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Wyświetlanie 1-2 z 2
Tytuł:
Facile synthesis of chitosan/CuO nanocomposites for potential use as biocontrol agents
Autorzy:
Siriphannon, P.
Iamphaojeen, Y.
Powiązania:
https://bibliotekanauki.pl/articles/201687.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
chitosan
CuO
nanocomposite
hydrothermal
antibacterial activity
chitozan
nanokompozyt
aktywność przeciwbakteryjna
Opis:
Chitosan/CuO nanocomposites (Chi/CuO) were prepared by facile and eco-friendly technique. The 2%w/v chitosan solution was mixed with 0.5 %w/w sodium tripolyphosphate (STPP), resulting in the formation of ionically crosslinked chitosan. The crosslinked chitosan was soaked in an aqueous solution containing 0.001, 0.01 or 0.1 mol/L CuSO4·5H2O for 24 hrs, in which the Cu2+ ions were absorbed into the chitosan network, forming as the chitosan/Cu2+ precursors. The chitosan/Cu2+ precursors were hydrothermally reacted in two different basic media, i.e. NaOH and NH4OH, at 100°C for 24 hrs, resulting in the nano-sized CuO crystals hydrothermally grew and embedded in the crosslinked chitosan matrix. The CuO grown in the NaOH possessed larger crystallite size and higher crystallinity than that in the NH4OH. In addition, the CuO crystallite size in the nanocomposites increased with the increase of initial concentration of Cu2+ starting agent due to the increase of Cu2+ quantity in the chitosan/Cu2+ precursors. The chitosan/CuO nanocomposites prepared by using 0.01 and 0.1 mol/L Cu2+ could exhibit the antibacterial activities after intimate contact with Staphylococcus aureus and Escherichia coli under JIS L 1902:1998 (Qualitative) test method, indicating their potential use as biocontrol agents.
Źródło:
Bulletin of the Polish Academy of Sciences. Technical Sciences; 2018, 66, 3; 311-316
0239-7528
Pojawia się w:
Bulletin of the Polish Academy of Sciences. Technical Sciences
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis, characterization and catalytic properties of SAPO-11 molecular sieve synthesized in hydrothermal media using di-isopropylamine as template
Autorzy:
Chellappa, T.
Costa, M. J. F.
Nascimento, W. A.
Ferreira De Lima, L.
Bassan, I. A.
Tavares, M.
Fernandes, V. J.
Menezes, A.
Guilherme Meira, L.
Telesforo Nóbrega De Medeiros, J.
Maribondo Do Nascimento, R.
Powiązania:
https://bibliotekanauki.pl/articles/200372.pdf
Data publikacji:
2014
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
microporous materials
SAPO-11
characterization
catalytic activity
molecular sieves
Opis:
A microporous SAPO-11 Molecular sieve was successfully synthesized by the hydrothermal method, using a single agent, as an organic template: di-isopropylamine (DIPA). The obtained solid was calcined at 550C for three hours, after which the flow of nitrogen was exchanged for that of synthetic air and submitted for another ten hours of calcination, so as to remove the single agent: di-isopropylamine, which after the removal of the template could be observed by the high crystallization of the sample. Furthermore, the molecular sieve was characterized by XRD, SEM, TG-DTG and N2 adsorption desorption (BET analysis). The obtained catalyst proved to have a high potential catalytic activity and selectivity, through the obtained characterization results, exhibiting good hydrothermal stability. The catalytic performance of SAPO-11 was tested by the deactivation/regenerability of the coked sample, furthered by cracking of n-hexane reaction and high olefins selectivity was obtained.
Źródło:
Bulletin of the Polish Academy of Sciences. Technical Sciences; 2014, 62, 3; 481-488
0239-7528
Pojawia się w:
Bulletin of the Polish Academy of Sciences. Technical Sciences
Dostawca treści:
Biblioteka Nauki
Artykuł
    Wyświetlanie 1-2 z 2

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