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Wyświetlanie 1-15 z 26
Tytuł:
Electrical Conductivity and Morphology Study of Polyaniline Powder Synthesised with Various Doping Ions
Autorzy:
Golba, S.
Popczyk, M.
Miga, S.
Jurek-Suliga, J.
Zubko, M.
Powiązania:
https://bibliotekanauki.pl/articles/351230.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
polyaniline
conductive polymers
conductivity
morphology
Opis:
Powdered polyaniline (PANI) was synthesised chemically with different doping anions namely hydrochloric acid, sulphuric acid and para-toluenesulfonic acid (pTSA). Two-step synthetic procedure was utilised at low temperature. The highest reaction efficiency was found for chlorine-doped PANI. Structural characterization with FTIR revealed the vibration bands characteristicto formation of the emeraldine salt. The surface morphology of doped PANIs was studied by SEM images which showed near globular shape and porous structures with different size of the aggregated particles. They were smaller for Cl-- or pTS--doped PANI while for SO4 2- the size was markedly larger. The XRD patterns revealed that there are ordered regions especially for pTS- doped PANI, while the highest conductivity value was recorded for Cl- doped one followed by organic pTS- doped and SO4 2- doped one.
Źródło:
Archives of Metallurgy and Materials; 2019, 64, 3; 1023-1028
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Decopperization and Coagulation by Use the Carbon-N-Ox Method
Autorzy:
Bydałek, A.
Migas, P.
Wołczyński, W.
Karwan-Baczewska, J.
Powiązania:
https://bibliotekanauki.pl/articles/355826.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
crystals morphology
calcium compounds
copper slag
salts
Opis:
This paper discusses the impact of complex chemical reagents during the process of decopperisation of slag. The beneficial effect of carbide response factors with the participation of nitrogen was indicated as well as the role of stimulators surfactants. Based on the results of the research the basic structure of the slag during decopperisation was systematized. The effects of coagulation of droplets of copper in the slag were shown in this paper.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 4; 2375-2380
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Using Deep Etching in the Study of Eutectic Silicon 3D-Morphology in AlSi7MgTi Cast Alloy
Autorzy:
Kuchariková, L.
Tillová, E.
Bonek, M. S.
Chalupová, M.
Powiązania:
https://bibliotekanauki.pl/articles/356318.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
modification
refinement
eutectic Si morphology
deep etching
Opis:
The effect of combination grain refinement with AlTi5B1 master (55 ppm) and Sr-modification with AlSr5 master (20, 30, 40, 50 and 60 ppm) on the microstructure, tensile and hardness properties of AlSi7MgTi cast alloy were systematically investigated. Eutectic silicon was studied by optical and scanning electron microscopy after standard (0.5% HF) and deep etching (HCl). Morphology of eutectic Si changes from compact plate-like (as-cast state) to fibbers (after modification). Si-fibbers in samples with 50 and 60 ppm Sr coarsen probably as a result of over-modification. The optimum mechanical properties has the experimental material which was grain refined and modified with 40 ppm of Sr (UTS = 220.6 MPa; ductility = 6.1%, and 82.3 HBW 5/250/15).
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 4; 2017-2022
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Studies on Viscoelastic, Thermal and Morphological Properties of Vinyl Ester - Mixed Diluents System
Autorzy:
Ranjan, J. K.
Raghu Raja Pandiyan, K.
Goswami, S.
Powiązania:
https://bibliotekanauki.pl/articles/354420.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
vinyl ester resin
dynamic mechanical analysis
TGA
DSC
morphology
Opis:
Vinyl ester resin networks formed by using mixture of diluents were prepared. Methyl methacrylate (MMA) diluent was mixed in various proportions with vinyl ester resin which was already premixed with styrene diluent (45 wt. %). Weight ratios e.g. 80:20, 70:30 and 60:40 of VE resin: MMA diluents were studied. Viscoelastic properties of the cross-linked resin were studied by dynamic mechanical analyzer in terms of storage modulus and tanδ. Thermal analysis was performed using non-isothermal mode of Differential scanning calorimetry. The samples with mixed diluents, showed higher modulus, and glass transition temperature in comparison to that of the pure vinyl ester-styrene resin cross-linked in presence of styrene only. The difference in thermal stability between vinyl ester-styrene and vinyl ester-MMA-styrene was checked. Vinyl Ester – 20 wt. % MMA-Styrene samples have the best thermal property among all other prepared samples. Multiphase morphology was formed for the thermoset crosslinked with mixed diluents in contrast to that formed with single diluent. With increase in MMA content in the resin dispersed domain size increased.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 3; 1845-1850
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Research on Distribution and Morphology of Primary Si Under the Effect of Direct Current
Autorzy:
Li, Jiayan
Njuguna, Benson Kihono
Ni, Ping
Wang, Liang
Tan, Yi
Powiązania:
https://bibliotekanauki.pl/articles/2049663.pdf
Data publikacji:
2021
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
silicon source
direct current
Joule heating
Si morphology
Fe impurity
Opis:
A source of pure silicon was added into an alloy refining system during a refining process with the application of a direct electric current. The effect of the temperature difference between the graphite electrodes and the alloy was decreased. The temperature increase value (ΔT) of the Al-28.51wt.%Si alloy sample caused by Joule heating was calculated by weighing the mass of primary silicon. When the current density was 5.0×105A/m2, the overall temperature increase in the alloy was about 90°C regardless of the alloy composition. Adequate silicon atoms recorded the footprint of the electric current in the alloy melt. The flow convection generated by the electric current in the melt during the solidification process resulted in the refinement of primary silicon. The Fe impurity content in alloy refining without the electric current density was 2.16 ppm. However, it decreased to 1.27 ppmw with the application of an electric current density of 5.0×105A/m2.
Źródło:
Archives of Metallurgy and Materials; 2021, 66, 2; 367-372
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Effect of Gas Pressure on Powder Size and Morphology in The Production of AZ91 Powder by Gas Atomization Method
Autorzy:
Akkaş, M.
Çetin, T.
Boz, M.
Powiązania:
https://bibliotekanauki.pl/articles/351517.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
gas atomization
AZ91 alloy powder
gas pressure
powder morphology
Opis:
In this study, the effect of gas pressure on the shape and size of the AZ91 alloy powder produced by using the gas atomization method was investigated experimentally. Experiments were carried out at 820°C constant temperature in 2-mm nozzle diameter and by applying 4 different gas pressures (0.5, 1.5, 2.5 and 3.5 MPa). Argon gas was used to atomize the melt. Scanning electron microscope (SEM) to determine the shape of produced AZ91 powders, XRD, XRF and SEM-EDX analysis to determine the phases forming in the internal structures of the produced powders and the percentages of these phases and a laser measuring device for powder size analysis were used. Hardness tests were carried out to determine the mechanical properties of the produced powders. The general appearances of AZ91 alloy powders produced had general appearances of ligament, acicular, droplet, flake and spherical shape, but depending on the increase in gas pressure, the shape of the powders is seen to change mostly towards flake and spherical. It is determined that the finest powder was obtained at 820°C with 2 mm nozzle diameter at 3.5 MPa gas pressure and the powders had complex shapes in general.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 4; 1587-1594
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Mechanical Modification of Al-6%Si By Semisolid Process
Autorzy:
Sarajan, Z.
Powiązania:
https://bibliotekanauki.pl/articles/353078.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
mechanical properties
Al-6%Si Alloy
stirring
morphology
semisolid process
Opis:
In this study by semisolid processing of Al-6%Si alloy, it has been found that small additions of Ti-6Al-4V shift the liquidus temperature up and the recalescence decreases. The nucleation event takes place at higher temperatures. Furthermore, the rate at which growth temperature increases is less than that of nucleation temperature and therefore more nuclei form with less potential for growth. In this processing refiner increases the α-Al percentage and reduces globule size. Improvement of mechanical property and microstructure characterization are the main advantages of this study.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 3; 1689-1696
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Mechanical Effects on Different Solid to Liquid Ratio of Geopolymer Filler in Epoxy Resin
Autorzy:
Hashim, Mohammad Firdaus Abu
Ghazali, Che Mohd Ruzaidi
Daud, Yusrina Mat
Faris, Meor Ahmad
Abdullah, Mohd Mustafa Al Bakri
Zainal, Farah Farhana
Hasyim, Saloma
Lokman, Muhammad Taqiyuddin
Powiązania:
https://bibliotekanauki.pl/articles/2048832.pdf
Data publikacji:
2022
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
geopolymer filler
fly ash
tensile
flexural
morphology
solid-liquid ratio
Opis:
Geopolymer is formed from the alkali activation of materials rich in Si and Al content with the addition of a silicate solution to enhance the properties of the materials. This paper presents research on the mechanical properties of fly ash-based geopolymer filler in epoxy resin by varying different solid to liquid ratios using sodium hydroxide and sodium silicate as the alkaline activator. However, the common problem observed from the solid to liquid ratio is the influence of curing time and compressive strength of geopolymer to have the best mechanical property. The mix design for geopolymers of solid to liquid ratio is essential in developing the geopolymer’s mechanical strength. A series of epoxy filled with fly ash-based geopolymer materials with different solid to liquid ratio, which is prepared from 0.5 to 2.5 solid to liquid ratio of alkaline activator. The tensile strength and flexural strength of the epoxy filled with fly ash-based geopolymer materials is determined using Universal Testing Machine under tensile and flexural mode. It was found that the optimum solid to liquid ratio is 2.0, with the optimum tensile and flexural strength value. However, both the tensile and flexural properties of epoxy filled with fly ash-based geopolymer suddenly decrease at a 2.5 solid to liquid ratio. The strength is increasing with the increasing solid to liquid ratio sample of geopolymer filler content.
Źródło:
Archives of Metallurgy and Materials; 2022, 67, 1; 215-220
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Chemically Modified Cellulose Capped Zinc Oxide Nanocomposite: Spectral and Optical Properties
Autorzy:
Jagadeeswari, R.
Selvakumar, P.
Jeevanantham, V.
Saravanan, R.
Powiązania:
https://bibliotekanauki.pl/articles/2049414.pdf
Data publikacji:
2021
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
chemically modified cellulose
hydrothermal
XRD
surface morphology
effective mass approximation
Opis:
In this study, a new chemically modified cellulose polymer-capped ZnO nanopowder prepared by hydrothermal method using chemically modified cellulose polymer as capping agent was successfully reported. The structural characteristics of CMC-capped ZnO nanopowder was reported by FTIR, XRD, SEM and EDX studies. XRD results revealed crystallographic properties like crystal composition, phase purity and crystallite size of the prepared CMC-capped ZnO nanopowder and average size calculated by Debye Scherrer formula as 14.66 nm. EDX studies revealed that the presence of elemental compositions of capping agent in the nanopowder samples. The optical characterization of the CMC-capped ZnO nanopowder was studied using UV absorption (λ max = 303 nm) and PL spectroscopy (λ ex = 295 nm). The average crystal diameter and grain size were calculated by effective mass approximation formula and compared with XRD findings that agreed well and verified CMC capped ZnO with particle size of 193 nm. Thus, the promising optical characteristics shown by the synthesized CMC capped ZnO nanopowders exposes its potential usage in bio-medical fields.
Źródło:
Archives of Metallurgy and Materials; 2021, 66, 3; 911-915
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Fabrication of Multilayer Cu/Ni Systems with Nanometric Layers by Electrolysis Method
Autorzy:
Spilka, M.
Babilas, R.
Ratuszek, W.
Kowalska, J.
Matus, K.
Powiązania:
https://bibliotekanauki.pl/articles/353254.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Cu/Ni multilayer systems
galvanic method
thickness measurement
surface morphology
topography
Opis:
The paper presents research results of multilayer systems composed of alternate Cu/Ni layers. The layers thickness obtained by the galvanic treatment was determined by using the transmission electron microscopy and X-ray diffraction method in the grazing incidence diffraction geometry. The surface morphology was observed using scanning electron microscope with EDS microanalysis. Observation of the surface topography of systems using the atomic force microscope was also carried out.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 4; 2067-2073
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Machinability Studies on the Turning of Magnesium Metal Matrix Composites
Autorzy:
Gobivel, K.
Vijay Sekar, K.S.
Powiązania:
https://bibliotekanauki.pl/articles/2125540.pdf
Data publikacji:
2022
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Mg-SiCp composite
cutting forces
surface quality
chip microstructure
tool morphology
Opis:
Magnesium-based MMCs are widely used in structural-based applications due to their lightweight, high hardness, corrosion and wear resistance. Also, machining is an important manufacturing process that is necessary to ensure dimensional accuracy and produce intricate shapes. In this context, the machining of Magnesium based metal matrix composites is undertaken to study the impact of the cutting parameters on the machinability behaviour. In this work, turning of pure Mg/SiCp on a Lathe is done and an in-depth assessment on the machining forces, machined surface quality, chip microstructure, and tool morphology has been carried out using TiAlN coated tooling insert. The analysis revealed that the thrust force decreased due to the thermal softening of the matrix meanwhile the feed force also followed the similar trend at higher cutting speeds because of the minimized built-up edge and cutting depth whereas principal cutting force was inconsistent at higher cutting speeds. The surface finish was better at high cutting speed - low feed combination. The chip microstructure revealed that gross fracture propagation at the free surface and variations in the shear bands have occurred at different cutting speeds. Tool studies using SEM analysis revealed wear modes like chipping and built-up edge at low cutting speeds, but with a reduced impact at intermediate cutting conditions, whereas abrasion wear was observed predominantly in the tool nose at higher cutting speeds.
Źródło:
Archives of Metallurgy and Materials; 2022, 67, 3; 939--948
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of Copper Powder Morphology on the Microstructure and Properties of Copper Matrix Bulk Composites Reinforced with Ni-doped Graphene
Autorzy:
Liu, Jituo
Wang, Xianhui
Liu, Jia
Li, Hangyu
Liang, Yan
Ren, Jingyi
Powiązania:
https://bibliotekanauki.pl/articles/2048818.pdf
Data publikacji:
2022
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Ni-doped graphene
copper base composite
copper powder morphology
mechanical properties
Opis:
To clarify the effect of copper powder morphology on the microstructure and properties of copper matrix bulk composites reinforced with Ni-doped graphene, spherical and dendritic copper powders were selected to fabricate the Ni-doped graphene reinforced copper matrix bulk composites. The Ni-doped graphene were synthesized by hydrothermal reduction method, followed by mixing with copper powders, and then consolidated by spark plasma sintering. It is found that the Ni-doped graphene are well bonded with the dendritic copper powder, whereas Ni-doped graphene are relatively independent on the spherical copper powder. The copper base bulk composite prepared by the dendritic copper powder has better properties than that prepared by spherical copper powder. At 0.5wt.% Ni-doped graphene, the dendritic copper base bulk composite has a good combination of hardness, electrical conductivity and yield strength, which are 81.62 HV, 87.93% IACS and 164 MPa, respectively.
Źródło:
Archives of Metallurgy and Materials; 2022, 67, 1; 341-348
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Modification of Surface Morphology and Surface Properties of Copper-Nickel Alloy by Anodic Treatment in a Deep Eutectic Solvent (Ethaline)
Autorzy:
Protsenko, V.
Butyrina, Tatyana
Makhota, Dmytro
Korniy, Sergiy
Danilov, Felix
Powiązania:
https://bibliotekanauki.pl/articles/27313867.pdf
Data publikacji:
2023
Wydawca:
Polska Akademia Nauk. Czasopisma i Monografie PAN
Tematy:
copper-nickel alloy
anodic treatment
deep eutectic solvent
surface morphology
hydrogen production
Opis:
A deep eutectic solvent, ethaline (as a typical representative of new-generation room temperature ionic liquids), was used to anodically treat the surface of copper-nickel alloy (55 wt.% Cu). Anodic treatment in ethaline allows flexibly affecting the patterns of surface morphology: formation of stellated crystallites and surface smoothing (i.e. electropolishing) are observed depending on the applied electrode potential. The measured values of roughness coefficient (Ra) well correlate with the changes in surface morphology. Anodic treatment of Cu-Ni alloy in ethaline contributes to a considerable increase in the electrocatalytic activity towards the hydrogen evolution reaction in an alkaline aqueous medium, which can be used to develop new high-efficient and inexpensive electrocatalysts within the framework of the concept of carbon-free hydrogen economy.
Źródło:
Archives of Metallurgy and Materials; 2023, 68, 2; 477--482
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Thermal Fatigue Damage and Residual Mechanical Properties of WCu45/FeCr18Ni9 Steel Brazed Joint with NiCrSiBFe Filler Metal
Autorzy:
Xia, Chunzhi
Fu, Linling
Du, Wenchao
Xu, Xiangping
Wang, Xiling
Zou, Jiasheng
Powiązania:
https://bibliotekanauki.pl/articles/2049429.pdf
Data publikacji:
2021
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Ni-based brazed joint
thermal fatigue damage
residual mechanical properties
fracture morphology
Opis:
Thermal fatigue properties of WCu45/ FeCr18Ni9 steel brazed joint with Ni-Cr-Si-B filler metal were investigated. Results indicated that the fatigue damage of Ni-based joint was aggravated with the increased of thermal fatigue cycles times. Moreover, the fatigue cracks appeared in the brazing seam and FeCr18Ni9 steel side near the brazing seam, and the bending strength of the brazed joint decreased from 333 MPa of original joint to 160 MPa of having experienced 200 thermal fatigue cycles. The fracture characteristic of Ni-based joint underwent 200 cycles was identified as mixed ductile-brittle fracture under the combined effect of external bending load and internal fatigue damage.
Źródło:
Archives of Metallurgy and Materials; 2021, 66, 1; 197-203
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Control of Nd-Fe-B Morphology as Function of the PVP Concentration Using Electrospinning Process
Autorzy:
Eom, Nu Si A.
Haq, Muhammad Aneeq
Lee, Jimin
Lim, Kyoung Mook
Kim, Taek-Soo
Choa, Yong-Ho
Kim, Bum Sung
Powiązania:
https://bibliotekanauki.pl/articles/351180.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Nd2Fe14B
1-D magnet fiber
electrospinning
magnet properties
morphology
Opis:
In this study, we demonstrate a facile and cost-effective way to synthesize Nd-Fe-B of various shapes such as powders, rods and fibers using electrospinning, heat-treatment and washing procedures. Initially Nd-Fe-B fibers were fabricated using electrospinning. The as-spun Nd-Fe-B fibers had diameters ranging 489 to 630 nm depending on the PVP concentration in reaction solutions. The different morphologies of the Nd2Fe14B magnetic materials were related to the difference in thickness of the as-spun fibers. The relationships between the as-spun fiber thickness, the final morphology, and magnetic properties were briefly elucidated. The intrinsic coercivity of Nd2Fe14B changed with the change in morphology from powder (3908 Oe) to fiber (4622 Oe). This work demonstrates the effect of the Nd-Fe-B magnetic properties with morphology and can be extended to the experimental design of other magnetic materials.
Źródło:
Archives of Metallurgy and Materials; 2020, 65, 3; 993-996
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 26

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