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Wyświetlanie 1-15 z 84
Tytuł:
The effect of SO3-Ph-BTBP on stainless steel corrosion in nitric acid
Autorzy:
Wilbraham, R. J.
Boxall, C.
Powiązania:
https://bibliotekanauki.pl/articles/147906.pdf
Data publikacji:
2015
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
corrosion
stainless steel
electrochemistry
6,6'-bis(1,2,4-triazin-3-yl)-2,2'-bipyridine
Opis:
SO3-Ph-BTBP is a hydrophilic tetra-N-dentate ligand proposed for An(III)/Ln(III) separation by solvent extraction, and a candidate for use in future advanced reprocessing schemes such as GANEX and SANEX. We present the first study of the effect of SO3-Ph-BTBP on the corrosion behavior of stainless steels. Specifically, studies have been performed using steels and conditions equivalent to those found in relevant nuclear reprocessing flow sheets. SO3-Ph-BTBP has been shown to have little effect on either steel passivation or reductive dissolution. However, if driven cathodically into a region of hydrogen evolution at the electrode surface or conversely anodically into a region of transpassive dissolution, observed currents are reduced in the presence of SO3-Ph-BTBP, suggesting corrosion inhibition of the steel potentially through weak absorption of a SO3-Ph- -BTBP layer at the metal-solution interface. The lack of any observed corrosion acceleration via complexation of Fe3+ is surprising and has been suggested to be due to the slow extraction kinetics of SO3-Ph-BTBP as a result of a requirement for a trans- to cis-conformational change before binding.
Źródło:
Nukleonika; 2015, 60, No. 4, part 2; 865-869
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Mössbauer study of vacuum annealed Fe100-xGax (10 less - than or equal to x less - than or equal to 35) thin films
Autorzy:
Szumiata, T.
Górka, B.
Brzózka, K.
Gawroński, M.
Gzik-Szumiata, M.
Javed, A.
Morley, N. A.
Gibbs, M. R. J.
Powiązania:
https://bibliotekanauki.pl/articles/147332.pdf
Data publikacji:
2013
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
Fe-Ga
thin films
CEMS
MOKE
Opis:
This work reports results from comparative Mossbauer studies of as-deposited and annealed Fe100.xGax (10 less - than or equal to x less - than or equal to 35) high magnetostrictive thin films of constant thickness (50 plus or minus 2 nm). Films were grown on Si(100) substrates using a co-sputtering and evaporation chamber where Fe has been sputtered and Ga was evaporated. During growth of films, a magnetic field of 65 kA/m has been applied in the plane of the film. Annealed films have been obtained by heating in vacuum for 1 h at 350 centigrade without magnetic field. After annealing, the saturation field of the Fe-Ga films has been significantly reduced. By means of the 57Fe CEMS technique the contributions from several phases have been found: Fe-Ga A2 (bcc), traces of DO3 phase, a gallium-rich disordered phase and iron oxides (both geothite and magnetite). For the sample with x = 26.5 the heat treatment reduces the DO3 phase content whereas for the film with x = 16.4 the opposite tendency has been observed. Mossbauer results were compared with XRD and MOKE findings.
Źródło:
Nukleonika; 2013, 58, 1; 27-30
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Generation of shock waves in dense plasmas by high-intensity laser pulses
Autorzy:
Pasley, J.
Bush, I. A.
Robinson, A. P. L.
Rajeev, P. P.
Mondal, S.
Lad, A. D.
Ahmed, S.
Narayanan, V.
Ravindra Kumar, D
Kingham, R. J.
Powiązania:
https://bibliotekanauki.pl/articles/147346.pdf
Data publikacji:
2015
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
shock waves
radiation hydrodynamics
laser–plasma interactions
fast ignition
inertial confinement fusion
Doppler spectroscopy
Opis:
When intense short-pulse laser beams (I > 1022 W/m2, τ < 20 ps) interact with high density plasmas, strong shock waves are launched. These shock waves may be generated by a range of processes, and the relative significance of the various mechanisms driving the formation of these shock waves is not well understood. It is challenging to obtain experimental data on shock waves near the focus of such intense laser–plasma interactions. The hydrodynamics of such interactions is, however, of great importance to fast ignition based inertial confinement fusion schemes as it places limits upon the time available for depositing energy in the compressed fuel, and thereby directly affects the laser requirements. In this manuscript we present the results of magnetohydrodynamic simulations showing the formation of shock waves under such conditions, driven by the j × B force and the thermal pressure gradient (where j is the current density and B the magnetic field strength). The time it takes for shock waves to form is evaluated over a wide range of material and current densities. It is shown that the formation of intense relativistic electron current driven shock waves and other related hydrodynamic phenomena may be expected over time scales of relevance to intense laser–plasma experiments and the fast ignition approach to inertial confi nement fusion. A newly emerging technique for studying such interactions is also discussed. This approach is based upon Doppler spectroscopy and offers promise for investigating early time shock wave hydrodynamics launched by intense laser pulses.
Źródło:
Nukleonika; 2015, 60, 2; 193-198
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Interactions between osmium atoms dissolved in iron observed by the 57Fe Mössbauer spectroscopy
Autorzy:
Konieczny, R.
Idczak, R.
Chojcan, J.
Powiązania:
https://bibliotekanauki.pl/articles/148144.pdf
Data publikacji:
2015
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
binding energy
enthalpy of solution
iron alloys
Mössbauer spectroscopy
Opis:
The room temperature 57Fe Mössbauer spectra for binary iron-based solid solutions Fe1−xOsx, with x in the range 0.01 ≤ x ≤ 0.05, were analyzed in terms of binding energy Eb between two Os atoms in the Fe-Os system. The extrapolated values of Eb for x = 0 were used for computation of enthalpy of solution of osmium in iron. The result was compared with that resulting from the cellular atomic model of alloys by Miedema. The comparison shows that our fi ndings are in qualitative agreement with the Miedema’s model predictions.
Źródło:
Nukleonika; 2015, 60, 1; 75-79
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Mean hyperfine fields at 57Fe in dilute iron-based alloys studied by Mössbauer spectroscopy
Autorzy:
Idczak, R.
Konieczny, R.
Chojcan, J.
Powiązania:
https://bibliotekanauki.pl/articles/147537.pdf
Data publikacji:
2015
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
hyperfine interactions
iron alloys
Mössbauer spectroscopy
Opis:
The room temperature Mössbauer spectra of 57Fe were measured for numerous dilute iron-based alloys Fe1-xDx (D = Al, Co, Cr, Mn, Mo, Ni, Os, Pt, Re, Ru, Ta, Ti, V, W, Zn), annealed at 1270 K for 2 h before the measurements. The spectra were analyzed using the Hesse–Rübartsch method in order to determine the mean hyperfi ne magnetic fi eld at the 57Fe nuclei as a function of concentration x of the minority component of the alloy. As the binary alloys are one-faze solid solutions of an element D in iron, a linear relationship between and x is observed. The result supports the suggestion that Mössbauer spectroscopy is a useful tool for the study of dissolution of different elements in iron.
Źródło:
Nukleonika; 2015, 60, 1; 39-42
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Thermodynamic properties of Au-Fe alloys studied with 57Fe Mössbauer spectroscopy
Autorzy:
Idczak, R.
Konieczny, R.
Chojcan, J.
Powiązania:
https://bibliotekanauki.pl/articles/147926.pdf
Data publikacji:
2013
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
Mössbauer spectroscopy
Au-Fe alloys
enthalpy of solution
short-range order
Opis:
The room temperature Mossbauer spectra of 57Fe were measured for Au1.xFex alloys with x in the range 0.01 less-than or equal to x less-than or equal to 0.03. The obtained data were analysed in terms of short range order parameter (SRO) and the binding energy Eb between two iron atoms in the studied materials using the extended Hrynkiewicz-Krolas idea. The estimated negative SRO parameters and the positive binding energy suggest ordering tendencies in Au-Fe alloys at low iron concentration. The extrapolated value of Eb for x = 0 was used for the computation of enthalpy of the solution of Fe in Au. The results were compared with the corresponding data derived from calorimetric measurements, previous Mossbauer experiments and resulting from the cellular atomic model of alloys by Miedema.
Źródło:
Nukleonika; 2013, 58, 1; 93-97
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Positron annihilation in precious and common opals
Autorzy:
Chojcan, J.
Sachanbiński, M.
Idczak, R.
Konieczny, R.
Powiązania:
https://bibliotekanauki.pl/articles/148010.pdf
Data publikacji:
2013
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
opal-A
porosity
positron annihilation
Opis:
The nano-porosity structure of several non-crystalline opal samples of different origin was investigated with positronium atoms. The obtained data show that the structure depends on both the kind of opal (precious, common or hyalite) as well as the place of its creation (sedimentary or volcanic rocks). The sizes of the pores "seen" by positronium atoms are relatively small, not greater than about 1 nm for all studied samples which may suggest that the pores are located inside the silica matter from which the samples are made. Moreover, the pores detected in the "sedimentary" precious opals are smaller and have less diverse sizes than those found in 'sedimentary" common opals and "volcanic' precious opals.
Źródło:
Nukleonika; 2013, 58, 1; 225-228
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
A Whole-Body Spectrometer (WBS) at the Institute of Nuclear Physics, Kraków : design and results for Polish citizens visiting Japan during the Fukushima accident
Autorzy:
Mietelski, J. W.
Janowski, P.
Kierepko, R.
Hajduk, R.
Bogacz, J.
Jurkowski, J.
Ochab, E.
Powiązania:
https://bibliotekanauki.pl/articles/146614.pdf
Data publikacji:
2013
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
whole-body spectrometry (WBS)
Fukushima
body burden
gamma spectrometry
doses
Opis:
The first Polish whole-body spectrometer (WBS) with scintillation detectors was constructed in Łódź in the early sixties of the last century and was operating there for more than 30 years. In 2008, the 19th century steel shield of this instrument was transported from Łódź to Kraków, where it was re-equipped with a modern gamma spectrometric system. Design and construction of this modernized spectrometer is presented along with the results for in-body contamination measurements of four Polish inhabitants who returned to Poland from Japan after the Fukushima accident compared with the results for typical Polish inhabitants, the volunteers from the Institute of Nuclear Physics (IFJ, Kraków) workers. Although, a clear signal from the Fukushima fallout was noticed for three of four persons who returned from Japan, the calculated doses were negligible. No traces of Fukushima-originating radionuclides were noticed for the examined people who have not traveled to Japan.
Źródło:
Nukleonika; 2013, 58, 4; 519-525
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Activity concentration of plutonium in atmospheric precipitation
Autorzy:
Kierepko, R.
Mietelski, J. W.
Powiązania:
https://bibliotekanauki.pl/articles/148396.pdf
Data publikacji:
2010
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
activity ratio 238Pu/239+240Pu
atmospheric precipitation
global fallout
Chernobyl
Opis:
Activity concentrations of plutonium isotopes (238Pu, 239+240Pu) were determined in atmospheric precipitation samples collected in Kraków from August 2005 to December 2007. The volume of 29 samples varied in the range 14–269 dm3. The method of samples collection, preparation and radiochemical analysis proper for the separation of plutonium are indicated in brief. Monthly plutonium deposition a showed seasonal variation for 239+240Pu the first maximum was observed in August 2005 and amounted to about 2.65±0.31 mBq/m2, the second one in July 2006 – 0.371±0.063 mBq/m2 and the third one in April 2007 – 0.859±0.075 mBq/m2 and for 238Pu in September 2005 – 0.090±0.038 mBq/m2, July 2006 – 0.177±0.074 mBq/m2 and the third maximum in May 2007 – 0.333±0.028 mBq/m2. Similar behaviour of activity concentration of plutonium was also observed in other parts of the earth. Anomalously high deposition of 239+240Pu (2.65±0.31 mBq/m2) was found in August 2005. The 238Pu/239+240Pu activity ratios higher than the global fallout value ~ 0.55 (in Poland) suggested participation from different sources of plutonium.
Źródło:
Nukleonika; 2010, 55, 2; 201-204
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Carbon-14 kinetic isotope effects in the debromination of p-nitrodibromocinnamic acid
Autorzy:
Bukowski, J.
Kanski, R.
Kanska, M.
Powiązania:
https://bibliotekanauki.pl/articles/147051.pdf
Data publikacji:
2002
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
bromine
carbon-14
elimination
kinetic isotope effect
mechanism
p-nitrodibromocinnamic acid
Opis:
The kinetic isotope effect (KIE) method was applied to study the mechanism of elimination of bromine from p-nitro-erythro-alfa,beta-dibromocinnamic acid labeled at the alfa-carbon. This compound was obtained starting from [2-14C]malonic acid via [2-14C]cinnamic acid and subsequent addition of bromide. The value of 14C KIE determined for alfa-position of side chain of p-nitro-erythro-alfa,beta-dibromocinamic acid proves that elimination of bromine leading to formation of (E)-p-nitrocinnamic acid proceeds via E2 mechanism.
Źródło:
Nukleonika; 2002, 47, 4; 133-136
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Electrode erosion mechanism in the rod plasma injector type of generator as deduced from the structure of irradiated substrates
Autorzy:
Piekoszewski, J.
Stanisławski, J.
Grotzschel, R.
Matz, W.
Jagielski, J.
Szymczyk, W.
Powiązania:
https://bibliotekanauki.pl/articles/147032.pdf
Data publikacji:
2002
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
plasma alloying
plasma melting
vapor ionization
Opis:
Titanium atoms were alloyed into a polycrystalline alundum substrate using a various number of intense pulses consisting of plasma of the working gas and vapor and low energy ions of Ti eroded from electrodes of the rod plasma injector type generator. It appears that at a single pulse titanium always forms a thin metallic film not mixed with the substrate material. With increasing number of pulses the amount of titanium atoms mixed into the substrate increases, whereas the thickness of the film - decreases. Analyses of phase composition and of structural properties, as well as computer simulations of thermal evolution brought the present authors to the conclusion that increase of number of pulses leads to decrease of melting temperature of the top layer of the substrate. It has also been confirmed that metallic ions eroded from electrodes do not undergo such acceleration like working gas ions do; their energy remains on the 200-300 eV level. It is concluded that erosion of the electrode material occurs during the last phase of the discharge via the vacuum arc mechanism.
Źródło:
Nukleonika; 2002, 47, 3; 113-117
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Stable isotope deuterium as a natural tracer of mixing processes in rivers
Autorzy:
Palige, J.
Ptaszek, S.
Zimnicki, R.
Chmielewski, A. G.
Wierzchnicki, R.
Powiązania:
https://bibliotekanauki.pl/articles/146756.pdf
Data publikacji:
2008
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
stable isotopes
tracer
deuterium
oxygen-18
river
water flow
Opis:
The possibility of application of naturally existing differences in isotope contents 18O/16O, 2H/1H in waters for investigation of transport and mixing of various waters in the tributary-river system is presented. Experiments carried out on the Bug-Narew rivers-Zegrze Lake and the BugoNarew-Vistula rivers systems have indicated that the hydrogen isotope ratio 2H/1H can be used as an intrinsic tracer of natural mixing processes occurring in rivers. The IRMS methodology was used for isotope ratio measurement of water samples. The degrees of water mixing as a function of distance from the confluence point of rivers were determined. The obtained results indicate that in water systems where the natural differences in ?2H are higher than 5‰ this technique can replace the time-consuming and expensive dye (or radiotracer) dispersion tests for evaluation of pollutant transport in rivers.
Źródło:
Nukleonika; 2008, 53, 2; 63-67
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Positron annihilation lifetime spectroscopy study of thermal processing and rehydration of dry leek (Allium porrum L.)
Autorzy:
Zaleski, R.
Wawryszczuk, J.
Sobczak, K.
Powiązania:
https://bibliotekanauki.pl/articles/146309.pdf
Data publikacji:
2010
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
positron annihilation
lifetime spectroscopy
food processing
rehydration
leek (Allium porrum L.)
Opis:
New application of positron annihilation lifetime spectroscopy (PALS) to development of food processing techniques is tested. Dehydrated leeks were an object of the study. Three experiments were performed consisting of evacuating air and volatile compounds from the sample, applying thermal treatment and rehydrating the sample. Distinct changes in positron lifetime spectra allowed the monitoring of alterations in the sample structure. The most likely origin of the particular components present in the spectra was able to be proposed from these data. Changes of the components were ascribed to the various processes occurring in the samples.
Źródło:
Nukleonika; 2010, 55, 1; 73-78
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Conceptual design of Light Impurity Monitor for Wendelstein 7-X
Autorzy:
Książek, I.
Burhenn, R.
Musielok, J.
Powiązania:
https://bibliotekanauki.pl/articles/146640.pdf
Data publikacji:
2011
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
plasma spectroscopy
stellarator
soft X-ray
Opis:
As plasma impurity ions can significantly influence the properties of a fusion plasma by dilution and enhancement of the radiation losses, the process of monitoring of their concentrations is one of the most important tasks. A Light Impurity Monitor is needed for monitoring the contamination of the stellarator plasma by carbon, nitrogen, boron, and oxygen impurities, which are indicators for the overload of the plasma facing components, leakage of the vacuum vessel, or wall condition, respectively. Their concentration will be estimated on the basis of emission intensities of their hydrogen-like ions. In this paper a conceptual design of such a spectrometer is presented, including the description of the geometry, the acquisition system and safety systems.
Źródło:
Nukleonika; 2011, 56, 2; 155-160
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Development of a radiolabeled glucagon compound for imaging
Autorzy:
Jalilian, A. R.
Jouiaei, M.
Doroudi, A. R.
Bolourinovin, F.
Garousi, J.
Powiązania:
https://bibliotekanauki.pl/articles/148402.pdf
Data publikacji:
2010
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
glucagons
radiolabeling
biodistribution
Ga-67
Opis:
In order to develop a possible Ga-labeled glucagon (GCG) compound for imaging studies, biosynthetic glucagon (GCG) was labeled with [67Ga]-gallium chloride after conjugation with freshly prepared diethylenetriaminepentaacetic acid dianhydride (ccDTPA). After solid phase purification of the radiolabeled hormone, high performance liquid chromatography (HPLC) and instant thin-layer chromatography (ITLC) showed a radiochemical purity around 95 per cent in optimized conditions (specific activity = 296–370 GBq/mM; labeling efficiency 85 per cent). Preliminary in vivo studies (IDźg–1 per cent) in male wild-type rats showed heart:muscle, liver:muscle, lung:muscle and stomach:muscle ratios to be 5.53, 2.9, 7.56, 3.69, 3.2 (in 5 min), respectively while after 2 h liver:blood, lung:blood and spleen:blood ratios were 14.21, 16.86 and 7.8, respectively. The data suggests 5 min post injection, the tracer is accumulated in GCGR rich tissues which is in agreement with biodistribution studies and reported GCG receptors (GCGRs). The results of the present study can possibly offer a candidate for non-invasive imaging of glucagon receptor related diseased and malignancies such as glucagonoma.
Źródło:
Nukleonika; 2010, 55, 2; 219-224
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 84

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