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    Wyświetlanie 1-11 z 11
    Tytuł:
    Synthesis, Structure and Energetic Properties of a Catenated N6, Polynitro Compound: 1,1’-Azobis(3,5-dinitropyrazole)
    Autorzy:
    Li, Y.-N.
    Shu, Y.-J.
    Wang, Y.-L.
    Wang, B.-Z.
    Zhang, S.-Y.
    Bi, F.-Q.
    Powiązania:
    https://bibliotekanauki.pl/articles/358573.pdf
    Data publikacji:
    2017
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    energetic compound
    1,1’-azobis(3,5-dinitropyrazole)
    synthesis
    energetic properties
    Opis:
    A nitrogen-rich, polynitro energetic compound with an N,N-azo linkage, 1,1’-azobis(3,5-dinitropyrazole) (ABDNP), has been synthesized by an oxidative coupling reaction of 1-amino-3,5-dinitropyrazole with different oxidizing agents. The target compound was characterized by IR spectroscopy, 1H and 13C nuclear magnetic resonance spectroscopy, elemental analysis, mass spectra, X-ray diffraction and differential scanning calorimetry (DSC). The DSC results show that 1,1’-azobis(3,5-dinitropyrazole) decomposes at a relatively high onset temperature (202.9 °C), which indicates that 1,1’-azobis(3,5-dinitropyrazole) has acceptable thermal stability. The energetic properties were obtained, with a measured density and heat of formation matched by theoretically computed values based on the B3LYP method.
    Źródło:
    Central European Journal of Energetic Materials; 2017, 14, 2; 321-335
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Review of the Photodecomposition of Some Important Energetic Materials
    Autorzy:
    Sun, Y.
    Shu, Y.
    Xu, T.
    Shui, M.
    Zhao, Z.
    Gu, Y.
    Wang, X.
    Powiązania:
    https://bibliotekanauki.pl/articles/358397.pdf
    Data publikacji:
    2012
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    photodecomposition mechanisms
    energetic materials
    Opis:
    The photodecomposition mechanisms of energetic materials vary with molecular structure, photodissociation wavelength, the phase of the material, experimental pressure and temperature etc. In this paper, the significant progress on photodecomposition studies of some important energetic materials achieved in recent years is introduced in detail, including nitromethane, DMNA (dimethylnitramine), TATB (1,3,5-triamino-2,4,6-trinitrobenzene), RDX (hexahydro-1,3,5-trinitro-1,3,5-triazine), HMX (1,3,5,7-tetranitro-1,3,5,7- tetrazacycloctane) and CL-20 (2,4,6,8,10,12-hexanitrohexaazaisowurtzitane). The difficulties and prospects of photodecomposition research of energetic materials are also indicated.
    Źródło:
    Central European Journal of Energetic Materials; 2012, 9, 4; 411-423
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Synthesis and Property of 1,4-Diamino-3,6- dinitropyrazolo[4,3-c]pyrazole and Its Derivatives
    Autorzy:
    Li, Y.-N.
    Wang, B.-Z.
    Shu, Y.-J.
    Zhang, S.-Y.
    Lian, P.
    Powiązania:
    https://bibliotekanauki.pl/articles/358674.pdf
    Data publikacji:
    2016
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    3,6-dinitropyrazolo[4,3-c]pyrazole (DNPP)
    1,4-diamino-3,6- dinitropyrazolo[4,3-c]pyrazole (DADNP)
    4,4’-(triaz-1-ene-1,3-diyl)bis(1- amine-3,6-dinitropyrazolo[4,3-c]pyrazole) (TBADNP)
    N-amination reaction
    synthesis
    property
    Opis:
    A synthetic procedure has been developed for the synthesis of 1,4-diamino- 3,6-dinitropyrazolo[4,3-c]pyrazole (DADNP) via N-amination reaction. Its derivatives, 4,4’-(triaz-1-ene-1,3-diyl)bis(1-amine-3,6-dinitropyrazolo[4,3-c] pyrazole) (TBADNP) and 1,4-dinitramino-3,6-dinitropyrazolo[4,3-c]pyrazole (DNADNP), were first designed and synthesized by the diazotization and nitrification of amino group, and their structures were characterized by IR, 1H NMR, 13C NMR, elementary analysis and MS. The thermal properties of target compounds were studied by means of differential scanning calorimetry (DSC) and thermogravimetry (TG). The thermal decomposition peak temperatures of DADNP, TBADNP and DNADNP are 227, 236 and 288 °C, respectively. Results show that the derivatives of 1,4-diamino-3,6-dinitropyrazolo[4,3-c]pyrazole have better thermal stability.
    Źródło:
    Central European Journal of Energetic Materials; 2016, 13, 2; 321-331
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Computational Investigation on the Structure and Performance of Novel 4,7-dinitro-furazano-[3,4-d]-pyridazine Derivatives
    Autorzy:
    Wang, K.
    Shu, Y.
    Liu, N.
    Ding, X.
    Wu, Z.
    Lu, Y.
    Powiązania:
    https://bibliotekanauki.pl/articles/358090.pdf
    Data publikacji:
    2017
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    4,7-dinitro-furazano-[3,4-d]-pyridazine
    heat of formation
    density
    detonation performance
    bond dissociation energy
    Opis:
    Seven novel energetic 4,7-dinitro-furazano-[3,4-d]-pyridazine derivatives were designed, and their optimized structures and performances were studied by density functional theory (DFT) at B3LYP/6-311g(d,p) level. The detonation performances were estimated by the Kamlet-Jacobs equations. The results show that these compounds have high crystal densities (1.818-1.925 g·cm−3), detonation velocities (8.51-9.56 km·s−1) and detonation pressures (32.28-41.70 GPa). The bond dissociation energies (BDEs) of the weakest bond (N–O bond) vary from 70.889 kJ·mol−1 to 173.283 kJ·mol−1, and some of them exhibit higher BDEs than that of RDX (N–NO2 bond, 149.654 kJ·mol−1) and HMX (N–NO2 bond, 154.905 kJ·mol−1). M4 and M5 exhibit similar and higher detonation performance than RDX (8.81 km·s−1, 34.47 GPa). The detonation performance of M7 (9.56 km·s−1, 41.70 GPa) even surpasses that of HMX (9.10 km·s−1, 39.00 GPa). Otherwise, the specific impulse values of M1-M7 (266-279 s) outperform HMX (266 s) by 0-13 s, which indicates that M1-M7 may show better performance as monopropellants. It is concluded that density, heat of formation, stability, detonation performance and specific impulse of the designed compounds depend on the position and number of the N→O oxidation bonds.
    Źródło:
    Central European Journal of Energetic Materials; 2017, 14, 1; 26-46
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    System and Method for Simultaneous Measurement of Nitrogen Content and Uniformity of Nitration of Nitrocellulose
    Autorzy:
    Liu, Y.
    Shao, Z.
    Wang, W.
    Li, W.
    Lv, Y.
    Sun, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/358714.pdf
    Data publikacji:
    2018
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    nitrocellulose
    uniformity of nitration
    nitrogen content
    mixed acid nitration
    cotton maturity
    Opis:
    Nitrocellulose (NC) is a common, commercially available, cellulosederived material and has been functionalized and widely applied in microfluidic technology, immunoassays and biochemical analyses. However, existing testing parameters always fail to completely and accurately reflect its inherent quality. In this study, we have designed and assembled a novel automatic polarizing microscope test system (PMTS) to scientifically test the nitrogen content and uniformity of nitration of NC based on the chromogenic principle of a polarization microscope. The advantages of this system are: (i) the PMTS requires less sample (only a few micrograms); (ii) the test period is shorter and the results can be obtained within 20 min; (iii) the method belongs to the nondestructive testing group, and the NC sample is not burned, dissolved, or damaged; and (iv) this method has increased accuracy, and the deviation of the nitrogen content is less than ±0.05%. The properties of various NC samples prepared by different nitricsulfuric acid systems from raw materials with diverse maturities were determined via PMTS. Five NC samples with different nitrogen contents (10.9%, 11.5%, 11.8%, 12.6% and 13.5%) were tested, and the variance of the corresponding uniformity of nitration of these samples were 3.17, 1.61, 1.15, 1.76, and 2.83. The uniformity of nitration initially decreased and then increased with increasing nitrogen content, and the best uniformity of nitration appeared at a nitrogen content of 12%. We also found that fibre maturity has a positive effect on the uniformity of nitration. This testing device and method, with its cost-effectiveness and field-portability, can significantly improve the accuracy of nitration content and uniformity, and has an important value in practical applications.
    Źródło:
    Central European Journal of Energetic Materials; 2018, 15, 4; 554-571
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    The Effect of the Energetic Additive Coated MgH2 on the Power of Emulsion Explosives Sensitized by Glass Microballoons
    Autorzy:
    Cheng, Y.
    Wang, Q.
    Liu, F.
    Ma, H.
    Shen, Z.
    Guo, Z.
    Liu, R.
    Powiązania:
    https://bibliotekanauki.pl/articles/357940.pdf
    Data publikacji:
    2016
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    emulsion explosive
    power
    hydrogen storage material
    magnesium hydride
    Opis:
    Traditional emulsion explosives, in spite of excellent water resistance, safe handling and good storage performance, have low power problems which seriously hinders their use. In order to improve the power of emulsion explosives, a hydrogen based emulsion explosive was devised. Scanning electron microscope pictures and experimental storage results show that the coating effect and stability of coated magnesium hydride (MgH2) are very good. The power of an emulsion explosive sensitized by glass microballoons was significantly increased (24.30 mm compression of lead block) after adding coated MgH2, compared to only 16.10 mm compression when not added. Thus emulsion explosives with coated MgH2 as an energetic additive have many potential applications.
    Źródło:
    Central European Journal of Energetic Materials; 2016, 13, 3; 705-713
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Thermally Induced Polymorphic Transformation of Hexanitrohexaazaisowurtzitane (HNIW) Investigated by in-situ X-ray Powder Diffraction
    Autorzy:
    Liu, Y.
    Li, S.
    Wang, Z.
    Xu, J.
    Sun, J.
    Huang, H.
    Powiązania:
    https://bibliotekanauki.pl/articles/358065.pdf
    Data publikacji:
    2016
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    HNIW
    polymorphism
    in situ X-ray diffraction
    phase transition
    heat stimulation
    Opis:
    The ε→γ phase transition of HNIW induced by heat was investigated with in situ X-ray powder diffraction (PXRD). The effects of purity, particle size, insensitive additives and the time of isothermal heat treatment on the phase transition were evaluated. It was found that the phase transition is irreversible with changes in temperature, and the two phases can coexist in a certain temperature range. Moreover, the initial phase transition temperature increases with increasing purity and decreasing particle size of HNIW, and thus with the approximate crystal density. The addition of graphite and paraffin wax to HNIW as insensitive additives leads to a decrease in the initial phase transition temperature, but the addition of TATB does not affect the initial phase transition temperature. Thus, TATB is a suitable insensitive additive. Moreover, at the critical temperature, the isothermal time determined the efficiency of the ε- to γ-phase transition. This work lays the foundations for the choice of molding technologies, performance test methods, ammunition storage options, as well as the manufacture of HNIW-based explosive formulations.
    Źródło:
    Central European Journal of Energetic Materials; 2016, 13, 4; 1023-1037
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Influence of Processing Techniques on Mechanical Properties and Impact Initiation of an Al-PTFE Reactive Material
    Autorzy:
    Feng, B.
    Fang, X.
    Li, Y.-C.
    Wu, S.-Z.
    Mao, Y.-M.
    Wang, H.-X.
    Powiązania:
    https://bibliotekanauki.pl/articles/358654.pdf
    Data publikacji:
    2016
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    Al-PTFE
    reactive materials
    quasi-static compression
    impact initiation
    Opis:
    Reactive materials (RMs) or impact-initiated materials have received much attention as a class of energetic materials in recent years. To assess the influence of processing techniques on mechanical properties and impact initiation behaviors of an Al-PTFE reactive material, quasi -static compression tests and drop-weight tests were performed. Scanning electron microscopy (SEM) was used to identify the characteristics of the interior microstructures of the Al-PTFE samples. A sintering process was found to transform Al-PTFE from a brittle to a ductile material with an increased elasticity modulus (from 108-160 MPa to 256-336 MPa) and yield stress (from 12-16 MPa to 19-20 MPa). Increasing the molding pressure from 36 MPa to 182 MPa increased the elastic modulus of all Al-PTFE samples and also the yield stress of unsintered ones. Unsintered samples in general required less energy to initiate than sintered ones. As the molding pressure increased, the impact initiation energy for sintered Al-PTFE fell from 96 J to 68 J, whereas the initiation energy for unsintered Al-PTFE rose from 68 J to 85 J. PTFE nanofiber networks observed in sintered samples formed under the higher molding pressures could contribute to the opposite trends observed in the impact initiation energy of unsintered and sintered Al-PTFE samples.
    Źródło:
    Central European Journal of Energetic Materials; 2016, 13, 4; 989-1004
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Research on the Mechanism and Kinetics of Polymorphic Transitions of ε CL-20 in Composite Systems
    Autorzy:
    Guo, X.-Y.
    Zhang, P.
    Xu, J.-J.
    Wang, Z.-H.
    Jiao, Q.-J.
    Powiązania:
    https://bibliotekanauki.pl/articles/358032.pdf
    Data publikacji:
    2015
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    polymorphic transition
    kinetics
    activation energy
    transition temperature
    Opis:
    In order to explore the polymorphic transition law for ε-CL-20 in composite systems, the polymorphic transition process of pure ε-CL-20 crystals stimulated by heat was investigated by the X-ray Diffraction (XRD) method, and the kinetic parameters of the polymorphic transition process were calculated (including the apparent activation energy Ea and the pre-exponential factor lnA). Meanwhile the effects of different additives on the polymorphic transition process and kinetics of ε-CL-20 were explored in detail. The experimental results showed that the ε-form tends to transform into the γ- form on heating and that the Ea and lnA for the transition process were 209.97 kJ/mol and 57.47, respectively. The first group of additives clearly promoted the polymorphic transition of ε-CL-20 and lowered the initial transition temperature and the activation energy. The second and third groups of additives inhibited the polymorphic transition of ε-CL-20 and raised the initial transition temperature and the activation energy.
    Źródło:
    Central European Journal of Energetic Materials; 2015, 12, 4; 689-702
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Combustion Characteristics and Mechanism of Boron-based, Fuel-rich Propellants with Agglomerated Boron Powder
    Autorzy:
    Xu, H. -X.
    Pang, W.-Q.
    Guo, H.-W.
    Zhao, F.-Q.
    Wang, Y.
    Sun, Z.-H.
    Powiązania:
    https://bibliotekanauki.pl/articles/358733.pdf
    Data publikacji:
    2014
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    analytical chemistry
    boron-based fuel-rich solid propellants
    agglomerated boron powder
    combustion performance
    combustion mechanism
    Opis:
    In order to extend the burning rate of boron-based, fuel-rich solid propellants with agglomerated boron powder, the effects of the boron content, the AP content, and of the magnesium powder content, on the burning rate and pressure exponent have been studied systematically. It has been shown that when the AP content is constant, the burning rate of the propellants increases with an increase in the agglomerated boron content. Furthermore, the burning rate and pressure exponent increase with increasing the contents of AP and magnesium powder. By means of single colour frame amplification photography and combustion wave tests, the combustion mechanism of these propellants has been investigated. It has been shown that the flame of the propellants becomes brighter by increasing the AP content, the dT/dxcp and dT/dxgp of the propellant FR-5 being around 6815 and 5789 °C/mm respectively, higher than those of FR-4, resulting in greater burning rates. The Ts of these propellants is above 683 °C, which is higher than the decomposition peak temperatures of agglomerated boron powder and of propellants (about 649 °C), which indicates that agglomerated boron powder is partially oxidized on the combustion surface, and the heat released from it may be beneficial to the combustion of the propellants.
    Źródło:
    Central European Journal of Energetic Materials; 2014, 11, 4; 575-587
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    The Microstructural Evolution in HMX Based Plastic-bonded Explosive During Heating and Cooling Process: an in situ Small-angle Scattering Study
    Autorzy:
    Yan, G.
    Tian, Q.
    Liu, J.
    Fan, Z.
    Sun, G.
    Zhang, C.
    Wang, Y.
    Chen, B.
    Gong, J.
    Zhou, X.
    Yang, Z.
    Nie, F.
    Li, J.
    Li, X.
    Powiązania:
    https://bibliotekanauki.pl/articles/358618.pdf
    Data publikacji:
    2016
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    SANS
    SAXS
    HMX-PBX
    thermal damages
    phase transition
    Opis:
    The thermal damage in octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine (HMX) based plastic-bonded explosive (PBX) was investigated using in situ small-angle neutron and X-ray scattering techniques. The microstructural evolution was quantitatively characterized by the model fitting parameters of total interfacial surface area (Sv) and void volume distribution. The Sv of HMX-PBX decreased markedly above 100 °C, indicating the movement of binder into the voids. After subsequent cooling to room temperature, the scattering intensity increased significantly with increasing storage time, and a new population of voids with average diameter of 20 nm was observed, accompanied by the gradual phase transition of HMX from δ- to β-phase. The experimental results implied that serious damage within the HMX-PBX was developed during storage after heating.
    Źródło:
    Central European Journal of Energetic Materials; 2016, 13, 4; 916-926
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-11 z 11

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