Temat: transmission electron microscopy X ray diffraction - Katalog OPAC zbiorów

Skocz do pozycji: 1.

Tytuł:: Ultrasonic-assisted synthesis of reactive carboxymethyl cellulose stabilized nano zero-valent iron and its application for removal of Cr6+ and Cu2+ ions
Autorzy:: Ayob, A.
Santiagoo, R.
Amneera, W. A.
Ismail, N.
Abdullah, A. Z.
Powiązania:: https://bibliotekanauki.pl/articles/207403.pdf
Data publikacji:: 2016
Wydawca:: Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:: high resolution transmission
electron microscopy
light scattering
transmission electron microscopy X ray diffraction
zero-valent iron
wysoka rozdzielczość transmisyjna
mikroskopia elektronowa
dyfrakcja rentgenowska
żelazo
Opis:: Carboxymethyl cellulose (CMC) was used in the chemical reduction using sodium borohydride to yield dispersive nano zero-valent iron (nZVI) particles as reactive and stable adsorbents. CMC- -stabilized nZVI particles were characterized via UV-visible light spectroscopy, X-ray diffraction, dynamic light scattering, transmission electron microscopy, and specific surface area assisted using a probe ultrasonication dispersing tool at 50% amplitude power. High catalytic reactivity obtained in pseudo-first order reaction for Cr⁶⁺ (rate constant K1 = 0.0311 min^–1) and pseudo-second order for Cu²⁺ (rate constant K2 = 0.0946 g·mg^–1·min^–1) indicated that colloidal stability of nZVI particles can be achieved with a stabilizer for the removal of toxic contaminants.
Źródło:: Environment Protection Engineering; 2016, 42, 2; 55-79
0324-8828
Pojawia się w:: Environment Protection Engineering
Dostawca treści:: Biblioteka Nauki

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Skocz do pozycji: 2.

Tytuł:: Catalytic decomposition of toluene over La1-xSr xMnO3/palygorskite synthesized catalysts
Autorzy:: Song, L.
Chen, T.
Chen, D.
Chen, Y.
Xie, J.
Liu, H.
Powiązania:: https://bibliotekanauki.pl/articles/207996.pdf
Data publikacji:: 2013
Wydawca:: Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:: catalysts
manganese
manganese oxide
toluene
transmission electron microscopy
X ray diffraction
Palygorskite
katalizatory
mangan
tlenek manganu
toluen
transmisyjna mikroskopia elektronowa
dyfrakcja promieniowania rentgenowskiego
Opis:: Palygorskite (PG) supported La1-xSrxMnO3 catalysts were fabricated by copreripitation. The catalysts were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), specific surface area (SSA) and H2 temperature programmed reduction (H 2-TPR). Catalytic activity for VOCs was examined by using toluene as a model compound. The results show that the surface area as well as mechanical strength of catalysts increase substantially after catalysts loaded in PG. XRD patterns show that after calcination at 700 0C, PG as a support in 9% LaMn03/PG and 9% La0.7Sr0.3MnO3/PG was transformed into amorphous phase and the morphology was not destroyed. It was well established that the main reductive components are factually Mn(III) or Mn(IV) oxides in catalysts based on the results of TPR. It was also found that Mn(IV) increases while Mn(III) reduces responding with the increasing amount of Sr. Toluene conversion rate of as-preparedμ% La1-xSr xMnO3/PG increases with the increasing values of x and μ when x=0-0.3 and μ = 3-9%. Toluene can be converted completely at 285 0C by 9% La0.7Sr0.3MnO3/PG catalyst while no significant change was observed after addition on the doping and loading amount of Sr. During a 100 h stability experiment of 9% La 0.7Sr0.3MnO3/PG catalyst, toluene removal was found to be above 95%.
Źródło:: Environment Protection Engineering; 2013, 39, 3; 31-42
0324-8828
Pojawia się w:: Environment Protection Engineering
Dostawca treści:: Biblioteka Nauki

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