Informacja

Drogi użytkowniku, aplikacja do prawidłowego działania wymaga obsługi JavaScript. Proszę włącz obsługę JavaScript w Twojej przeglądarce.

Wyszukujesz frazę "SEM," wg kryterium: Temat


Wyświetlanie 1-8 z 8
Tytuł:
Cobalt adsorption on the nano-hydroxyapatite matrix: isotherm and kinetic studies
Autorzy:
Narwade, V. N.
Khairnar, R. S.
Powiązania:
https://bibliotekanauki.pl/articles/202076.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
hydroxyapatite
cobalt
adsorption
XRD
SEM
hydroksyapatyt
kobalt
adsorpcja
Opis:
Cobalt radionuclide is one of the prime contaminants generated during operation of pressurized heavy water. The paper reports the study of cobalt adsorption on hydroxyapatite (HAp) nanoceramic. A modified wet chemical precipitation method is used for HAp synthesis. The HAp nano-material is characterized by XRD, FTIR, TG/DTA, AFM, SEM, and EDAX. Experiments are performed in batches to observe the effect of cobalt adsorption on HAp matrix. The adsorption of cobalt on HAp is examined at room temperature. The isotherm and kinetic studies showed that the Freundlich isotherm and pseudo-second order model are the best choices to describe the nature of adsorption.
Źródło:
Bulletin of the Polish Academy of Sciences. Technical Sciences; 2017, 65, 2; 131-137
0239-7528
Pojawia się w:
Bulletin of the Polish Academy of Sciences. Technical Sciences
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Interfacial transition zone of cement paste-reactive aggregate in cement-zeolite mortars
Autorzy:
Owsiak, Z.
Czapik, P.
Powiązania:
https://bibliotekanauki.pl/articles/199790.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
alkali-aggregate reaction
SEM-EDS
mortar expansion
zeolites
zaprawa ekspansywna
zeolity
Opis:
Alkali-aggregate reaction is an expansive chemical reaction between the alkalis present in cement paste and minerals contained in aggregates. Mineral admixtures can mitigate the detrimental processes caused by this reaction. One of the minerals that reduce the effects of the alkali-aggregate reaction is natural zeolite. This study attempts to explain the process that takes place in the zone surrounding reactive gravel in the cement mortar made with an addition of natural zeolite. Mortar bar expansion tests were performed and a scanning electron microscope equipped with an energy-dispersive X-ray spectrometer was used to observe the paste-aggregate interfacial zone. The results confirmed the influence of the zeolite on the reduction in reactive aggregate-based mortar expansion. The microstructure of the aggregatepaste interfacial region was described and particular sub-zones varying in terms of calcium, sodium, potassium and silicon contents were determined.
Źródło:
Bulletin of the Polish Academy of Sciences. Technical Sciences; 2015, 63, 1; 31-34
0239-7528
Pojawia się w:
Bulletin of the Polish Academy of Sciences. Technical Sciences
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of lithium nitrate on the reaction between opal aggregate and sodium and potassium hydroxides in concrete over a long period of time
Autorzy:
Zapała-Sławeta, J.
Owsiak, Z.
Powiązania:
https://bibliotekanauki.pl/articles/200662.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
alkali-silica reaction
lithium nitrate
ettringite formation
expansion
SEM/EDS
azotan litu
ekspansja
Opis:
Alkali-silica reaction (ASR) is a reaction between amorphous or poorly crystallized siliceous phase, present in aggregates, and sodium and potassium hydroxides in the pore solution of concrete. Chemical admixtures such as lithium compounds are known to have high potential of inhibiting ASR. The aim of this study was to determine the effect of lithium nitrate on ASR in mortars containing high reactive opal aggregate over a long period of time. Mortar bar expansion tests were performed and microstructures of mortar bars were observed by scanning electron microscopy coupled with an energy dispersive X-ray microanalyser. Results from this study showed that effectiveness of lithium nitrate in mitigating ASR was limited over a long period of time. A larger amount of ASR gel which was formed in the presence of lithium nitrate indicated that the deterioration processes intensify within longer periods of time, which so far has not been observed in literature. Microscopic observation confirmed the presence of alkali-silica gel and delayed ettringite in mortars with lithium nitrate.
Źródło:
Bulletin of the Polish Academy of Sciences. Technical Sciences; 2017, 65, 6; 773-778
0239-7528
Pojawia się w:
Bulletin of the Polish Academy of Sciences. Technical Sciences
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Residual life estimation of fabricated humidity sensors using different artificial intelligence techniques
Autorzy:
Bhargava, C.
Aggarwal, J.
Sharma, P. K.
Powiązania:
https://bibliotekanauki.pl/articles/201564.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
composite material
artificial intelligence
humidity sensor
accelerated life testing
SEM
materiał kompozytowy
sztuczna inteligencja
czujnik wilgotności
Opis:
Background: a humidity sensor is used to sense and measure the relative humidity of air. A new composite system has been fabricated using environmental pollutants such as carbon black and low-cost zinc oxide, and it acts as a humidity sensor. Residual life of the sensor is calculated and an expert system is modelled. For properties and nature confirmation, characterization is performed, and a sensing material is fabricated. Methodology: characterization is performed on the fabricated material. Complex impedance spectroscopy (CIS), Fourier transform infrared spectroscopy (FTIR), X-ray diffraction (XRD) and scanning electron microscopy (SEM) are all used to confirm the surface roughness, its composite nature as well as the morphology of the composite. The residual lifetime of the fabricated humidity sensor is calculated by means of accelerated life testing. An intelligent model is designed using artificial intelligence techniques, including the artificial neural network (ANN), fuzzy inference system (FIS) and adaptive neuro-fuzzy inference system (ANFIS). Results: maximum conductivity obtained is 6.4£10−3 S/cm when zinc oxide is doped with 80% of carbon black. Conclusion: the solid composite obtained possesses good humidity-sensing capability in the range of 30–95%. ANFIS exhibits the maximum prediction accuracy, with an error rate of just 1.1%.
Źródło:
Bulletin of the Polish Academy of Sciences. Technical Sciences; 2019, 67, 1; 147-154
0239-7528
Pojawia się w:
Bulletin of the Polish Academy of Sciences. Technical Sciences
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Experimental research on influence of gas impact on thermal and mechanical properties of auxetic material covered with titanium silicide coating
Autorzy:
Miedzińska, D.
Gieleta, R.
Małek, E.
Zasada, D.
Stankiewicz, M.
Marszałek, K.
Powiązania:
https://bibliotekanauki.pl/articles/201182.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Ti-Si layers
damage
impact
thermal resistance
SEM
auxetic materials
Ti-Si
uszkodzenia
uderzenia
opór cieplny
materiały auksetyczne
Opis:
The aim of the presented work was to study the auxetic textiles covered with titanium silicide coating. The research was carried out to develop the material structure, which will be used for protective clothing, e.g. for firemen. The new material should be characterized by increased heat resistance coupled with protection against gas pressure impact caused e.g. by gas installation damage. In the paper, an assessment of the change in heat resistance properties of a Ti-Si coated auxetic textile loaded with gas pressure impulse was carried out.
Źródło:
Bulletin of the Polish Academy of Sciences. Technical Sciences; 2018, 66, 2; 165-172
0239-7528
Pojawia się w:
Bulletin of the Polish Academy of Sciences. Technical Sciences
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis and characterization of AA5083 and AA2024 reinforced with SiO2 particles
Autorzy:
Raja, R.
Jannet, S.
Thampy, M. A.
Powiązania:
https://bibliotekanauki.pl/articles/200119.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
in situ reaction
SEM
wear rate
stir casting
tensile strength
EDX
reakcja in situ
szybkość zużywania
wytrzymałość na rozciąganie
Opis:
Among the types of different particulates, silica is a standout as one of the the cheapest and low-density particulates accessible in substantial amounts. The present study has been centered around the synthesis and study of aluminum matrix composite strengthened with nano-sized SiO2  particles of various weight percentage by means of the stir casting technique. The EDX emphasized the presence of various elements and augmented the in situ reaction. The tensile strength and wear studies were also carried out. The reinforcement materials percentage variation was one of the important factors for the present studies. The Aluminum Alloy 5083 and 2024, which are magnesium and copper-based alloys, had a significant effect on the material characterization.
Źródło:
Bulletin of the Polish Academy of Sciences. Technical Sciences; 2018, 66, 2; 127-132
0239-7528
Pojawia się w:
Bulletin of the Polish Academy of Sciences. Technical Sciences
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Corrosion behavior of ZrC particles reinforcement with Al-12Si composites by weight loss method using acidic media
Autorzy:
John, C. F.
Paul, R. C.
Singh, S. C. E.
Jacobjose, J.
Ramkumar, T.
Hikku, G. S.
Sharma, R. K.
Sengottuvel, P.
Powiązania:
https://bibliotekanauki.pl/articles/200059.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Al-Si-ZrC composites
powder metallurgy
weight loss method
corrosion rate
SEM
kompozyty Al-Si-ZrC
metalurgia proszków
metoda redukcji masy
szybkość korozji
Opis:
This paper aims to investigate the corrosion behavior of zirconium carbide (ZrC) reinforced Al – Si metal matrix composites (MMCs) in a mixture of acidic solution using weight loss method. The composites are prepared by powder metallurgy method. Al-12Si-xZrC composites containing 0, 5, and 10 weight percentage of ZrC particles are compacted in a die set assembly and sintered in an inert gas muffle furnace. The acidic solutions used for corrosion are 1 N HCl, 1 N H2SO4 and 1 N HNO3. The corrosion characteristics of Al-12Si-xZrC composites and the pure Al were experimentally evaluated. The corrosion test was carried out at different weight proportions of the samples in various concentrations of the acid such as 1 N HCl, 1 N H2SO4 and 1 N HNO3 for different exposure time (i.e., 24 h, 72 h, 144 h and 216 h), respectively. The results specified that corrosion rate of composites was lower than that of base metal Al under the corrosive atmosphere, regardless of exposure time and acidic solutions used as corrodents. Al-12Si-xZrC composites become more corrosion resistant as the ZrC content is increased. This is because of the development of stable oxide layer above the specimens. Scanning electron microscopy (SEM) confirms the degree of attack of acidic solution on the surface of the examined material.
Źródło:
Bulletin of the Polish Academy of Sciences. Technical Sciences; 2018, 66, 1; 9-16
0239-7528
Pojawia się w:
Bulletin of the Polish Academy of Sciences. Technical Sciences
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The possibility of producing graded Al2O3-Mo, Al2O3-Cu, Al2O3-W composites using CSC method
Autorzy:
Wachowski, M.
Kaszuwara, W.
Miazga, A.
Konopka, K.
Zygmuntowicz, Justyna
Powiązania:
https://bibliotekanauki.pl/articles/201338.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
centrifugal slip casting
ceramic-metal composites
SEM
Al2O3-Mo
Al2O3-Cu
Al2O3-tungsten
Al203-W
odlewanie odśrodkowe
kompozyty ceramiczno-metalowe
Al2O3-W
Opis:
The subject of the study was the production and characterization of three ceramic-metal graded composites, which differed in addition of the metallic phase. The following composites systems were investigated: Al2O3-Mo, Al2O3-Cu, Al2O3-W. Composites were produced by centrifugal slip casting method. This technique combines the classic casting of the slurry into porous molds with the action of centrifugal force. As a result, sleeve-shaped shapes with a metallic phase gradient were obtained. X-ray phase analysis have not revealed new phases in the produced composites. The type of metallic phase and its distribution in the ceramic matrix influenced the hardness of the produced composites.
Źródło:
Bulletin of the Polish Academy of Sciences. Technical Sciences; 2019, 67, 2; 179-184
0239-7528
Pojawia się w:
Bulletin of the Polish Academy of Sciences. Technical Sciences
Dostawca treści:
Biblioteka Nauki
Artykuł
    Wyświetlanie 1-8 z 8

    Ta witryna wykorzystuje pliki cookies do przechowywania informacji na Twoim komputerze. Pliki cookies stosujemy w celu świadczenia usług na najwyższym poziomie, w tym w sposób dostosowany do indywidualnych potrzeb. Korzystanie z witryny bez zmiany ustawień dotyczących cookies oznacza, że będą one zamieszczane w Twoim komputerze. W każdym momencie możesz dokonać zmiany ustawień dotyczących cookies