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Tytuł:
Effect of Particle Sizes of Slag on Reduction Characteristics of Nickel Slag-Coal Composite Briquette
Autorzy:
Li, Xiaoming
Li, Yi
Xing, Xiangdong
Wang, Yanjun
Wen, Zhenyu
Yang, Haibo
Powiązania:
https://bibliotekanauki.pl/articles/2049420.pdf
Data publikacji:
2021
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
resources reutilization
nickel slag
particle size
direct reduction
reduction characteristics
Opis:
Nickel slag has a high-content iron and is a secondary utilization resource with great development potential. The coal-based direct reduction is an innovative technology that can be used to utilize the iron resources in nickel slag. The effect of the particle size of nickel slag on the strength and the reduction of nickel slag-coal composite briquettes were investigated. Four samples with particle size of 75~106 μm, 106~150 μm, 150~270 μm, and >270 μm were selected. The drop strength increased 9.4 times and the compressive strength reached 281.1 N when the nickel slag particle size decreased from >270 μm to 75~106 μm. The reduction degree determined by the data from the thermogravimetric experiment indicated that its maximum was 79.545%. The reduction experiments performed at 1200°C for 45 minutes indicated that the nickel slag with particle sizes between 75~106 μm were appropriate for the reduction of the nickel slag-coal composite briquettes.
Źródło:
Archives of Metallurgy and Materials; 2021, 66, 1; 127-134
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Reduction of Industrial Nickel Oxides with a Hydrogen Bearing Gas Between 523 and 673K
Autorzy:
Plascencia, G.
Powiązania:
https://bibliotekanauki.pl/articles/352276.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
nickel oxides reduction
hydrogen reduction
Avrami-Erofeyev kinetic model
nucleation and growth
activation energy
Opis:
Reduction of three industrial nickel oxides (Goro, Tokyo and Sinter 75) with a hydrogen bearing gas was revisited in the temperature interval from 523 to 673 K (250 to 400°C). A pronounced incubation period is observed in the temperature interval tested. This period decreases as the reduction temperature increases. Thermogravimetric data of these oxides were fitted using the Avrami-Erofeyev kinetic model. The reduction of these oxides is controlled by a nucleation and growth mechanism of metallic nickel over the oxides structure. Rate kinetic constants were re-evaluated and the activation energy for the reduction of these oxides was re-calculated.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 2; 781-789
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of Different Plants Extracts on Silver Nanopar ticles Green Synthesis
Autorzy:
Velgosova, O.
Mražíková, A.
Veselovský, L.
Willner, J.
Fornalczyk, A.
Powiązania:
https://bibliotekanauki.pl/articles/351682.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
nanoparticles
silver
biosynthesis
reduction agents
TEM
Opis:
Three plants extracts were used for biosynthesis of Ag nanoparticles (AgNPs). AgNPs nucleation process requires effective reduction agents which secure Ag+ to Ag0 reduction and also stabilizing/capping agents. The UV-vis and TEM observation revealed that the best results were obtained by R. officinalis leaf extract. The strong SPR band peak appeared at the wavelength 418 nm. Synthetized AgNPs were globular, fine (~20 nm), uniform and stabile throughout the experiment. A rapid rate of AgNPs synthesis was also significant and economically advantageous factor. Fine (10-20 nm) and globular nanoparticles were synthetized also by U. dioica leaf extract, but the stability of nanoparticles was not permanent. Despite V. vitis-idaea fruit extract contains a lot of reducing agents, UV-vis did not confirm the presence of AgNPs in solution. Synthetized Ag particles were very unstable, Ag particles agglomerated very fast and clearly indicated sediment was formed.
Źródło:
Archives of Metallurgy and Materials; 2019, 64, 2; 665-670
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Preparation of Nickel Nanoparticles Using Nickel Raffinate Separated by Solvent Extraction from The Spent FeCl3 Etching Solution
Autorzy:
Park, Il-Jeong
Swain, Basudev
Kim, Dae-Weon
Kim, Geon-Hong
Han, Deok-Hyun
Jung, Hang-Chul
Powiązania:
https://bibliotekanauki.pl/articles/354453.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
nickel
recycling
solvent extraction
chemical reduction
Opis:
FeCl3 bearing etching solution is mainly used for etching of metals used in shadow masks, PCBs and so on. Due course of Invar alloy etching process the FeCl3 bearing etching solution get contaminated with Ni2+ which affect adversely the etching efficiency. Hence, FeCl3 bearing etching solution discarded after several cycle of operation causes an environmental and economic problem. To address both the issues the etching solution was purified through solvent extraction and remained Ni2+ recovered by wet chemical reduction using hydrazine. For optimum Fe3+ extraction efficiency, various extraction parameter were optimized and size and morphology of the recovered pure Ni powder was analyzed. The reported process is a simple process to purify and recover Ni from industry etching solution.
Źródło:
Archives of Metallurgy and Materials; 2019, 64, 2; 531-534
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Numerical Modeling of Copper Reduction in Fire Refining Process
Autorzy:
Kolczyk, E.
Miczkowski, Z.
Czernecki, J.
Powiązania:
https://bibliotekanauki.pl/articles/354138.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
numerical modelling
copper reduction
anode furnace
tuyere
Opis:
Copper reduction represents one of the steps in the process of fire refining of blister copper. Process of copper reduction with natural gas as performed in the anode furnace was modeled. Numerical analysis was conducted using the IPSA (Inter- Phase-Slip Algorithm) module of PHOENICS package and standard turbulent model k - ε. The model takes into account the liquid phase - slag and phase of natural gas which is supplied through the tuyere from the bottom of the charge. Calculations were made for two different diameters of tuyeres for supply of reducer. Based on the calculations and analysis, it was found out that the gas flow which causes strong movement in the bath guarantees homogeneous composition of the liquid copper in each process stage. Application of a tuyere with a larger diameter results in a greater intensity of the reduction process and better use of the reducer.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 2A; 521-528
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Recovery of Pig Iron from Copper Smelting Slag by Reduction Smelting
Autorzy:
Erdenebold, U.
Choi, M.-H.
Wang, J.-P.
Powiązania:
https://bibliotekanauki.pl/articles/355067.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
copper slag
reduction
pig iron
fayalite
recovery
Opis:
Copper slag is a by-product obtained during smelting and refining of copper. Copper smelting slag typically contains about 1 wt.% copper and 40 wt.% iron depending upon the initial ore quality and the furnace type. Main components of copper slag are iron oxide and silica. These exist in copper slag mainly in the form of fayalite (2FeO ·SiO2 ). This study was intended to recover pig iron from the copper smelting slag by reduction smelting method. At the reaction temperature of below 1400°С the whole copper smelting slag was not smelted, and some agglomerated, showing a mass in a sponge form. The recovery behavior of pig iron from copper smelting slag increases with increasing smelting temperature and duration. The recovery rate of pig iron varied greatly depending on the reaction temperature.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 4; 1793-1798
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Thermodynamics and Kinetics Analysis on Carbothermic Reduction of Calcined Magnesite in Vacuum
Autorzy:
Tang, Qifeng
Ao, Jinqing
Peng, Biyou
Guo, Biao
Yang, Tao
Powiązania:
https://bibliotekanauki.pl/articles/2125546.pdf
Data publikacji:
2022
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
calcined magnesite
carbothermic reduction
vacuum
thermodynamics
kinetics
Opis:
The carbothermic reduction of calcined magnesite in vacuum was studied. By thermodynamic analysis, the starting temperature of reduction reaction dropped from 2173K to 1523K when system pressure dropped from 1 atmosphere to 100 Pa. The experiments were carried out at different conditions under 10~100 Pa and the experimental results shown that the reduction extent of MgO improved by increasing the reaction temperature and time, the pellet forming pressure as well as adding fluoride as catalyst. The rate-determining step of carbothermic reduction process was gas diffusion with the apparent activation energy of 241.19~278.56 kJ/mol.
Źródło:
Archives of Metallurgy and Materials; 2022, 67, 3; 1021--1026
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
A Study on the Recovery of Zinc and Pig Iron from Byproducts after Steelmaking Dust Treatment
Autorzy:
Wang, Jei-Pl
Powiązania:
https://bibliotekanauki.pl/articles/2203737.pdf
Data publikacji:
2023
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
steelmaking dust
reduction
recovery
zinc
pig iron
Opis:
In this study, a research was conducted to recover metallic zinc and pig iron and to improve the purity and the recovery rate through a reduction process for zinc and iron in the byproducts that are generated after steelmaking dust treatment. As the result of the calcination, it was confirmed that Cl (6.06%) and K (3.37%) decreased to Cl (2.75%) and K (0.22%), respectively. For the zinc powder that was recovered with reaction temperature of 1100°C, reaction time of 4 hours, and argon gas of 1L/min as the optimal conditions. The measurement for the purity of zinc was 99.8% and the recovery rate was 92.14%. The melt reduction for recovering pig iron from the residue was reacted under reaction temperature of 1600°C, flux composition (CaO:SiO2) of 1:1, and reducing agent infusion ratio (residue: C) of 14:1, and the pig iron was measured to have a purity of 87.7% and a recovery rate of 91.81%.
Źródło:
Archives of Metallurgy and Materials; 2023, 68, 1; 205--208
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Reduction Kinetics Behavior of FeO-CaO-SiO2-MgO-Al2O3 Molten Slag Using Solid-Carbon
Autorzy:
Gao, Q.
Shen, Y.
Wei, G.
Shen, F.
Powiązania:
https://bibliotekanauki.pl/articles/353876.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
kinetics
molten slag
reduction
blast furnace
carbon
Opis:
Reduction of FeO-bearing molten slag using solid-carbon, existing in primary slag of blast furnace (BF), consumes much BF energy. It is also a limit for BF efficiency. In this paper, reduction kinetics behavior of FeO-CaO-SiO2-MgO-Al2O3 molten slag (primary slag of BF) was investigated, and the restrictive step of the reaction was identified. It has been found that the reduction process of FeO-CaO-SiO2-MgO-Al2O3 BF slag using solid-carbon is a second-order reaction. And the reduction process is controlled by both diffusion of FeO and gasification reaction of carbon in molten slag. The apparent activation energy of reaction is 342.37 kJ/mol, the diffusion activation energy of FeO in molten slag is 355 kJ/mol, and the gasification reaction activation energy of carbon is 152.98 kJ/mol. Additionally, it is also concluded that reduction rate is influenced by temperature (T), mass fraction of FeO (w(FeO)), and basicity (R) of the slag. Moreover, a reduction model of this slag system was established and verified by a series of experiments.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 1; 257-263
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Utilization of the steelmaking slag by reduction with the use of the modified the chemical composition of the input material
Zagospodarowanie żużli stalowniczych poprzez zastosowanie metody redukcji i modyfikacji składu chemicznego materiału redukowanego
Autorzy:
Falkus, J.
Trębacz, L.
Zawada, B.
Powiązania:
https://bibliotekanauki.pl/articles/353341.pdf
Data publikacji:
2010
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
żużel
utylizacja
redukcja
modelowanie
slag
utilization
reduction
modeling
Opis:
Utilization of the steelmaking slag by reduction is the technology which seems to be today rather controversial. However it is possible to use this way of utilization in case if the economical surround will be changed. One of the possible improvement for the described method is the modifying input materials for process reduction. The thermodynamic model was developed which enable to optimize the chemical composition of the final product. The laboratory investigations confirmed a good agreement between model calculations and experimental results.
Zastosowanie technologii redukcji żużla do utylizacji żużli stalowniczych wydaje się być dzisiaj pomysłem kontrowersyjnym. Jednakże wybór tej ścieżki utylizacji może stać się prawdopodobny w sytuacji zmiany warunków ekonomicznych w otoczeniu branży hutniczej. Jedną z metod udoskonalenia rozważanej technologii jest zastosowanie metody modyfikowania materiału wejściowego do procesu redukcji. Opracowany został model termodynamiczny, który umożliwia optymalizację składu chemicznego finalnego produktu prowadzonego procesu. Badania laboratoryjne potwierdziły dobrą zgodność obliczeń modelowych z wynikami eksperymentów.
Źródło:
Archives of Metallurgy and Materials; 2010, 55, 4; 1105-1112
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Numerical investigation of heat exchange in rotary furnace
Autorzy:
Kolczyk, E.
Miczkowski, Z.
Czernecki, J.
Powiązania:
https://bibliotekanauki.pl/articles/354348.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
numerical simulation
heat exchange
rotary furnace
slag reduction process
Opis:
Process of heat exchange in a rotary furnace during converter slag reduction was modelled.Temperature distribution in the furnace and temperature of the charge (slag) only were examined. Influence of modification of the process gas supply method by changing the number of nozzles on the course of the reduction process was analyzed. It has been found out that application of a nozzle as a submerged flame burner provides possibilities to reach higher charge temperature. Application of more nozzles in the process of converter slag reduction can increase temperature of reduced slag and provide better uniformity of charge heating.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 1; 149-153
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Numerical Modelling of Chamfer Billet of High Carbon Steel During Continuous Casting
Autorzy:
Zong, Nanfu
Ma, Sida
Sun, Weizhao
Liu, Yang
Jing, Tao
Powiązania:
https://bibliotekanauki.pl/articles/2125549.pdf
Data publikacji:
2022
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
chamfer billet
internal cracks
GCr15 steel
soft reduction
Opis:
The formation of internal cracks in as-cast billet is mainly attributed to the stress and strain states near the solidifying front. This study investigates the effect of chamfer configuration of as-cast billet on the maximal principal stress and the tensile stress during soft reduction process. The LIT and ZDT of GCr15 bearing steel are calculated by the solidification phase transformation model. What’s more, the 3D finite element models is established to investigate stress and strain states in the brittle temperature range. The relationships between chamfer angle and maximal principal stress, internal crack, as well as equivalent plastic strain are analyzed. Numerical results reveal that a chamfer configuration of as-cast billet is much more effective than a rectangular one on decreasing the risk of internal cracks.
Źródło:
Archives of Metallurgy and Materials; 2022, 67, 3; 967--974
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
A Novel FE/MC-based Mathematical Model of Mushy Steel Deformation with GPU Support
Autorzy:
Hojny, Marcin
Dębiński, Tomasz
Powiązania:
https://bibliotekanauki.pl/articles/2106557.pdf
Data publikacji:
2022
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
FEM
Monte Carlo
extra-high temperatures
soft-reduction
GPU
Opis:
The paper presents the results of work leading to the construction of a spatial hybrid model based on finite element (FE) and Monte Carlo (MC) methods allowing the computer simulation of physical phenomena accompanying the steel sample testing at temperatures that are characteristic for soft-reduction process. The proposed solution includes local density variations at the level of mechanical solution (the incompressibility condition was replaced with the condition of mass conservation), and at the same time simulates the grain growth in a comprehensive resistance heating process combined with a local remelting followed by free/controlled cooling of the sample tested. Simulation of grain growth in the entire computing domain would not be possible without the support of GPU processors. There was a 59-fold increase in the computing speed on the GPU compared to single-threaded computing on the CPU. The study was complemented by examples of experimental and computer simulation results, showing the correctness of the adopted model assumptions.
Źródło:
Archives of Metallurgy and Materials; 2022, 67, 2; 735--742
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Recovery of Iron from Copper Slag by Carbothermic Reduction and Magnetic Separation in the Presence of CaO
Autorzy:
Chun, T.
Mu, G.
Di, Z.
Long, H.
Ning, C.
Li, D.
Powiązania:
https://bibliotekanauki.pl/articles/355597.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
copper slag
recovery of iron
carbothermic reduction
magnetic separation
Opis:
The carbothermic reduction of copper slag at the different binary basicity (CaO/SiO2 ) was carried out for recovering iron by wet magnetic separation. Calcium carbonate is found to be capable of improving the iron recovery, as well as increasing the particle size of metallic iron significantly. Experimental evidence showed that CaO reacted with SiO2 to form calcium silicate and FeO was liberated from the 2FeO.SiO2 , decreased the content of Fe in the slags, which improved the iron recovery during the magnetic separation. The final product, assaying 90.23%Fetotal (representing a metallization degree of 93.94%) and 0.58% Cu at the iron recovery of 85.70% was achieved at the basicity of 0.60, which can be briquetted as a burden material for weathering resistant steel making by electric arc furnace to replace part of scrap.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 1; 299-305
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of Internal Cracking on Carbide Precipitation in Continuous Casting Bloom Induced by Soft Reduction Technology and the Resulting Segregated Band in Hot-Rolled Wire Rods
Autorzy:
Zong, Nanfu
Jing, Tao
Liu, Yang
Powiązania:
https://bibliotekanauki.pl/articles/2048876.pdf
Data publikacji:
2022
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
internal cracking
carbide precipitation
segregated band
soft reduction technology
Opis:
Internal cracking surrounding primary carbides in high carbon steel as-cast blooms induced by soft reduction is investigated to elucidate their influence of internal cracking on carbide precipitation and the resulting segregated band in hot-rolled wire rods. The primary carbides precipitation in high carbon steel has been investigated using both experimental observations and finite element simulations for as-cast blooms induced by soft reduction. It is found that the carbides precipitation in the vicinity of existing internal cracks is often located midway between the surface and centreline of the bloom, further increases the occurrence of the segregated bands in the hot-rolled wire rods. In addition, the growth of primary carbides surrounding the internal cracking are based on the chemical driving force and high density precipitate zones have been clarified in continuous casting bloom induced by soft reduction. It clearly shows that the spatial distribution of internal cracking surrounding primary carbides that play a key role in the formation of the segregated bands in the final steel products.
Źródło:
Archives of Metallurgy and Materials; 2022, 67, 1; 73-82
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 34

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