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Wyszukujesz frazę "hydrogen corrosion" wg kryterium: Temat

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    Wyświetlanie 1-4 z 4
    Tytuł:
    PEO layers on Mg-based metallic glass to control hydrogen evolution rate
    Autorzy:
    Cesarz-Andraczke, K.
    Kazek-Kęsik, A.
    Powiązania:
    https://bibliotekanauki.pl/articles/200823.pdf
    Data publikacji:
    2020
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    amorphous magnesium alloys
    corrosion rate
    plasma electrolytic oxidation
    hydrogen evolution
    Opis:
    The amorphous Mg-based alloys may be used as metallic biomaterials for resorbable orthopedic implants. The Mg-Zn-Ca metallic glasses demonstrate variable in time degradation rate in simulated body fluid. In this work the Mg66Zn30Ca4 alloy was chosen as a substrate for coatings. This paper reports on the surface modification of a Mg66Zn30Ca4 metallic glass by plasma electrolytic oxidation (PEO). The structure characterization of uncoated Mg66Zn30Ca4 alloy was performed by using TEMand XRD method. The immersion tests of coated and uncoated Mg66Zn30Ca4 alloy were carried out in Ringer’s solutionat 37°C. The volume of released hydrogen by immersion tests was determined. The coatings structure and chemical composition after immersion tests by SEM/EDS were studied. Based on SEM images of surface structure samples, immersion tests results and hydrogen evolution measurement was proposed the course of corrosion process in Ringer’s solution for Mg-based metallic glasses with PEO coating. Results of immersion tests in Ringer’s solution allowed to determine the amount of evolved hydrogen in a function of time for Mg66Zn30Ca4 metallic glass and sample with PEO coating. In comparison to the non-coated Mg66Zn30Ca4 alloy, the sample with PEO layer showed a significantly decreased hydrogen evolution volume.
    Źródło:
    Bulletin of the Polish Academy of Sciences. Technical Sciences; 2020, 68, 1; 119-124
    0239-7528
    Pojawia się w:
    Bulletin of the Polish Academy of Sciences. Technical Sciences
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Protection properties of conversion coatings based on nitrates for resorbable Mg alloy
    Autorzy:
    Cesarz-Andraczke, Katarzyna
    Powiązania:
    https://bibliotekanauki.pl/articles/2090712.pdf
    Data publikacji:
    2021
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    magnesium alloys
    protection coatings
    hydrogen evolution
    corrosion behavior
    stopy magnezu
    powłoki ochronne
    wydzielanie wodoru
    zachowanie korozyjne
    Opis:
    In this work, conversion coatings based on nitrates Ca(NO 3) 2 and Zn(NO 3) 2 were produced on the surface of MgZn49Ca4 to protect against corrosion. The main aim of this study was to prepare dense and uniform coatings using a conversion method (based on nitrates Ca(NO 3) 2 and Zn(NO 3) 2) for resorbable Mg alloys. The scientific goal of the work was to determine the pathway and main degradation mechanisms of samples with nitrate-based coatings as compared with an uncoated substrate. Determining the effect of the coatings produced on the Mg alloy was required to assess the protective properties of Mg alloy-coating systems. For this purpose, the morphology and chemical composition of coated samples, post corrosion tests and structural tests of the substrate were performed (optical microscopy, SEM/EDS). Immersion and electrochemical tests of samples were also carried out in Ringer’s solution at 37°C. The results of immersion and electrochemical tests indicated lower corrosion resistance of the substrate as compared with coated samples. The hydrogen evolution rate of the substrate increased with the immersion time. For coated samples, the hydrogen evolution rate was more stable. The ZnN coating (based on Zn(NO 3) 2) provides better corrosion protection because the corrosion product layer was uniform, while the sample with a CaN coating (based on Ca(NO 3) 2) displayed clusters of corrosion products. It was found that pitting corrosion on the substrate led to the complete disintegration and non-uniform corrosion of the coated samples, especially the CaN sample, due to the unevenly-distributed products on its surface.
    Źródło:
    Bulletin of the Polish Academy of Sciences. Technical Sciences; 2021, 69, 1; e136045, 1--7
    0239-7528
    Pojawia się w:
    Bulletin of the Polish Academy of Sciences. Technical Sciences
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Protection properties of conversion coatings based on nitrates for resorbable Mg alloy
    Autorzy:
    Cesarz-Andraczke, Katarzyna
    Powiązania:
    https://bibliotekanauki.pl/articles/2173570.pdf
    Data publikacji:
    2021
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    magnesium alloys
    protection coatings
    hydrogen evolution
    corrosion behavior
    stopy magnezu
    powłoki ochronne
    wydzielanie wodoru
    zachowanie korozyjne
    Opis:
    In this work, conversion coatings based on nitrates Ca(NO 3) 2 and Zn(NO 3) 2 were produced on the surface of MgZn49Ca4 to protect against corrosion. The main aim of this study was to prepare dense and uniform coatings using a conversion method (based on nitrates Ca(NO 3) 2 and Zn(NO 3) 2) for resorbable Mg alloys. The scientific goal of the work was to determine the pathway and main degradation mechanisms of samples with nitrate-based coatings as compared with an uncoated substrate. Determining the effect of the coatings produced on the Mg alloy was required to assess the protective properties of Mg alloy-coating systems. For this purpose, the morphology and chemical composition of coated samples, post corrosion tests and structural tests of the substrate were performed (optical microscopy, SEM/EDS). Immersion and electrochemical tests of samples were also carried out in Ringer’s solution at 37°C. The results of immersion and electrochemical tests indicated lower corrosion resistance of the substrate as compared with coated samples. The hydrogen evolution rate of the substrate increased with the immersion time. For coated samples, the hydrogen evolution rate was more stable. The ZnN coating (based on Zn(NO 3) 2) provides better corrosion protection because the corrosion product layer was uniform, while the sample with a CaN coating (based on Ca(NO 3) 2) displayed clusters of corrosion products. It was found that pitting corrosion on the substrate led to the complete disintegration and non-uniform corrosion of the coated samples, especially the CaN sample, due to the unevenly-distributed products on its surface.
    Źródło:
    Bulletin of the Polish Academy of Sciences. Technical Sciences; 2021, 69, 1; art. no. e136045
    0239-7528
    Pojawia się w:
    Bulletin of the Polish Academy of Sciences. Technical Sciences
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Hydrides precipitation in Ti6Al4V titanium alloy used for airframe manufacturing
    Autorzy:
    Băilă, D. I.
    Tonoiu, S.
    Powiązania:
    https://bibliotekanauki.pl/articles/200617.pdf
    Data publikacji:
    2019
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    hydrides precipitation
    Ti6Al4V alloy
    hydrogen embrittlement
    pitting corrosion
    wytrącanie wodorków
    Stop Ti6Al4V
    kruchość wodorowa
    korozja wżerowa
    Opis:
    The aeronautical industry is a sector constantly looking for new materials and equipment because of its tendency to expand quickly. The Ti6Al4V titanium alloy is used frequently in the aeronautic, aerospace, automobile, chemical and medical industry because it presents high strength combined with low density (approximately 4.5 g/cm3), good creep resistance (up to 550°C), excellent corrosion resistance, high flexibility, good fatigue and biocompatibility. As a result of these properties, this titanium alloy is considered an excellent material for manufacturing structural parts in the aircraft industry for modern aeronautic structures, especially for airframes and aero-engines. But its use is also problematic because the Ti6Al4V titanium alloy manifests hydrogen embrittlement, by means of hydrides precipitation in the metal. The Ti6Al4V alloy becomes brittle and fractures because of hydrogen diffusion into metal and because titanium hydrides appear and create pressure from within the metal, thus generating corrosion. Because of titanium hydrides, the titanium alloy suffers from reduced ductility, tensile strength and toughness, which can result in fractures of aeronautical parts. This poses a very serious problem for aircrafts. In this paper, rapid hydrogen embrittlement is presented along with XRD, SEM and TEM analysis. Its goal is to detect the presence of titanium hydrides and to spot the initial cracks in the metallic material.
    Źródło:
    Bulletin of the Polish Academy of Sciences. Technical Sciences; 2019, 67, 3; 643-649
    0239-7528
    Pojawia się w:
    Bulletin of the Polish Academy of Sciences. Technical Sciences
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-4 z 4

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