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    Wyświetlanie 1-7 z 7
    Tytuł:
    Oxidation Behavior of Steel with Cr Content and Water Flow Rate
    Autorzy:
    Kim, D.-J.
    Kim, K. M.
    Shin, J. H.
    Cheong, Y. M.
    Lee, E. H.
    Lee, G. G.
    Kim, S. W.
    Kim, H. P.
    Choi, M. J.
    Lim, Y. S.
    Hwang, S. S.
    Powiązania:
    https://bibliotekanauki.pl/articles/351548.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    steel
    flow accelerated corrosion
    Cr content
    flow rate
    surface oxides
    Opis:
    Fast water flow facilitates ferrous ion transport leading to flow accelerated corrosion (FAC) of carbon steel and the possibility of a large accident through a failure of a secondary pipe in a nuclear power plant. Ion transport is directly linked to oxide properties such as the thickness, chemical composition and porosity. This work deals with a precise observation of the cross section of the corroded specimen focusing on an oxide passivity and its thickness using SEM (scanning electron microscope) and TEM (transmission electron microscope) as well as an apparent weight loss and a surface observation for the specimens corroded using a rotating cylindrical electrode autoclave system in pure water of pH 7 at 150°C having dissolved oxygen below 1 ppb within a flow rate range of 0 to 10 m/s. The Cr content in steel was changed from 0.02 to 2.4 wt%. Increasing the Cr content in the alloy, the FAC rate and oxide thickness decreased. The oxide porosity tends to decrease with the Cr content and immersion time owing to the development of Cr containing oxide. The oxidation behavior is not changed with the immersion time.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1383-1387
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Study On The Electro-Refining Of Tin In Acid Solution From Electronic Waste
    Badanie elektrorafinacji cyny w roztworze kwasu z e-odpadów
    Autorzy:
    Son, S. H.
    Park, S. C.
    Kim, J. H.
    Kim, Y. H.
    Lee, M. S.
    Ahn, J.-W.
    Powiązania:
    https://bibliotekanauki.pl/articles/352665.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    electrorefining
    tin
    electronic waste
    recycling
    high purity
    elektrorafinacja
    cyna
    odpady elektroniczne
    recykling
    Opis:
    The tin metal could be retractable from wasted tin scrap, sludge, and wasted electroplated solution hydrometallurgical treatment, and purification process. In order to be used as resource of electronic devices, the retracted crude metal should be purified to the extent of higher than 99.9%. In this study, tin electro-refining process was performed to purify the casted tin crude metal at various experimental conditions: at the current density of 3, 5A/dm2, and in various electrolytes such as hydrochloric acid, sulfuric acid and methansulfonic acid. Additional experiment was conducted using Rotating Disk Electrode (RDE) in order to investigate the rate determining step of tin electro-refining process. The current efficiency, 65.6%, was achievable at the condition of current density, 5A/dm2, and in the electrolyte of Hydrochloric acid. During tin electro-refining process, impurity dissolved from tin crude metal into the electrolyte was analyzed using Inductively Coupled Plasma Optical Emission Spectrometer (ICP-OES), and the result showed the concentration of impurity metal gradually increased. Quantitative analysis on casted tin crude metal showed that it consists of tin with 93.9 wt.% and several impurity metals of Ag, Bi, Pb, Cu, and etc. After tin electro-refining process, the purity of tin increased up to 99.985 wt.%.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1217-1220
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Multistep Heat-Treatment Effects on Electrospun Nd-Fe-B-O Nanofibers
    Autorzy:
    Jeon, E. J.
    Eom, N. S. A.
    Lee, J.
    Lee, B.
    Cho, H. M.
    On, J. S.
    Choa, Y.-H
    Kim, B. S.
    Powiązania:
    https://bibliotekanauki.pl/articles/354311.pdf
    Data publikacji:
    2018
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Nd-Fe-B
    nanofibers
    electrospinning
    heat treatment
    Opis:
    Neodymium-Iron-Boron (Nd-Fe-B) magnets are considered to have the highest energy density, and their applications include electric motors, generators, hard disc drives, and MRI. It is well known that a fiber structure with a high aspect ratio and the large specific surface area has the potential to overcome the limitations, such as inhomogeneous structures and the difficulty in alignment of easy axis, associated with such magnets obtained by conventional methods. I n this work, a suitable heat-treatment procedure based on single-step and multistep treatments to synthesize sound electrospun Nd-Fe-B-O nanofibers of Φ572 nm was investigated. The single-step heat-treated (directly heat-treated at 800°C for 2 h in air) samples disintegrated along with the residual organic compounds, whereas the multistep heat-treated (sequential three-step heat-treated including three steps;: dehydration (250°C for 30 min in an inert atmosphere), debinding (650°C for 30 min in air), and calcination (800°C for 1 h in air)) fibers maintained sound fibrous morphology without any organic impurities. They could maintain such fibrous morphologies during the dehydration and debinding steps because of the relatively low internal pressures of water vapor and polymer, respectively. In addition, the NdFeO3 alloying phase was dominant in the multistep heat-treated fibers due to the removal of barriers to mass transfer in the interparticles.
    Źródło:
    Archives of Metallurgy and Materials; 2018, 63, 3; 1433-1437
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Microstructure Evolution of Ni-Based ODS Superalloy Powders During Horizontal Rotary Ball Milling
    Autorzy:
    Lee, H.-E.
    Kim, Y. S.
    Park, J. K.
    Oh, S.-T.
    Powiązania:
    https://bibliotekanauki.pl/articles/355552.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    high energy ball milling
    Ni-base ODS superalloy
    particle and crystalline size
    microstructure
    Opis:
    Microstructure evolution of Ni-based oxide dispersion-strengthened alloy powders with milling time is investigated. The elemental powders having a nominal composition of Ni-15Cr-4.5Al-4W-2.5Ti-2Mo-2Ta-0.15Zr-1.1Y2O3 in wt % were ball-milled by using horizontal rotary ball milling with the change of milling velocity. Microstructure observation revealed that large aggregates were formed in the early stages of ball milling, and further milling to 5 h decreased particle size. The average crystalline size, estimated by the peak broadening of XRD, decreased from 28 nm to 15 nm with increasing milling time from 1 h to 5 h. SEM and EPMA analysis showed that the main elements of Ni and Cr were homogeneously distributed inside the powders after ball milling of 5 h.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1253-1255
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effects Of Environmental Factors On The Dispersion Behavior Of Iron Oxide In Aqueous Solutions With Poly Acrylic Acid
    Wpływ parametrów charakteryzujących wodne roztwory poli(kwasu akrylowego) na dyspersję tlenku żelaza
    Autorzy:
    Lee, E.-H.
    Kim, K.-M.
    Maeng, W.-Y.
    Hur, D.-H.
    Powiązania:
    https://bibliotekanauki.pl/articles/354513.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    polyacrylic acid
    dispersion stability
    magnetite
    nanoparticles
    suspension
    poli(kwas akrylowy)
    stabilność dyspersji
    magnetyt
    nanocząstki
    zawiesina
    Opis:
    After preparing aqueous suspensions from magnetite particles with a poly-acrylic acid, we investigated the effects of several experimental parameters. We characterized the stability of the suspensions using visual inspection, sedimentation, adsorption, and thermal stability of the dispersant. The dispersion stability is affected by the solution pH, the concentrations of magnetite particles, the molecular weight, the concentration of the dispersants, and the temperature. The stability of the suspensions increased as the concentration of the dispersant and the temperature increased. In terms of the molecular weights of the dispersant, the suspensions with dispersant of low-molecular weight (1800) were more stable than those of high-molecular weight (250000) at room temperature. However, at high temperature the suspensions with high-molecular weight showed stability. The adsorption efficiency of the dispersant was very low. The dispersant of high-molecular weight showed a higher thermal integrity than that of low-molecular weight. From this work, we obtained the optimum conditions for stable aqueous suspensions of magnetite particles.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1561-1564
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    A Study On The Metal Carbide Composite Diffusion Bonding For Mechanical Seal
    Badanie łączenia dyfuzyjnego kompozytu metal węglik na mechaniczne uszczelnienie
    Autorzy:
    Kim, D.-K.
    Shon, I.-J.
    Song, J.
    Ryu, W.-J.
    Shin, H.-Ch.
    Kwon, E.-Y.
    Shin, H.
    Kang, S.-J.
    Powiązania:
    https://bibliotekanauki.pl/articles/356399.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    diffusion bonding
    nanostructures
    mechanical seal
    hard metal
    mechanical properties
    łączenie
    nanostruktura
    uszczelnienie mechaniczne
    twardy metal
    właściwości mechaniczne
    Opis:
    Mechanical Seal use highly efficient alternative water having a great quantity of an aqueous solution and has an advantage no corrosion brine. Metal Carbide composites have been investigated as potential materials for high temperature structural applications and for application in the processing industry. The existing Mechanical seal material is a highly expensive carbide alloy, and it is difficult to take a price advantage. Therefore the study of replacing body area with inexpensive steel material excluding O-ring and contact area which demands high characteristics is needed. The development of WC-Ni base carbide alloy optimal bonding composition technique was accomplished in this study. To check out the influence of bonding temperature and time, bonding characteristics of sintering temperature was experimented. The bonding statuses of this test specimen were excellent. The hardness of specimen and bonding rate were measured using ultrasound equipment. In this work, Powder of WC (involved VC, Cr), Co and Mo2C mixed by attrition milling for 24hours. Nanostructured WC-27.6wt.%Ni-1.5wt.%Si-0.11wt.%VC-1.1wt.%B4C composite were fabricated at 1190°C by high temperature vacuum furnace. To check out the influence of bonding temperature and time, bonding characteristics of sintering temperature was experimented. Its relative density was about 99.7%. The mechanical properties (hardness and fracture toughness) were 87.2 HRA and 4.2 M·Pam1/2, respectively. The bonding status of this test specimen was excellent and the thickness of bonding layer was 20 ~30§ at 1050 and 1060°C bonding temperature.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1479-1483
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Correlation Between Superheated Liquid Fragility And Onset Temperature Of Crystallization For Al-Based Amorphous Alloys
    Korelacja między krytycznymi parametrami cieczy i temperaturą początku krystalizacji dla amorficznych stopów na bazie Al
    Autorzy:
    Guo, J.
    Hu, X.
    Liu, J.
    Feng, T.
    Yoon, E. Y.
    Kim, H. S.
    Powiązania:
    https://bibliotekanauki.pl/articles/353707.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    superheated liquid fragility
    onset temperature of crystallization
    thermal stability
    krytyczny parametr cieczy
    temperatura początku krystalizacji
    stabilność termiczna
    Opis:
    Amorphous alloys or metallic glasses have attracted significant interest in the materials science and engineering communities due to their unique physical, mechanical, and chemical properties. The viscous flow of amorphous alloys exhibiting high strain rate sensitivity and homogeneous deformation is considered to be an important characteristic in thermoplastic forming processes performed within the supercooled liquid region because it allows superplastic-like deformation behavior. Here, the correlation between the superheated liquid fragility, and the onset temperature of crystallization for Al-based alloys, is investigated. The activation energy for viscous flow of the liquid is also investigated. There is a negative correlation between the parameter of superheated liquid fragility and the onset temperature of crystallization in the same Al-based alloy system. The activation energy decreases as the onset temperature of crystallization increases. This indicates that the stability of a superheated liquid can affect the thermal stability of the amorphous alloy. It also means that a liquid with a large superheated liquid fragility, when rapidly solidified, forms an amorphous alloy with a low thermal stability.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1543-1546
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-7 z 7

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