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Wyszukujesz frazę "GC-MS analysis" wg kryterium: Temat


Wyświetlanie 1-2 z 2
Tytuł:
FROM HARVESTING TO DISTILLATION – EFFECT OF ANALYTICAL PROCEDURES ON THE YIELD AND CHEMICAL COMPOSITION OF RHODODENDRON TOMENTOSUM (LEDUM PALUSTRE) ESSENTIAL OIL
Autorzy:
Łuczkiewicz, Maria
Jesionek, Anna
Zabiegala, Bozena
Bucinski, Adam
Powiązania:
https://bibliotekanauki.pl/articles/895545.pdf
Data publikacji:
2019-02-28
Wydawca:
Polskie Towarzystwo Farmaceutyczne
Tematy:
drying
GC/MS analysis
Likens-Nickerson apparatus
Clevenger apparatus
Deryng apparatus
distillation
Opis:
Abstract: Rhododendron tomentosum possesses the anti-inflammatory, analgesic and antimicrobial properties, determined by the chemical composition of its essential oil. The effects of place (Miszewko, Lubichowo) and time of harvesting (June, November) as well as drying (air-drying, oven-drying, freeze-drying) and isolation (in Deryng, Clevenger and Likens-Nickerson apparatus) procedures on the yield and quality of R. tomentosum essential oil were studied. Ledol (8.1-14.4%), palustrol (6.9-13.0%) and γ-terpineol (8.5-9.1%) predominated in the plants collected from Miszewko, while γ-terpineol (11.8-22.2%), p-cymene (5.3-12.6%) and geranyl acetate (5.7-7.5%) prevailed in the biomass from Lubichowo. The shoots produced more volatiles in the flowering phase than in the end of the vegetation. Oven-drying at 30ºC with controlled air flow was suggested as the quick dehydration method. Hydrodistillation in Deryng and Clevenger apparatus resulted in comparatively high essential oil yield (about 1%). All studied drying and distillation methods did not influence significantly the general profile of R. tomentosum essential oil.
Źródło:
Acta Poloniae Pharmaceutica - Drug Research; 2019, 76, 1; 83-92
0001-6837
2353-5288
Pojawia się w:
Acta Poloniae Pharmaceutica - Drug Research
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Chemical profile and antibacterial activity of essential oils from leaves and fruits of Gaultheria procumbens L. cultivated in Poland
Autorzy:
Magiera, Anna
Sienkiewicz, Monika
Olszewska, Monika
Kicel, Agnieszka
Michel, Piotr
Powiązania:
https://bibliotekanauki.pl/articles/895472.pdf
Data publikacji:
2019-02-28
Wydawca:
Polskie Towarzystwo Farmaceutyczne
Tematy:
essential oil
antibacterial activity
chemical composition
methyl salicylate
Gaultheria procumbens L
GC-FID/MS analysis
Opis:
Essential oils (EOs) of Gaultheria procumbens were obtained by hydrodistillation with the yield of 1.30% ± 0.05 (v/dw) for leaves and 2.68% ± 0.08 (v/dw) for fruits. The GC-FID/MS analysis led to the identification of 64 volatile components, among which 27 were found in leaf EO, 49 in fruit EO, and 59 analytes were detected for the first time in G. procumbens. Methyl salicylate, which is known as a potent anti-inflammatory agent, was the dominant component making up to 97.5% and 99.8% of the total fruit and leaf EOs, respectively. The remaining volatiles of the leaves included mainly monoterpenes (α-pinene, β-pinene, limonene), methyl-o-anisate, massoilactone, spiro[4,5]decane-1-one, and aliphatic alcohols (heptan-2-ol, octan-1-ol), while the fruit EO contained apart from the dominant aliphatic and aromatic alcohols (benzyl alcohol, heptan-2-ol, p-cymen-7-ol) also carboxylic acids (3-hydroxyphenylacetic acid, heptanoic acid, octanoic acid) and aldehydes (hexanal, furfural, pent-4-enal). The antibacterial activity of the EOs was evaluated using a microdilution broth method against twelve reference strains, as well as clinical and environmental isolates. Differences between activity parameters of both EOs were not statistically significant (p > 0.05) for most tested bacteria. On the other hand, both EOs were significantly more effective against Gram-negative (MIC, 8.2-10.0 mg/mL) than Gram-positive bacteria (MIC, 13.5-16.7 mg/mL). Leaves and especially fruits of G. procumbens cultivated in Poland were proved valuable sources of methyl salicylate-rich EOs of moderate antibacterial activity, which, therefore, could partly explain the traditional use of the plant materials and the EOs in the treatment of bacterial infections-related inflammatory disorders.
Źródło:
Acta Poloniae Pharmaceutica - Drug Research; 2019, 76, 1; 93-102
0001-6837
2353-5288
Pojawia się w:
Acta Poloniae Pharmaceutica - Drug Research
Dostawca treści:
Biblioteka Nauki
Artykuł
    Wyświetlanie 1-2 z 2

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