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Wyświetlanie 1-4 z 4
Tytuł:
Nanopores with controlled profiles in track - etched membranes
Autorzy:
Sartowska, B. A.
Powiązania:
https://bibliotekanauki.pl/articles/146896.pdf
Data publikacji:
2012
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
nanopore
scanning electron microscopy (SEM)
surfactant
track-etched membranes (TMs)
Opis:
Track-etched membranes are porous systems consisting of a polymer foil with thin channels-pores - from surface to surface. The increasing interest in this kind of material is connected with the development of nanoporous materials with unique properties such as diode-like effects in membranes with highly asymmetrical nanopores. The materials can be used for molecular sensors and atom beam optics, development of nanocapillary bodies for modelling the transport of molecules and ions in constrained volumes. Control over pore geometry opens the way to a number of new applications of track-etch membranes (TMs). The nanopores were obtained by the ion-track etching method using surfactant-doped alkaline solutions. Control over the pore profile and dimensions was achieved by varying the alkali concentration in the etchant and the etching time. The pore geometry was characterized in detail using field-emission scanning electron microscopy (SEM). SEM images of the surfaces and cleavages of TMs with different pore morphology are shown.
Źródło:
Nukleonika; 2012, 57, 4; 575-579
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The origin and chronology of medieval silver coins based on the analysis of chemical composition
Autorzy:
Pańczyk, E.
Sartowska, B.
Waliś, L.
Dudek, J.
Weker, W.
Widawski, M.
Powiązania:
https://bibliotekanauki.pl/articles/147506.pdf
Data publikacji:
2015
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
elemental composition
medieval Central Europe coins
scanning electron microscopy (SEM)
laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS)
numismatists
Opis:
Medieval Central Europe coins – the Saxon coins, also called as the Otto and Adelheid denarii, as well as the Polish ones, the Władysław Herman and Bolesław Śmiały coins – were examined to determine their provenance and dating. Their attribution and chronology often constitute a serious problem for historians and numismatists. For hundreds of years, coins were in uncontrolled conditions and in variable environment. Destructed and inhomogeneous surface were the effect of corrosion processes. Electron microscopy with energy dispersive X-ray analysis (scanning electron microscopy with energy dispersive X-ray spectroscopy (SEM-EDS)), X-ray fluorescence (XRF) analysis (energy dispersive X-ray fluorescence (EDXRF) and total reflection X-ray fluorescence (TXRF)), and laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS) were applied. The results of these investigations are significant for our knowledge of the history of Central European coinage, especially of Polish coinage.
Źródło:
Nukleonika; 2015, 60, No. 3, part 2; 657-663
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Atomic force microscopy investigation of electron beam (EB) irradiated composites based on biodegradable polymers and coconut fiber*
Autorzy:
Kodama, Y.
Oishi, A.
Nagasawa, N.
Nakayama, K.
Tamada, M.
Machado, L. D. B.
Powiązania:
https://bibliotekanauki.pl/articles/147470.pdf
Data publikacji:
2013
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
atomic force microscopy (AFM)
coconut fiber
electron beam (EB) radiation
force modulation microscopy (FMM)
poly(ε-caprolactone) (PCL)
poly(L-lactic acid) (PLLA)
scanning electron microscopy (SEM)
Opis:
In this study, the addition of natural fibers to biodegradable PCL, PLLA blend and the effect of ionizing radiation on the surface of composites were investigated by force modulation microscopy (FMM), atomic force microscopy (AFM) and scanning electron microscopy (SEM). Hot pressed sheets were prepared using pellets of twin extruded PCL:PLLA 20:80 (w:w) blend containing 5% or 10% weight concentration of coconut fiber. In this study coconut fibers non treated chemically and acetylated ones were used. Irradiation was performed using an electron beam (EB) accelerator and an absorbed dose of 100 kGy. FMM images acquisition was obtained using a silicon cantilever, intermittent contact mode (tapping mode). Also, AFM images were obtained using tapping mode but J scanner. By FMM, it was possible to observe regions with different elasticity indicating fiber presence under the surface of the composite. Furthermore, it appears that the spherical structures size decreased on composites. This probably was induced by ionizing radiation.
Źródło:
Nukleonika; 2013, 58, 4; 459-468
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
X-ray techniques in the investigation of a Gothic sculpture : the risen Christ
Autorzy:
Mikołajska, A.
Walczak, M.
Kaszowska, Z.
Urbańczyk-Zawadzka, M.
Powiązania:
https://bibliotekanauki.pl/articles/146866.pdf
Data publikacji:
2012
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
cultural heritage
X-ray image
X-ray dual source computed tomography (DSCT)
scanning electron microscopy energy dispersed X-ray spectroscopy (SEM-EDX)
Opis:
For over a century, X-ray radiation has played an important role in the area of the conservation and restoration of cultural heritage objects. X-ray techniques are amongst the most fundamental and helpful methods used in the investigation of art works. This paper reviews the application of traditional radiography, X-ray dual source computed tomography (DSCT) and scanning electron microscopy combined with energy dispersed X-ray spectroscopy (SEM-EDX) to the investigation of a wooden, Gothic sculpture, The risen Christ. Thanks to the properties of X-ray radiation (different absorption by various materials) first two methods allow the assessment of the preservation state and the observation of the internal structure of an object in 3-D. While SEM-EDX analysis permits the elemental analysis of the polychrome layers. As a result 2-D and 3-D images, permitting the full volume inspection of an object, were taken in a totally non-destructive way. The morphological and physical information about the inner structure of the investigated wooden sculpture was obtained, revealing changes related to previous restorations, as well as ageing effects. Employing the SEM-EDX, painting materials (pigments and filers), were identified. Gained data is essential for restorers to understand the whole structure of the studied object and to decide which further investigation and restoration steps have to be undertaken.
Źródło:
Nukleonika; 2012, 57, 4; 627-631
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
    Wyświetlanie 1-4 z 4

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