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Tytuł:
Ionic [Ru] complex with recyclability by electro-adsorption for efficient catalytic transfer hydrogenation of aryl ketones
Autorzy:
Yue, C. J.
Xue, Q. N.
Gu, L. P.
Wang, J. F.
Powiązania:
https://bibliotekanauki.pl/articles/778543.pdf
Data publikacji:
2017
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
ionic Ru complex
transfer hydrogenation
electron-adsorption
catalyst recovery
Opis:
The efficient reuse of homogeneous catalyst is important. Cation complex of [Ru(η6 -p-cymene)(PPh3 )(CH3 CN) Cl]PF6  with different ligands was synthesized and characterized by infrared spectroscopy (IR), 1 H-, 13 C- and 31 P-nuclear magnetic resonance spectroscopy (1 H-, 1 3C- and 31 P-NMR), element analysis (EA), and high resolution mass spectrometry (HR-MS). The complex was used as a catalyst for the hydrogen transfer reduction of carbonyl for the first time, presenting an excellent catalytic performance of 89%–98% conversion of acetophenone and its derivatives. The catalyst may be efficiently reused by the electro-adsorption of 10 times to one catalyst recovery. The cation [Ru] complex presented advantages of both homogeneous and heterogeneous catalysts.
Źródło:
Polish Journal of Chemical Technology; 2017, 19, 4; 75-79
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Laboratory investigation of self-healing properties on geosynthetic clay liners with flaw
Autorzy:
Zhang, G.-W.
Zhang, H.-Y.
Wang, J.-F.
Zhou, L.
Liu, P.
Jiang, X.
Powiązania:
https://bibliotekanauki.pl/articles/204652.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
landfills
geosynthetic clay liner
self healing
hydraulic conductivity
Opis:
The objective of this paper is to evaluate the self- healing properties of a commercially-available geosynthetic clay liner (GCL) using flexible-wall permeameter. The GCLs are produced by the same factory, but the contents of bentonite are different. Also the hydraulic conductivities (HC) of GCLs with no defect are different. In this study, specimens were completely saturated under the backpressure of 20 kPa before the test. Permeability tests were performed on GCL specimens with penet rating flaw and also on specimens permeated with distilled water and CaCl2 solutions. The test results were presented and discussed. Experimental results showed that the GCL with penetrating flaw did not exhibit complete self-healing in the case of flaw. After 120 days, the hydraulic conductivity increased by approximately an order of magnitude. In addition, CaCl2 solutions had a significant influence on the hydraulic conductivity. The research findings might be of interest to researchers and engineers who design liners for landfills and other liquid containment facilities.
Źródło:
Archives of Environmental Protection; 2015, 41, 1; 53-58
2083-4772
2083-4810
Pojawia się w:
Archives of Environmental Protection
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Investigation on different behavior and mechanism of Ca(II) and Fe(III) adsorption on spodumene surface
Autorzy:
Yu, F.
Wang, Y.
Wang, J.
Xie, Z.
Powiązania:
https://bibliotekanauki.pl/articles/110230.pdf
Data publikacji:
2014
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
spodumene surface
calcium ions
iron ions
adsorption mechanism
DFT calculation
Opis:
Behavior and mechanism of Ca2+ and Fe3+ adsorption on spodumene surface were investigated by micro flotation tests, zeta potential measurements, and density functional theory (DFT) calculation methods. The micro flotation tests showed that Ca2+ and Fe3+ activated the flotation of spodumene remarkably. However, the effect of Fe3+ was more significant than that of Ca2+. Additionally, Fe3+ significantly changed the zeta potential of spodumene while Ca2+ showed a little change. Meanwhile, the calculated adsorption energy of Fe3+ on spodumene surface was much greater than that of Ca2+ indicating that Fe3+ is more apt to be adsorbed on spodumene surface than Ca2+. The value of bond population in Ca-O illustrated that the bond of Ca-O consists of partial covalent proportion and some ionic component. On the contrary, the bond of Fe-O showed a relatively strong covalent property. The partial density of states (PDOS) of free Ca/Fe and the reacted O atom on spodumene (110) surface before and after the adsorption showed that Fe 3d orbital and O 2p orbital formed hybridization. The density of states (DOS) near the Fermi level of spodumene surface after adsorption with Fe3+ was much stronger than that with Ca2+.
Źródło:
Physicochemical Problems of Mineral Processing; 2014, 50, 2; 535-550
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Numerical analysis of controlling separation in axial cascades by excitation of periodical incoming wake
Autorzy:
Liu, F.
Wang, J.
Wu, K.
Powiązania:
https://bibliotekanauki.pl/articles/1933188.pdf
Data publikacji:
2008
Wydawca:
Politechnika Gdańska
Tematy:
unsteady excitation
compressor cascade
separation control
incoming wake
vortex shedding
Opis:
Numerical analysis has been performed of time-space structures in a large turning angle axial cascade subject to unsteady incoming wake excitation. The results have shown that intentional unsteady excitation could increase the cascade's time-averaged performance. As a result, the vortex structures corresponding to the external exciting frequency are strengthened and other disordered vortices are involved, so that the separation structures of the suction surface are translated from disorder to order. Two interaction regimes between incoming periodic wakes and separation structures are analyzed, indicating that turbulent kinetic energy can enhance momentum interchange and that wave-vortex resonance can promote rolled-up and plus-minus pairing of vortices. Based .on these, responses of separation structures from two periodic incoming wake regimes are compared. The feasibility of far-field noise reduction in ducting fans by using periodic incoming wake is considered.
Źródło:
TASK Quarterly. Scientific Bulletin of Academic Computer Centre in Gdansk; 2008, 12, 1-2; 21-34
1428-6394
Pojawia się w:
TASK Quarterly. Scientific Bulletin of Academic Computer Centre in Gdansk
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
A Visual Detection Method of Longitudinal Crack Based on Computer Image Processing During Slab Continuous Casting
Autorzy:
Liu, Y.
Wang, X.
Sun, Y.
Du, F.
Gao, Y.
Wang, F.
Wang, J.
Powiązania:
https://bibliotekanauki.pl/articles/351636.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
longitudinal crack
visual detection
image processing
continuous casting
Opis:
Based on the mould temperature measured by thermocouples during slab continuous casting, a difference of temperature thermograph is developed to detect slab cracks. In order to detect abnormal temperature region caused by longitudinal crack, the suspicious regions are extracted and divided by virtue of computer image processing algorithms, such as threshold segmentation, connected region judgement and boundary tracing. The abnormal regions are then determined and labeled with the eight connected component labeling algorithm. The boundary of abnormal region is also extracted to depict characteristics of longitudinal crack. Based on above researches, longitudinal crack with abnormal temperature region can be detected and is different from other abnormalities. Four samples of temperature drop are picked up to compare with longitudinal crack on the abnormal region formation, length, width, shape, et al. The results show that the abnormal region caused by longitudinal crack has a linear and vertical shape. The height of abnormal region is more than the width obviously. The ratio of height to width is usually larger than that of other temperature drop regions. This method provides a visual and easy way to detect longitudinal crack and other abnormities. Meanwhile it has a positive meaning to the intelligent and visual mould monitoring system of continuous casting.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 2; 673-680
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Trophic connectivity between intertidal and offshore food webs in Mirs Bay, China
Autorzy:
Ning, J.
Du, F.
Wang, X.
Wang, L.
Li, Y.
Powiązania:
https://bibliotekanauki.pl/articles/47613.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Instytut Oceanologii PAN
Tematy:
intertidal zonation
offshore zone
food web
different habitat
trophic interaction
stable isotope
carbon isotope composition
Mirs Bay
China
Źródło:
Oceanologia; 2019, 61, 2
0078-3234
Pojawia się w:
Oceanologia
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Distribution and role of the genus Oithona (Copepoda: Cyclopoida) in the South China Sea
Autorzy:
Wang, L.
Du, F.
Wang, X.
Li, Y.
Ning, J.
Powiązania:
https://bibliotekanauki.pl/articles/47786.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Instytut Oceanologii PAN
Tematy:
Oithona
Copepoda
Cyclopoida
temperature
hydrological factor
phytoplankton
ichthyoplankton
South China Sea
Oithona plumifera
Oithona similis
Opis:
The relationships between the small cyclopoid copepod Oithona and hydrological factors, phytoplankton and ichthyoplankton were evaluated using the data obtained in the central South China Sea (SCS) in summer 2014. The genus abundance ranged from 6.00 ind. m3 to 93.75 ind. m3 with high abundance band occurring in the branch of SCS Monsoon Jet. The lower temperature and higher salinity in the surface water of the band than other zones indicated that deep water intrusion was a positive factor for aggregation of the genus. The community structure of the genus was dominated by Oithona plumifera and Oithona similis made up 97% of the genus abundance associated with Oithona tenuis. The result of db-RDA analysis showed that the community structure of the genus was affected by temperature, Chl a, larval fishes and fish spawns, and temperature was the most important limiting factor. The result of GAMs analysis showed that abundance of O. tenuis, and copepodites were affected by Chl a, larval fishes and fish spawns; abundance of O. similis was affected by Chl a and fish spawns; and abundance of O. plumifera was affected by Chl a and larval fishes. Therefore, we suggest that the branch of SCS Monsoon Jet and deep water intrusion favor aggregation of plankton in the central SCS in summer. We confirm that the temperature is the limiting factor to the reproduction of the genus Oithona in tropic seas and the genus Oithona is a food-web linker between primary production and larval fishes in the central SCS.
Źródło:
Oceanologia; 2017, 59, 3
0078-3234
Pojawia się w:
Oceanologia
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Dual reference beam digital off-axis holography for exact suppression of zero-order term and twin image without spectrum loss
Autorzy:
Wang, M.
Wang, K.
Zheng, M.
Li, F.
Wu, J.
Powiązania:
https://bibliotekanauki.pl/articles/174894.pdf
Data publikacji:
2017
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
noise suppression
pixel-by-pixel multiplication
digital off-axis holography
Opis:
In this paper, we describe an effective approach to suppressing zero-order term and twin image by using pixel-by-pixel multiplication of double holograms in digital off-axis holography. This method records two holograms, respectively, by using the reference waves in different directions. It shows not only a simpler algorithm and easier implementation in experiment, but also exact and complete suppression of the zero-order term and twin image without any spectrum loss of the object in the image reconstruction, particularly when the image and the zero-order term are fairly close to each other. The experimental result approves of the theoretical prediction very well. This approach provides an effective solution to suppressing undesired noises in the digital off-axis holography.
Źródło:
Optica Applicata; 2017, 47, 3; 435-443
0078-5466
1899-7015
Pojawia się w:
Optica Applicata
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Morphology and developmental traits of the trilobite Changaspis elongata from the Cambrian Series 2 of Guizhou, South China
Autorzy:
Du, G.-Y.
Peng, J.
Wang, D.-Z.
Wang, Q.-J.
Wang, Y.-F.
Zhang, H.
Powiązania:
https://bibliotekanauki.pl/articles/22906.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Instytut Paleobiologii PAN
Opis:
The morphology and ontogeny of the trilobite Changaspis elongata based on 216 specimens collected from the Lazizhai section of the Balang Formation (Stage 4, Series 2 of the Cambrian) in Guizhou Province, South China are described. The relatively continuous ontogenetic series reveals morphological changes, and shows that the species has seventeen thoracic segments in the holaspid period, instead of the sixteen as previously suggested. The development of the pygidial segments shows that their number gradually decreases during ontogeny. A new dataset of well-preserved specimens offers a unique opportunity to investigate developmental traits after segment addition is completed. The ontogenetic size progressions for the lengths of cephalon and trunk show overall compliance with Dyar’s rule. As a result of different average growth rates for the lengths of cephalon, trunk and pygidium, the length of the thorax relative to the body shows a gradually increasing trend; however, the cephalon and pygidium follow the opposite trend. Morphometric analysis across fourteen post-embryonic stages reveals growth gradients with increasing values for each thoracic segment from anterior to posterior. The reconstruction of the development traits shows visualization of the changes in relative growth and segmentation for the different body parts. The new dataset and growth gradient of the trunk suggest that the thoracic segment growth dynamics of early Cambrian to Silurian trilobites follow the same general continuous, steady-state growth gradient decreasing from posterior to anterior.
Źródło:
Acta Palaeontologica Polonica; 2019, 64, 4
0567-7920
Pojawia się w:
Acta Palaeontologica Polonica
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Evaluation of Adjustable Thermal Insulations of Tibetan Clothing by Manikin Testing
Ocena możliwości zmian izolacji cieplnej ubiorów tybetańskich przy wykorzystaniu manekina
Autorzy:
Guo, X F
Wang, Y Y
Li, J
Powiązania:
https://bibliotekanauki.pl/articles/232266.pdf
Data publikacji:
2013
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Biopolimerów i Włókien Chemicznych
Tematy:
Tibetan clothing
style
thermal insulation
clothing area factor
thermal manikin
ubiór tybetański
styl
izolacja cieplna
przewodzenie ciepła
manekin termiczny
Opis:
The thermal insulation of clothing needs to be easily adjusted in an unsteady environment, but this is extremely difficult for most clothing. To reveal the effect of different styles of Tibetan clothing on their thermal property, the total thermal insulations of Tibetan clothing in three typical styles were measured using a thermal manikin. The clothing area factors (fcl) of the Tibetan clothing and body surface area covered by a Tibetan robe were tested with a photographic method. The results showed the following: 1) For similar insulation, fcl of Tibetan clothing is about 0.23 bigger than that of western clothing, estimated from ISO 11079; 2)the style of Tibetan clothing significantly affects the fcl (p < 0.05, fcl = 1.229 + 0.007 BSAC) and the intrinsic thermal insulation (p < 0.05, Icl = 0.166 + 0.016 BSAC); 3)the adjustable thermal insulation of Tibetan clothing proved its adaptability to the large air temperature difference environment on the Tibetan plateau ,which should be valuable for the product development of clothing used in a unsteady environment.
Odzież powinna umożliwiać zmianę jej przewodności cieplnej w niestabilnym środowisku, jednak dla większości odzieży jest to niezwykle trudne. W celu określenia wpływu różnych stylów ubiorów tybetańskich na ich właściwości termiczne określono całkowitą izolację termiczna dla trzech typowych stylów odzieży tybetańskiej przy zastosowaniu manekina termicznego. Wpływ konfiguracji ubioru sprawdzono metodą fotograficzną za pomocą termowizji, określając jednocześnie powierzchniowy współczynnik okrycia ciała fcl. Wykazano, że 1) przy podobnej izolacji fcl ubiorów tybetańskich jest o 0.23 większy od ubiorów zachodnich (ISO11079); 2) styl ubiorów tybetańskich znacząco wpływa na fcl jak i wewnętrzną izolacje cieplną; 3) możliwość regulacji izolacji termicznej tybetańskiego ubioru zapewnia zdolność przystosowania się do dużych różnic temperatury otoczenia na płaskowyżu tybetańskim. Wyniki badań mogą znaleźć zastosowanie w projektowaniu odzieży noszonej w niestabilnym środowisku.
Źródło:
Fibres & Textiles in Eastern Europe; 2013, 1 (97); 87-91
1230-3666
2300-7354
Pojawia się w:
Fibres & Textiles in Eastern Europe
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Identification of sonar detection signal based on fractional Fourier transform
Autorzy:
Wang, B.
Tang, J.
Yu, F.
Zhu, Z.
Powiązania:
https://bibliotekanauki.pl/articles/259724.pdf
Data publikacji:
2018
Wydawca:
Politechnika Gdańska. Wydział Inżynierii Mechanicznej i Okrętownictwa
Tematy:
fractional Fourier transform
watermark
sonar
Opis:
Aiming at the source of underwater acoustic emission, in order to identify the enemy emission sonar source accurately. Using the digital watermarking technology and combining with the good time-frequency characteristics of fractional Fourier transform (FRFT),this paper proposes a sonar watermarking method based on fractional Fourier transform. The digital watermark embedding in the fractional Fourier transform domain and combined with the coefficient properties of the sonar signal in the fractional Fourier transform to select the appropriate watermark position. Using the different characteristics of the signals before and after embedding, an adaptive threshold was set for the watermark detection to realize the discrimination of sonar signals. The simulation results show the feasibility and has better resolution and large watermark capacity of this method, while the robustness of the watermark is better, and the detection precision is further improved.
Źródło:
Polish Maritime Research; 2018, S 2; 125-131
1233-2585
Pojawia się w:
Polish Maritime Research
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
A polarization filter at 1550 nm based on photonic crystal fiber with symmetry around gold-coated holes
Autorzy:
Zha, F.
Li, J.
Sun, P.
Wang, X.
Powiązania:
https://bibliotekanauki.pl/articles/173897.pdf
Data publikacji:
2018
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
photonic crystal fiber
polarization filter
finite element method
surface plasmon resonance
Opis:
A polarization photonic crystal fiber based on surface plasmon resonance is proposed in this paper. The photonic crystal fiber with gold coated holes is studied through using the finite element method. The impacts of structural parameters on the resonance characteristics are discussed. Numerical simulations show that the resonance wavelength can be modulated by changing the parameters of the air holes and thickness of gold layer. At the resonance wavelength 1550 nm, the loss is 3.8045 dB/m in x-polarization and the loss is 28464 dB/m in y-polarization by adjusting the size of the gold-coated holes and the place of air holes. Results show that the loss of y-polarized mode is much larger than the loss of x-polarized mode. The y-polarized mode is suppressed, and only x-polarized mode can be guided at the resonance wavelength of y-polarized mode. The results indicate that the mode polarized in one direction can be filtered out selectively by adjusting the diameter of air holes, and the filtering effect in a communication band is achieved.
Źródło:
Optica Applicata; 2018, 48, 4; 609-620
0078-5466
1899-7015
Pojawia się w:
Optica Applicata
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
New specimens of the multituberculate mammal Sphenopsalis from China: Implications for phylogeny and biology of taeniolabidoids
Autorzy:
Mao, F.-Y.
Wang, Y.-Q.
Meng, J.
Powiązania:
https://bibliotekanauki.pl/articles/20957.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Instytut Paleobiologii PAN
Tematy:
new specimen
multituberculate mammal
mammal
Sphenopsalis
China
phylogenesis
biology
taeniolabidoid
Mammalia
Multituberculata
Taeniolabidoidea
Paleogene
Erlian Basin
Inner Mongolia
Opis:
Multituberculates are the most diverse and best known group of Mesozoic mammals; they also persisted into the Paleogene and became extinct in the Eocene, possibly outcompeted by rodents that have similar morphological and presumably ecological adaptations. Among the Paleogene multituberculates, those that have the largest body sizes belong to taeniolabidoids, which contain several derived species from North America and Asia and some species with uncertain taxonomic positions. Of the known taeniolabidoids, the poorest known taxon is Sphenopsalis nobilis from Mongolia and Inner Mongolia, China, represented previously by a few isolated teeth. Its relationship with other multituberculates thus has remained unclear. Here we report new specimens of Sphenopsalis nobilis collected from the upper Paleocene of the Erlian Basin, Inner Mongolia, China, during a multi-year field effort beginning in 2000. These new specimens document substantial parts of the dental, partial cranial and postcranial morphologies of Sphenopsalis, including the upper and lower incisors, partial premolars, complete upper and lower molars, a partial rostrum, fragments of the skull roof, middle ear cavity, a partial scapula, and partial limb bones. With the new specimens we are able to present a detailed description of Sphenopsalis, comparisons among relevant taeniolabidoids, and brief phylogenetic analyses based on a dataset consisting of 43 taxa and 102 characters. In light of the new evidence, we assess the phylogenetic position of Sphenopsalis and re-establish the family Lambdopsalidae. The monophyly of Taeniolabidoidea is supported in all our phylogenetic analyses. Within Taeniolabidoidea the Asian lambdopsalids and the North American taeniolabidids represent two significantly different trends of adaptations, one characterized by shearing (lambdopsalids) and the other by crushing and grinding (taeniolabidids) in mastication, which supports their wider systematic separation, as speculated when Sphenopsalis was named.
Źródło:
Acta Palaeontologica Polonica; 2016, 61, 2
0567-7920
Pojawia się w:
Acta Palaeontologica Polonica
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Accelerated storage degradation testing and failure mechanisms of aerospace electromagnetic relay
Badania przyspieszone degradacji w czasie składowania przekaźników elektromagnetycznych stosowanych w przemyśle lotniczym oraz mechanizmów ich uszkodzeń
Autorzy:
Wang, Z. B.
Shang, S.
Wang, J.-W.
Huang, Z.-L.
Sai, F.
Powiązania:
https://bibliotekanauki.pl/articles/302000.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Polskie Naukowo-Techniczne Towarzystwo Eksploatacyjne PAN
Tematy:
electrical contact
electromagnetic relay
failure mechanisms
storage reliability
degradation testing
Styk elektryczny
przekaźnik elektromagnetyczny
mechanizmy uszkodzeń
niezawodność składowania
badania degradacji
Opis:
It is difficult to obtain the failure data of high-reliability and long-lifetime aerospace electromagnetic relay (EMR), even if based on the traditional accelerated storage life testing method. Based on the reliability test technique, the scheme of accelerated degradation testing for aerospace EMR was designed. The test system of aerospace electromagnetic relay storage parameters under temperature-accelerated stress was designed and developed. The most past research on storage reliability of relay only focuses on the measurement of contact resistance. The relay time parameters (pick-up time, opening time, overtravel time, rebound duration time, etc.) which reflect main performance function were not monitored. So, in this study the relay time parameters and relay contact resistance were detected simultaneously. According to the analysis on experiment results of contact resistance, relay time parameters, the degradation phenomena of aerospace EMR in long-term storage are investigated, which provides the bases for determining degradation sensitive parameters. Finally, based on the structure and function of aerospace EMR, the storage failure mechanism is investigated by conductive properties themselves. The microscopic morphology and changes in chemical elements for relay contact surface was analyzed by SEM and EDX regularly, which provide references for the relay storage failure mechanism.
Ze względu na wysoką niezawodność i długi cykl życia przekaźników elektromagnetycznych stosowanych w przemyśle lotniczym (EMR), trudno jest uzyskać dane o ich uszkodzeniach, nawet gdy korzysta się z tradycyjnej metody przyspieszonych badań dopuszczalnego okresu składowania. W przedstawionym artykule, opracowano, w oparciu o technikę badania niezawodności, schemat przyspieszonego badania degradacji przekaźników elektromagnetycznych stosowanych w lotnictwie. Zaprojektowano i zpracowano system oceny parametrów składowania przekaźników elektromagnetycznych używanych w lotnictwie w warunkach przyspieszonych przy skrajnych temperaturach. Ostatnie badania nad niezawodnością składowania przekaźników koncentrują się wyłącznie na pomiarze rezystancji styku. Nie były w nich monitorowane parametry czasowe przekaźnika (czas załączania, czas otwarcia, czas opóźnienia, czas trwania odbicia itp.), które odzwierciedlają jego główne funkcje. W przedstawionych badaniach mierzono jednocześnie parametry czasowe przekaźników i rezystancję styków. W oparciu o analizę uzyskanych wyników doświadczeń, badano zjawiska degradacji EMR podczas ich długoterminowego składowania, co stanowiło podstawę do wyznaczenia parametrów wrażliwych na degradację. Wreszcie, w oparciu o strukturę i funkcje EMR, badano mechanizm powstawania uszkodzeń podczas ich składowania na podstawie właściwości przewodzących. Prowadzone regularnie metodami SEM i EDX analizy budowy mikroskopowej oraz przemian pierwiastków chemicznych zachodzących na powierzchni styków przekaźnika stanowią odniesienie dla badań mechanizmu powstawania uszkodzeń podczas składowania przekaźników.
Źródło:
Eksploatacja i Niezawodność; 2017, 19, 4; 530-541
1507-2711
Pojawia się w:
Eksploatacja i Niezawodność
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Oxidation of a lignin model compound of benzyl-ether type linkage in water with H2O2 under an oxygen atmosphere catalyzed by Co(Salen)
Utlenianie modelowego związku ligniny z typem wiązania benzylowo-eterowego w wodzie z H2O2 w atmosferze tlenu katalizowane Co(Salen)
Autorzy:
Zhou, X.F.
Qin, J.X.
Wang, S.R.
Powiązania:
https://bibliotekanauki.pl/articles/52363.pdf
Data publikacji:
2011
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Technologii Drewna
Tematy:
oxidation
lignin model compound
benzyl-ether type
linkage
water
oxygen atmosphere
cobalt salen complex
catalytic property
analytical technique
veratrylglycerol-beta-guaiacyl-alpha,gamma-dimethylether
Opis:
The catalytic properties of Cobalt salen? complex in the oxidation of a lignin model compound [veratrylglycerol-β-guaiacyl-α,γ-dimethylether, VGD] have been investigated in order to obtain the mechanistic aspects of the reaction between Co(salen) and VGD under an oxygen atmosphere using hydrogen peroxide as an oxidant. VGD was found to undergo structural changes in response to the catalytic reaction as characterised by different analytical techniques (FT-IR, H-1 NMR and GC-MS), yielding 2-methoxy phenol and biphenyl. A mechanism for the oxidation of VGD was postulated.
Zbadano katalityczne właściwości kompleksu Co(Salen) w utlenianiu modelowego związku ligniny (veratrylglycerol-β-guaiacyl-α,γ-dimetyleter, VGD) w celu określenia mechanicznych aspektów reakcji pomiędzy Co(salen) i VGD w atmosferze tlenu przy zastosowaniu nadtlenku wodoru jako utleniacza. Zaobserwowano, że w VGD zaszły zmiany strukturalne w odpowiedzi na reakcję katalityczną, co przedstawiono za pomocą różnych technik analitycznych (FTIR, H-1 NMR oraz GC-MS). W efekcie otrzymano 2-metoksy fenol i bifenyl.
Źródło:
Drewno. Prace Naukowe. Doniesienia. Komunikaty; 2011, 54, 186
1644-3985
Pojawia się w:
Drewno. Prace Naukowe. Doniesienia. Komunikaty
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 45

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