent of silver in mother liquor was recovered by cementation with a lead sheet. The depleted CaCl2 solution can be sent to the leaching step again to close the loop.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2019, 55, 1; 173-183
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Classification techniques and parameter optimization of Cyclone Continuous Centrifugal Separator for hematite ore
    Autorzy:
    Zhang, Pei
    Xie, Haiyun
    Jin, Yanling
    Chen, Jialing
    Zeng, Peng
    Li, Yuanhong
    Chen, Luzheng
    Liu, Dianwen
    Powiązania:
    https://bibliotekanauki.pl/articles/2200335.pdf
    Data publikacji:
    2023
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    hematite
    Cyclonic Continuous Centrifugal Separator
    CCCS
    classification
    Response Surface Methodology
    Opis:
    The Cyclonic Continuous Centrifugal Separator (CCCS) is a new type of separation equipment developed based on cyclonic continuous centrifugal separation technology and combined with the separation principle of the fluidized bed. Taking hematite as the research object, the main parameters and conditions of the best hematite classification were determined through the classification test by using CCCS. Based on the classification test, the significance order of each process parameter and their interaction with hematite classification efficiency of the underflow products was analyzed with the Response Surface Methodology, the optimal process parameter of hematite classification was obtained and a multiple regression equation was established. The optimized process conditions were as follows, feeding pressure 55.48 kPa, backwash pressure 9.79 kPa, and underflow pressure 31.94 kPa. Under these conditions, the average hematite ore classification efficiency of coarse fraction (-2~+0.15mm), medium fraction (-0.15~+0.074mm) and fine fraction (-0.074mm) were 85.08%, 65.10% and 51.41%, respectively, and the relative errors with the predicted values were 1.6%, 4.0% and 2.5%, respectively. The results showed that the analytical model has good predictive performance. This research provides a certain prospect for the application of Cyclonic Continuous Centrifugal Separation to hematite ore classification. it provides a reference for the application of the Response Surface Methodology in the classification of hematite by Cyclonic Continuous Centrifugal Separation.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2023, 59, 1; art. no. 158864
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    New insights into the promotion mechanism of $(NH_4)_2SO_4$ in sulfidization flotation: a combined experimental and computational study
    Autorzy:
    Chen, Daixiong
    Liu, Mengfei
    Hu, Bo
    Dong, Yanhong
    Xue, Wei
    He, Peng
    Chen, Fang
    Zhu, Jianyu
    Zhang, Chenyang
    Powiązania:
    https://bibliotekanauki.pl/articles/1446762.pdf
    Data publikacji:
    2021
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    malachite
    promotion
    sulfidization
    flotation
    mechanism
    Opis:
    Ammonium sulfate ((NH4)2SO4) exhibits promoting effects in malachite sulfidization flotation. However, the promotion mechanism remains poorly understood. In this study, micro-flotation tests, zeta-potential measurements, scanning electron microscopy coupled with energy-dispersive spectroscopy (SEM-EDS), atomic force microscopy (AFM), X-ray photoelectron spectroscopy (XPS) and materials studio simulation (DFT) were used to investigated the promotion mechanism of $(NH_4)_2SO_4$. Micro-flotation test demonstrates that the recovery of malachite from 73% increased to 83%, when the (NH4)2SO4 was added. Contact angle and zeta potential test results indicate that addition of $Na_2S•9H_2O$ changes the surface properties of malachite and provide the conditions for adsorption of butyl xanthate (BX). After promoting the sulfidization by $(NH_4)_2SO_4$, BX is more effective in improving the hydrophobicity. SEM-EDS and AFM results show that $(NH_4)_2SO_4$ can improve performance and stability of sulfidization. X-ray photoelectron spectroscopy indicates that after sulfidization, polysulfides and cuprous were appeared in malachite surface, infers that a redox reaction occurs between sulfur and copper on the surface of malachite. After addition of $(NH_4)_2SO_4$, the percentage of polysulfides and cuprous were increased, it implies $(NH_4)_2SO_4$ can accelerate the redox reaction. Computational results show that after adding $(NH_4)_2SO_4$, the adsorption energy of HS- on the malachite surface is reduced, implies that $(NH_4)_2SO_4$ can improve the stability of HS-adsorption on the surface of malachite.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2021, 57, 5; 57-70
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Study on the mechanism and kinetics of sulfuric acid leaching scandium from rich scandium anatase
    Autorzy:
    He, Fei
    Gao, Likun
    Chen, Long
    Rao, Bing
    Shen, Hairong
    Peng, Kebo
    Gao, Guangyan
    Powiązania:
    https://bibliotekanauki.pl/articles/2146896.pdf
    Data publikacji:
    2022
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    anatase ore
    sulfuric acid
    leaching
    kinetics
    scandium
    Opis:
    Scandium and its compounds have excellent properties, and are widely used in cutting-edge fields such as optics, electronics, and alloys. Thus, scandium is an important strategic metal. However, scandium is extremely sparsely distributed in the earth's crust, rarely occurs as an independent mineral, and requires a complex recovery process. Therefore, the study of the extraction of scandium is of great practical significance. This study examined the leaching test and kinetics of scandium under the acid leaching system of refractory anatase ore. Under appropriate two-stage countercurrent leaching conditions, the first stage of the particle size of fraction of -0.074 mm 82.6%, initial H2SO4 concentration of 6 mol/L, leaching temperature of 100 °C, acid/solid ratio of 3 ml/g, stirring speed of 300 rpm, and leaching time of 50 min; and the second stage of the initial H2SO4 concentration of 11 mol/L, leaching temperature of 150 °C, acid/solid ratio of 4 ml/g, stirring speed of 300 rpm, and leaching time of 50 min, a scandium leaching rate of 96.98% was achieved. The kinetics of scandium leaching conformed to a shrinking-core model, and sulfuric acid concentration and temperature were the most important parameters affecting the scandium leaching rate. The kinetic analysis of scandium leaching at different sulfuric acid concentrations showed that as the concentration increased, the sulfuric acid leaching of scandium changed from being chemical reaction-controlled to internal diffusion-controlled, and the apparent reaction order was 1.2429. The kinetics of scandium leaching at different temperatures showed that the sulfuric acid leaching of scandium was reaction-controlled and the apparent activation energy was 42.21 kJ-mol-1.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2022, 58, 3; art. no. 146171
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effect of preoxidation on copper flotation from copper-lead mixed concentrate
    Autorzy:
    Peng, Zeng
    Haiyun, Xie
    Yanling, Jin
    Pei, Zhang
    Jialing, Chen
    Liu, Dianwen
    Powiązania:
    https://bibliotekanauki.pl/articles/24085956.pdf
    Data publikacji:
    2023
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    copper-lead mixed concentrate
    peroxidation
    separation of copper and lead
    response surface methodology
    Opis:
    Flotation separation of galena and chalcopyrite is always a difficult problem in mineral processing. In this paper, the selective preoxidation of galena and chalcopyrite with sulfuric acid was developed, and then the two minerals were completely separated by flotation. The surface oxidation mechanism of galena and chalcopyrite with sulfuric acid was analyzed by Fourier transform infrared spectroscopy (FT-IR) and Atomic Force Microscopy (AFM), and the results showed that hydrophilic oxide film was formed on the galena surface, while the surface of chalcopyrite is still hydrophobic sulfide film, which led to the separation of the two minerals by flotation. In addition, the Response Surface Methodology (RSM) was used to analyze the influence of main preoxidation parameters on the flotation separation of copper-lead concentrate, and the parameters were further optimized, as follows: sulfuric acid concentration of 5.3 mol/L, oxidation temperature of 101.8 °C and time of 48.3 min. The mixed concentrate containing Cu 11.57% and Pb 16.75% was preoxidized under the above conditions, and the flotation separation verification results showed that Cu concentrate with Cu grade of 18.09% and recovery of 95.41%, and Pb concentrate with Pb grade of 44.96% and recovery of 95.94% was obtained respectively. This paper provides a new method of preoxidation combined flotation to achieve high-efficiency separation of copper-lead mixed concentrate.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2023, 59, 2; art. no. 163253
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    A novel process for extraction of iron from a refractory red mud
    Autorzy:
    Ding, Wei
    Xiao, Junhui
    Peng, Yang
    Shen, Siyue
    Chen, Tao
    Zou, Kai
    Wang, Zhen
    Powiązania:
    https://bibliotekanauki.pl/articles/1450194.pdf
    Data publikacji:
    2020
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    red mud
    sodium sulfate
    segregation roasting
    magnetic separation
    iron recovery
    Opis:
    Red mud is a kind of solid waste produced during alumina extraction from bauxite. To extraction valuable iron from red mud, the technology of adding sodium sulfate-segregation roasting-magnetic separation to treat red mud was developed. During the paper, the effects of various process parameters on the extraction of iron by segregation roasting-magnetic separation were studied, and the phase transformation behavior and microstructure of iron are explored. Repeated test results showed that magnetic concentrate (mass percent), TFe of 80.29 % and overall iron recovery of 92.08 %was obtained. The X-ray diffraction (XRD) and scanning electron microscopy (SEM) results indicated that after the segregation roasting, the hematite was transformed into a new metal phase consisting mainly of metallic iron and magnetite. The addition of sodium sulfate during the segregation roasting can obviously improve the efficiency of segregation roasting-magnetic separation for iron extraction.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2020, 56, 6; 125-136
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Comparison of mechanical flotation cell and cyclonic microbubble flotation column in terms of separation performance for fine graphite
    Autorzy:
    Bu, X.
    Zhang, T.
    Chen, Y.
    Peng, Y.
    Xie, G.
    Wu, E.
    Powiązania:
    https://bibliotekanauki.pl/articles/110791.pdf
    Data publikacji:
    2018
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    mechanical flotation
    column flotation
    Fuerstenau upgrading curve
    graphite
    Opis:
    Comparison of flotation performance between the flotation column and mechanical flotation was carried out to promote the grade and economic value of the graphite ore (15.40% ash content). The ash content of the concentrate of the mechanical flotation was 10.77% at the yield of 79.34%. In contrast, the yield of the concentrate of the column flotation was increased to 88.93% with 10.55% ash content. Comparative study of the Fuerstenau upgrading curves indicated that the column flotation was more efficient for cleaning the graphite ore in the presence of the centrifugal force field, nanobubbles (generated by hydrodynamic cavitation), and the thicker froth layer in comparison with the mechanical flotation.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2018, 54, 3; 732-740
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Reverse flotation of collophanite at natural pH using isooctyl polyoxyethylene ether phosphate as a collector
    Autorzy:
    Li, Hongqiang
    Zhang, Wen
    Chen, Qian
    Huang, Peng
    Kasomo, Richard M.
    Zou, Ze
    Weng, Xiaoqing
    He, Dongsheng
    Yang, Siyuan
    Song, Shaoxian
    Powiązania:
    https://bibliotekanauki.pl/articles/1445877.pdf
    Data publikacji:
    2021
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    reverse flotation
    dolomite
    fluorapatite
    AEP
    selective adsorption
    Opis:
    Reverse flotation of collophanite at natural pH could significantly decrease the cost of pH regulators. In this study, isooctyl polyoxyethylene ether phosphate (AEP) was tested as a new surfactant in the reverse flotation of collophanite. Micro-flotation tests were conducted, and the adsorption mechanism of the new collector was analysed using X-ray photoelectron spectroscopy (XPS) and zeta potential analyses. The results of the flotation tests demonstrated that AEP could enable dolomite to float under natural pH (pH=7.2) and showed profound selectivity towards dolomite as opposed to fluorapatite. Based on the zeta potential and XPS results, the adsorption phenomena are mainly attributed to calcium active sites on both mineral surfaces. Dolomite possesses more magnesium active sites than fluorapatite, which tend to reinforce the interaction effect between AEP and dolomite. Furthermore, when compared to CO32- ions on the dolomite surface, PO43- ions on the fluorapatite surface tend to exhibit a stronger hindrance to the adsorption of AEP on the fluorapatite surface. This is attributed to their larger volumes and more charges on their surfaces, thereby causing a floatability difference between the two minerals.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2021, 57, 4; 78-86
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Study on separation of fine-particle ilmenite and mechanism using flocculation flotation with sodium oleate and polyacrylamide
    Autorzy:
    Peng, Yang
    Xiao, Junhui
    Deng, Bing
    Wang, Zhen
    Liu, Nengyun
    Yang, Daoguang
    Ding, Wei
    Chen, Tao
    Wu, Qiang
    Powiązania:
    https://bibliotekanauki.pl/articles/1450088.pdf
    Data publikacji:
    2020
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    sodium oleate
    polyacrylamide
    synergistic effect
    ilmenite
    flocculation flotation
    Opis:
    In this paper, sodium oleate, polyacrylamide, soluble starch and sodium carboxymethyl cellulose were used as flocculants to study the flocculation and sedimentation behavior of microfine ilmenite. Sedimentation test shows that sodium oleate and polyacrylamide have good flocculation effect on ultrafine ilmenite. The flocculation rate of ilmenite can be further improved by the combination of sodium oleate and polyacrylamide. It was found that both flocculants could generate chemical adsorption with ilmenite surface, and they all react with $Fe^{3+}$ on ilmenite surface. However, sodium oleate reacts with $Fe^{3+}$ to form a water-insoluble iron oleate precipitate which coats the surface of the ilmenite and hinders the action of polyacrylamide and the remaining $Fe^{3+}$. This problem can be avoided by adding polyacrylamide followed by sodium oleate, and the flotation recovery can be increased significantly.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2020, 56, 1; 161-172
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-9 z 9

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