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Wyświetlanie 1-15 z 120
Tytuł:
Performance evaluation of a rectifi er column using gamma column scanning
Autorzy:
Aquino, D. D.
Mallillin, J. P.
Sulit, R. F.
Hila, F. C.
Nuñez, I. A. A.
Bulos, A. D. M.
Powiązania:
https://bibliotekanauki.pl/articles/146268.pdf
Data publikacji:
2017
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
gamma column scanning
distillation column
density profile
processing plant
refinery
Opis:
Rectifier columns are considered to be a critical component in petroleum refineries and petrochemical processing installations as they are able to affect the overall performance of these facilities. It is deemed necessary to monitor the operational conditions of such vessels to optimize processes and prevent anomalies which could pose undesired consequences on product quality that might lead to huge financial losses. A rectifier column was subjected to gamma scanning using a 10-mCi Co-60 source and a 2-inch-long detector in tandem. Several scans were performed to gather information on the operating conditions of the column under different sets of operating parameters. The scan profiles revealed unexpected decreases in the radiation intensity at vapour levels between trays 2 and 3, and between trays 4 and 5. Flooding also occurred during several scans which could be attributed to parametric settings.
Źródło:
Nukleonika; 2017, 62, 4; 285-287
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Monte Carlo simulation of the positron implantation profiles in the layered samples
Autorzy:
Dryzek, J.
Horodek, P.
Powiązania:
https://bibliotekanauki.pl/articles/146332.pdf
Data publikacji:
2010
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
positron implantation
implantation profile
GEANT4 tool kit
Opis:
Theoretical studies of the positron implantation profiles in the layered samples are presented. Simulations performed using a GEANT4 tool kit revealed accumulation of positrons in denser layer embedded by less dens environment. This effect is significant for implantation profiles of slow positrons formed in a beam. Nevertheless, it is also present in conventional experiments, where positrons are emitted from radioactive nuclei. In some cases the diffusion process, which follows the implantation and thermalization processes, can smear this effect. However, defects on the interfaces or differences in the positron affinity can sustain it.
Źródło:
Nukleonika; 2010, 55, 1; 13-16
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
GEANT4 simulation of implantation profiles for positrons injected in solids from radioactive sources 22Na and 68Ge/68Ga
Autorzy:
Horodek, P.
Dryzek, J.
Powiązania:
https://bibliotekanauki.pl/articles/146334.pdf
Data publikacji:
2010
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
positron annihilation
implantation profile
absorption coefficient
GEANT4 tool kit
Opis:
We calculated theoretically the mass absorption coefficients for positrons emitted from the commonly used sources 22Na and 68Ge/68Ga in numerous materials. For this purpose, we used the tool kit GEANT4 which allows to generate the implantation profile. An excellent agreement between the experimental profile and the calculated one was achieved. The calculated values of the mass absorption coefficients coincide well with the experimental values determined by the DSIP method.
Źródło:
Nukleonika; 2010, 55, 1; 17-19
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Local electronic and charge state of iron in FeTe2
Autorzy:
Stanek, J.
Fornal, P.
Powiązania:
https://bibliotekanauki.pl/articles/147241.pdf
Data publikacji:
2004
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
Mössbauer
chemical bonding
charge state
tellurides
Opis:
From 57Fe Mössbauer spectrum of FeTe2 taken in high external magnetic field (B = 4.6 T), the sign of electric field gradient was determined as negative, with an asymmetry parameter of 0.2. A comparison of these data with results of calculation of the electric field gradient within point charge model suggests the lattice character of electric field gradient with some contribution from covalency effects. The effective magnetic field acting on 57Fe is less than the applied, which points out the diamagnetic Fe+2 state of iron. This "electronic state" is in a contradiction to Fe+3 "charge state" concluded from 125Te experiments on 3d transition metal ditellurides as well as from 57Fe quadrupole splitting and isomer shift.
Źródło:
Nukleonika; 2004, 49,suppl.3; 63-65
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Phase constitution of an LaFe11.0Co0.8(Si0.4Al0.6)1.2 alloy investigated by Mössbauer spectroscopy
Autorzy:
Gębara, P.
Pawlik, P.
Wysłocki, J. J.
Szwaja, M.
Powiązania:
https://bibliotekanauki.pl/articles/147912.pdf
Data publikacji:
2013
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
magnetocaloric materials
Mössbauer spectroscopy
Opis:
In the present work the phase constitution and magnetic ordering of the magnetocaloric LaFe11.0Co0.8(Si0.4Al0.6)1.2 alloy in the as-cast state and after annealing at 1323 K for 1 h (in case of ribbons) and 49 days (in case of bulk) were studied. For bulk and ribbon samples in as-cast state three crystalline phases were identified: dominant ferromagnetic alfa-Fe, minor ferromagnetic La(Fe,Co)Si and traces of paramagnetic La(Fe,Si)13 phase. Appropriate heat treatment resulted in the evolution of phase constitution of the alloy, where two crystalline phases were developed: the dominant paramagnetic La(Fe,Si)13 phase and a minor fraction of the ferromagnetic alfa-Fe for both bulk and ribbon samples.
Źródło:
Nukleonika; 2013, 58, 1; 113-116
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Simultaneous transmission and scattering Mössbauer measurements of powder samples
Autorzy:
Fornal, P.
Stanek, J.
Powiązania:
https://bibliotekanauki.pl/articles/148213.pdf
Data publikacji:
2007
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
methodology of Mössbauer spectroscopy
CEMS
micro-powders
Opis:
A vertical experimental set-up for simultaneous recording transmission and scattering Mössbauer spectra is described. Application of the apparatus for the study of model powder mixture of two components with different grain sizes shows differences in the relative intensity ratio of these fractions in absorption and conversion electron Mössbauer spectroscopy (CEMS) spectra. This effect, explained as a result of the size selectivity of CEMS technique, is parameterized by the grain radius ratio of components. The possible application for investigation of isolated surface nano- and microobjects is discussed.
Źródło:
Nukleonika; 2007, 52, supl. 1; 13-16
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
In situ measurement of diffusivity
Autorzy:
Berne, P.
Pocachard, J.
Powiązania:
https://bibliotekanauki.pl/articles/148818.pdf
Data publikacji:
2005
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
diffusion
porous media
in situ measurement
Opis:
The mechanism of molecular diffusion controls the migration of contaminants in very low-permeability porous media, like underground facilities for the storage of hazardous waste. Determining the relevant diffusion coefficients is, therefore, of prime importance. A few techniques exist for the in situ measurement of that quantity, but they suffer from many handicaps (duration, complexity and cost of the experiments). We propose here two innovative methods that have some potential to improve this situation. So far, we have found them feasible on the basis of design calculations and laboratory experiments. This work is presently protected by a patent.
Źródło:
Nukleonika; 2005, 50, 1; 3-7
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Sedimentation of Fe2O3 and metallic iron nanoparticles exhibiting Brownian movement
Autorzy:
Fornal, P.
Stanek, J.
Powiązania:
https://bibliotekanauki.pl/articles/147364.pdf
Data publikacji:
2013
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
Brownian movement
nanoparticles
sedimentation
Opis:
Sedimentation of nanoparticles in water solutions was studied in situ by transmission Mössbauer spectroscopy in horizontal and vertical geometry. The studied specimens were Fe2O3 of a commercial pigment and metallic iron nanoparticles in slurry used in a water purification technology. The sedimentation is selective and leads to the gradual removing of the bigger particles from a solution. The iron nanoparticles in the solution are relatively chemically stable until, due to the drying, the sediment becomes exposed to the air.
Źródło:
Nukleonika; 2013, 58, 1; 39-42
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Hyperfine interactions in x-Bi0.95Dy0.05FeO3-(1-x)-Pb(Fe2/3W1/3)O3 multiferroics
Autorzy:
Zachariasz, P.
Stoch, A.
Stoch, P.
Maurin, J.
Powiązania:
https://bibliotekanauki.pl/articles/147354.pdf
Data publikacji:
2013
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
multiferroics
multifunctional materials
Néel temperature
Opis:
The complex perovskite system xźBi0.95Dy0.05FeO3-(1 - x)źPb(Fe2/3W1/3)O3 was synthesized by the solid-state reaction method and was studied by means of Mössbauer spectroscopy. For different Dy-doped bismuth ferrite (BDF) contents (x = 0.1, 0.3, 0.5, 0.7) the formation of single-phase sinters was confirmed using an X-ray diffraction technique. The random distributions of Fe/W cations in crystallographic structures have been proved. A monotonically, saturation- like increase of Néel temperatures with growing BDF contribution was confirmed, and a straightforward dependence between TN temperatures and the mean hyperfine magnetic fields at Fe nuclei was shown.
Źródło:
Nukleonika; 2013, 58, 1; 53-56
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Gamma-Ray Spectrometry Laboratory for high-precision measurements of radionuclide concentrations in environmental samples
Autorzy:
Jodłowski, P.
Kalita, S. J.
Powiązania:
https://bibliotekanauki.pl/articles/148485.pdf
Data publikacji:
2010
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
gamma-ray spectrometry
environmental samples
efficiency
self-absorption
coincidence summing
Opis:
The paper outlines the methodology used in the Gamma-Ray Spectrometry Laboratory for high-precision measurements of radionuclide activity concentrations in environmental samples. The Laboratory equipment includes a semiconductor detector HPGe with a 42% relative efficiency. The detector is placed in a Pb housing made of bricks 10 cm in thickness. Three measurement geometries are considered: Marinelli beakers 710 cm3 in volume and two cylindrical geometries 121 and 48 cm3 in volume. In the efficiency calibration (E = 32 division sign 1836 keV) mixed gamma standard solutions were used. Obtained experimental efficiency values epsilon were fitted with two quadratic functions. The junction point is that equivalent to 200 keV. Uncertainty of the calibration curve is 2% for E > 200 keV. The relationship between the total efficiency and the energy epsilon t(E) was also found for energies E = 33 division sign 1250 keV. Self-absorption correction factors Cs are calculated by the method proposed by K. Debertin, the uncertainty level being 1 division sign 2% for E > 100 keV. These correction factors are calculated by an original computer program. Coincidence summing correction factors Cc for the selected nuclides are derived using the ETNA computer program, basing on the relationships epsilon(E) and epsilon t(E). Minimum detectable activity (MDA) for selected nuclides encountered in environmental samples was determined for the water matrix. The methodology used was successfully verified in the course of international intercomparison measurements.
Źródło:
Nukleonika; 2010, 55, 2; 143-148
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Hyperfine interactions in Tb0.27-xYxDy0.73Fe2 compounds at 295 K
Autorzy:
Krawczyk, A.
Zwoźniak, A.
Guzdek, P.
Stoch, P.
Zachariasz, P.
Suwalski, J.
Pszczoła, J.
Powiązania:
https://bibliotekanauki.pl/articles/147818.pdf
Data publikacji:
2013
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
hyperfine interaction
intermetallics
Laves phase
Mössbauer effect
Opis:
This paper concerns the synthesis of yttrium-dilute Tb0.27-xYxDy0.73Fe2 intermetallic series with a borderline compound Tb0.27Dy0.73Fe2 known as Terfenol-D by arc melting, XRD analysis and 57Fe Mössbauer effect studies at 295 K. XRD analysis (295 K) shows that all samples crystallize in a cubic, Fd3m, MgCu2-type structure. The lattice parameter increases along with yttrium content. Mössbauer effect spectra for the Tb0.27-xYxDy0.73Fe2 series collected at 295 K consist of two subspectra due to easy direction of magnetization <111>. Hyperfine interaction parameters: isomer shift, magnetic hyperfine field and a quadrupole splitting were obtained from the fitting procedure of the spectra.
Źródło:
Nukleonika; 2013, 58, 1; 133-135
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Hyperfine interactions in Dy(Co0.4-xNixFe0.6)2 compounds at 295 K
Autorzy:
Zwoźniak, A.
Krawczyk, A.
Stoch, P.
Guzdek, P.
Zachariasz, P.
Suwalski, J.
Pszczoła, J.
Powiązania:
https://bibliotekanauki.pl/articles/148005.pdf
Data publikacji:
2013
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
hyperfine interaction
intermetallics
Mössbauer effect
Slater-Pauling dependence
Opis:
57Fe Mössbauer effect studies were performed for the cubic C15, Fd3m, MgCu2-type Dy(Co0.4-xNixFe0.6)2 intermetallics. Hyperfine interaction parameters : isomer shift, magnetic hyperfine field and quadrupole interaction parameter were obtained from the fitting procedure of the collected 57Fe Mössbauer effect spectra. As a result of Co/Ni substitution, a Slater-Pauling type curve for the average magnetic hyperfine field vs. Ni content in the Dy(Co0.4-xNixFe0.6)2 series is observed.
Źródło:
Nukleonika; 2013, 58, 1; 179-181
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Mössbauer effect studies of Dy(Fe0.4-xNixCo0.6)2
Autorzy:
Jabłońska, A.
Suwalski, J.
Stoch, P.
Pszczoła, J.
Guzdek, P.
Szamański, P.
Pańta, A.
Powiązania:
https://bibliotekanauki.pl/articles/148209.pdf
Data publikacji:
2007
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
crystal structure
Mössbauer effect
hyperfine interaction
Slater-Pauling curve
band structure
Opis:
A consequence of the Fe/Ni substitution in the Dy(Fe0.4Co0.6)2 compound was studied in the present paper. For this purpose the synthesis and X-ray analysis (295 K) of the Dy(Fe0.4 xNixCo0.6)2 series were performed. The cubic, MgCu2-type, Fd3m crystal structure was observed across the series. 57Fe Mössbauer effect spectra for the series were collected at 77 K. The obtained crystallographic data and the hyperfine interaction parameters are presented. The magnetic hyperfine fields form a separate branch of the Slater-Pauling curve known for the Dy(Mn1 xFex)2 and Dy(Fe1 xCox)2 series. The data are qualitatively related to the Stoner model.
Źródło:
Nukleonika; 2007, 52, supl. 1; 55-58
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Assessment of the control rods shadow effect in the VENUS-F core
Autorzy:
Cetnar, J.
Domańska, G.
Gajda, P.
Janczyszyn, J.
Powiązania:
https://bibliotekanauki.pl/articles/147908.pdf
Data publikacji:
2014
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
accelerator driven systems (ADS)
control rod
FREYA
GUINEVERE
reactivity
Opis:
The partitioning and transmutation (P&T) of spent nuclear fuel is an important fi eld of present development of nuclear energy technologies. One of the possible ways to carry out the P&T process is to use the accelerator driven systems (ADS). This technology has been developed within the EURATOM Framework Programmes for several years now. Current research in this fi eld is carried out within the scope of 7th FP project FREYA. Important parts of the project are experiments performed in the GUINEVERE facility devoted to characterising the subcritical core kinetics and development of reactivity monitoring techniques. The present paper considers the effects of control rods use on the core reactivity. In order to carry out the evaluation of the experimental results, it is important to have detailed core characteristics at hand and to take into consideration the differences in the effect of control rods acting separately or together (the so-called shadow effect) on both the reactivity value and the measured neutron fl ux. Also any core asymmetry should be revealed. This goal was achieved by both MCNP simulations and the experimental results. However, in the case of experimental results, the need for calculating respective correction factors was unavoidable.
Źródło:
Nukleonika; 2014, 59, 4; 137-143
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Properties of TiN protective coatings on steel
Autorzy:
Fornal, P.
Stanek, J.
Jaglarz, J.
Dąbrowski, M.
Powiązania:
https://bibliotekanauki.pl/articles/148888.pdf
Data publikacji:
2003
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
Conversion Electron Mössbauer Spectroscopy
hard coating
oxidation
TiN
Opis:
The properties of fast cutting steel SW7M, stainless steel 1H18N9T, and tool steel NC11 coated with a TiN protective layer were studied using 57Fe Conversion Electron Mössbauer Spectroscopy. The adhesion of the coatings is determined by the thickness of Fe-N and Fe-Ti interface. The model of the abrasion of the protected tools, based on fast diffusion of Fe ions to the surface though the TiN layer and further oxidation is proposed.
Źródło:
Nukleonika; 2003, 48,suppl.1; 21-24
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 120

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