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    Wyświetlanie 1-8 z 8
    Tytuł:
    Microstructure and Mechanical Properties of Hot-deformed AlMg4 Alloys with the Variations of Mn, Fe, and Si Contents
    Autorzy:
    Lee, Da B.
    Kim, Bong H.
    Choi, Kweon H.
    Yang, Seung Y.
    Kim, Nam S.
    Ha, Seong H.
    Yoon, Young O.
    Lim, Hyun K.
    Kim, Shae
    Hyun, Soong K..
    Powiązania:
    https://bibliotekanauki.pl/articles/351603.pdf
    Data publikacji:
    2020
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Al-Mg alloy
    intermetallic compounds
    homogenization
    hot-rolling
    microstructure
    Opis:
    This paper aims to investigate the microstructural evolution and mechanical properties of hot-deformed AlMg4 alloys with Mn, Fe, and Si as the main impurities. For this purpose, solidification behavior and microstructural evolution during hot-rolling and heat-treatment processes are investigated by using theoretical calculations and experimental characterization. The crystallization and morphological transformation of intermetallic Al3 Fe, Al6 Mn, and Mg2 Si phases are revealed and discussed in terms of the variation in chemical composition. Following a homogenization heat-treatment, the effect of heat treatment on the intermetallic compounds is also investigated after hot-rolling. It was revealed that the Mg2 Si phase can be broken into small particles and spherodized more easily than the Al3 Fe intermetallic phase during the hot-rolling process. For the Mn containing alloys, both yield and ultimate tensile strength of the hot-rolled alloys increased from 270 to 296 MPa while elongation decreased from 17 to 13%, which can be attributed to Mn-containing intermetallic as well as dispersoid.
    Źródło:
    Archives of Metallurgy and Materials; 2020, 65, 4; 1255-1259
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Warm Tensile Deformation Behavior and Constitutive Equation of Supersaturated Solid-Solutionized Al-9Mg Extruded Alloy
    Autorzy:
    Yang, Seung Y.
    Kim, Bong H.
    Lee, Da B.
    Choi, Kweon H.
    Kim, Nam S.
    Ha, Seong H.
    Yoon, Young O.
    Lim, Hyun K.
    Kim, Shae
    Kim, Young J.
    Powiązania:
    https://bibliotekanauki.pl/articles/2048882.pdf
    Data publikacji:
    2021
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    aluminum alloy
    Al-9Mg alloy
    tensile test
    constitutive equation
    Opis:
    In this paper, as a purpose to apply the supersaturated solid-solutionized Al-9Mg alloy to the structural sheet parts of automotive, tensile tests were conducted under the various conditions and a constitutive equation was derived from the tensile test results. Al-9Mg alloy was produced using a special Mg master alloy containing Al2Ca during the casting process and extruded into the sheet. In order to study the deformation behavior of Al-9Mg alloy in warm temperature forming environments, tensile tests were conducted under the temperature of 373 K-573 K and the strain rate of 0.001/s~0.1/s. in addition, by using the raw data obtained from tensile tests, a constitutive equation of the Al-9Mg alloy was derived for predicting the optimized condition of the hot stamping process. Al-9Mg alloy showed uncommon deformation behavior at the 373 K and 473 K temperature conditions. The calculated curves from the constitutive equation well-matched with the measured curves from the experiments particularly under the low temperature and high strain rate conditions.
    Źródło:
    Archives of Metallurgy and Materials; 2021, 66, 4; 1013-1018
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Characterization of Ca Precipitation in Al-Mg Alloys Containing a Trace of Ca During Homogenization
    Autorzy:
    Ha, Seong-Ho
    Shin, Young-Chul
    Kim, Bong-Hwan
    Yoon, Young-Ok
    Lim, Hyun-Kyu
    Lim, Sung-Hwan
    Kim, Shae K.
    Powiązania:
    https://bibliotekanauki.pl/articles/2049165.pdf
    Data publikacji:
    2021
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Al-Mg system
    precipitation
    Mg+Al2Ca mater alloy
    transmission electron microscope
    phase diagram
    Opis:
    In this study, precipitation of Ca in Al-Mg alloys containing a trace of Ca during homogenization was investigated using a transmission electron microscope (TEM) and calculated phase diagrams. TEM result indicated that the Ca-based particles found in the examined sample are Ca7Mg7.5Si14. From the calculation of Scheil-Gulliver cooling, it was found that the Ca was formed as Al4Ca and C36 laves phases with Mg2Si and Al13Fe4 from other impurities phase during solidification. No Ca-Mg-Si ternary phase existed at the homogenization temperature in the calculated phase diagram. From the phase diagram of Al-Al4Ca-Mg2Si three-phase isothermal at 490°C, it was shown that Ca7Mg6Si14 phase co-exists with Al, Mg2Si and Al4Ca in the largest region and with only Al and Mg2Si in Al4Ca-poor regions. It was thought that the Ca7Mg6Si14 ternary phase was formed by the interaction between Mg2Si and Al4Ca considering that the segregation can occur throughout the entire microstructures.
    Źródło:
    Archives of Metallurgy and Materials; 2021, 66, 4; 959-962
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effect of Cu Addition on Oxide Growth of Al-7 mass%Mg Alloy at High Temperature
    Autorzy:
    Ha, Seong-Ho
    Shah, Abdul Wahid
    Kim, Bong-Hwan
    Yoon, Young-Ok
    Lim, Hyun-Kyu
    Kim, Shae K.
    Powiązania:
    https://bibliotekanauki.pl/articles/2049221.pdf
    Data publikacji:
    2021
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Al-Mg system
    Cu addition
    oxidation
    phase diagram
    Opis:
    Effect of Cu addition on oxide growth of Al-7 mass%Mg alloy at high temperature was investigated. As-cast microstructures of Al-7 mass%Mg and Al-7 mass%Mg-1 mass%Cu alloys showed α-Al dendrites and area of secondary particles. The 1 mass%Cu addition into Al-7 mass%Mg alloy formed Mg32(Al, Cu)49 ternary phase with β-Al3Mg2. The total fraction of two Mg-containing phases in Cu-added alloy was higher than the β-Al3Mg2 fraction in Cu-free alloy. From measured weight gains depending on time at 500°C under an air atmosphere, it was shown that all samples exhibited significant weight gains depending on time. Al-7mass%Mg1mass%Cu alloy showed the relatively increased oxidation rate when compared with Cu-free alloy. All the oxidized cross-sections throughout the entire oxidation time showed coarse and dark areas regarded as oxides grown from the surface to inside, but bigger oxidized areas were formed in the Al-7mass%Mg-1mass%Cu alloy containing higher fraction of Mg-based phases in the as-cast microstructure. As a result of compositional analysis on the oxide clusters, it was found that the oxide clusters contained Mg-based oxides formed through internal oxidation during a long time exposure to oxidizing environments.
    Źródło:
    Archives of Metallurgy and Materials; 2021, 66, 3; 699-702
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Influence of Si Addition on Oxide Growth of Al-6 mass%Mg Alloy Melts
    Autorzy:
    Yoon, Young-Ok
    Ha, Seong-Ho
    Shah, Abdul Wahid
    Kim, Bong-Hwan
    Lim, Hyun-Kyu
    Kim, Shae K.
    Powiązania:
    https://bibliotekanauki.pl/articles/2049203.pdf
    Data publikacji:
    2021
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Al-Mg system
    Si addition
    oxidation
    phase diagram
    Opis:
    Influence of Si addition on oxide layer growth of Al-6 mass%Mg alloys in molten state was investigated in this study. After melt holding for 24 h, the melt surface of only Si-free alloy became significantly bumpy, while no considerably oxidized surface was observed even with 1 mass%Si addition. There was no visible change on the appearance of melt surfaces with increasing Si content. As a result of compositional analysis on the melt samples between before and after melt holding, the Si-added alloys nearly maintained their Mg contents even after the melt holding for 24 h. On the other hand, the Mg content in the Si-free alloy showed a great reduction. The bumpy surface on Si-free alloy melt showed a large amount of pores and oxide clusters in its cross-section, while the Si-added alloy had no significantly grown oxide clusters on the surfaces. As a result of compositional analysis on the surfaces, the oxide clusters in Si-free alloy contained a great amount of Mg and oxygen. The oxide layer on the Si-added alloy was divided into Mg-rich and Mg-poor areas and contained certain amounts of Si. Such a mixed oxide layer containing Si would act as a protective layer during the melt holding for a long duration.
    Źródło:
    Archives of Metallurgy and Materials; 2021, 66, 3; 695-698
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Microstructure Formation of Al-5 mass%Mg Alloy Melts by Interaction with Silica
    Autorzy:
    Kim, Sun-Ki
    Ha, Seong-Ho
    Kim, Bong-Hwan
    Yoon, Young-Ok
    Lim, Hyun-Kyu
    Kim, Shae K.
    Kim, Yong-Jig
    Powiązania:
    https://bibliotekanauki.pl/articles/2049152.pdf
    Data publikacji:
    2021
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Al-Mg system
    silica
    reduction
    Mg2Si
    phase diagram
    Opis:
    Dissolution of Si in Al-5 mass%Mg alloy melt by the reduction of SiO2 and its effect on microstructure formation of the alloy after solidification were investigated. Al-5 mass%Mg alloy without silica powder had approximately 0.05 mass%Si as an impurity. No significant difference in Si content was observed after the reaction with silica for 10 min, while the Si content increased up to about 0.12 mass% after 30 min. From the microstructure analysis and calculation of Scheil-Gulliver cooling, it was considered that as-cast microstructures of Al-5 mass%Mg-1 mass% SiO2 alloys had the distribution of eutectic phase particles, which are comprised of β-Al3Mg2 and Mg2Si phases. Based on the phase diagrams, only limited amount of Mg can be selectively removed by silica depending on the ratio of Si and Mg. Addition of silica of more than approximately 1.5 mass% in Al-5 mass%Mg alloy led to the formation of spinel and removal of both mg and Al from the melt.
    Źródło:
    Archives of Metallurgy and Materials; 2021, 66, 4; 947-950
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Fabrication of a Spherical Titanium Powder by Combined Combustion Synthesis and DC Plasma Treatment
    Autorzy:
    Choi, S. H.
    Ali, B.
    Hyun, S. K.
    Sim, J. J.
    Choi, W. J.
    Joo, W.
    Lim, J. H.
    Lee, Y. J.
    Kim, T. S.
    Park, K. T.
    Powiązania:
    https://bibliotekanauki.pl/articles/356067.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    combustion synthesis
    DC plasma treatment
    titanium powder
    3D printing process
    combustion parameters
    Opis:
    Combustion synthesis is capable of producing many types of refractory and ceramic materials, as well as metals, with a relatively lower cost and shorter time frame than other solid state synthetic techniques. TiO2 with Mg as reductant were dry mixed and hand compacted into a 60 mm diameter mold and then combusted under an Ar atmosphere. Depending on the reaction parameters (Mg concentration 2 ≤ α ≤ 4), the thermocouples registered temperatures between 1160°C and 1710°C . 3 mol of Mg gave the optimum results with combustion temperature (Tc) and combustion velocity (Uc) values of 1372°C and 0.26 cm/s respectively. Furthermore, this ratio also had the lowest oxygen concentration in this study (0.8 wt%). After combustion, DC plasma treatment was carried out to spheroidize the Ti powder for use in 3D printing. The characterization of the final product was performed using X-ray diffraction, scanning electron microscopy, energy dispersive spectroscopy, and N/O analysis.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1057-1062
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Reaction Kinetics and Morphological Study of TiNb2O7 Synthesized by Solid-State Reaction
    Autorzy:
    Choi, S. H.
    Ali, B.
    Choi, K. S.
    Hyun, S. K.
    Sim, J. J.
    Choi, W. J.
    Joo, W.
    Lim, J. H.
    Lee, T. H.
    Kim, T. S.
    Park, K. T.
    Powiązania:
    https://bibliotekanauki.pl/articles/355326.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    solid state reaction
    kinetic analysis
    quantitative phase analysis
    TiNb2O7 synthesis
    Opis:
    Although TiNb2O7 is regarded as a material with high application potential in lithium-ion batteries (LIBs) and solid-oxide fuel cells (SOFCs), it has been difficult to find suitable cost-effective conditions for synthesizing it on a commercial scale. In this study, TiNb2O7 compounds were synthesized by a solid state synthesis process. For stoichiometrically precise synthesis of the TiNb2O7 phase, the starting materials, TiO2 and Nb2O5 were taken in a 1:1 molar ratio. Activation energy and reaction kinetics of the system were investigated at various synthesis temperatures (800,1000,1200, and 1400°C) and for various holding durations (1,5,10, and 20 h). Furthermore, change in the product morphology and particle size distribution were also evaluated as a function of synthesis temperature and duration. Additionally, quantitative phase analysis was conducted using the Rietveld refinement method. It was found that increases in the synthesis temperature and holding time lead to increase in the mean particle size from 1 to 4.5 μm. The reaction rate constant for the synthesis reaction was also calculated.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1051-1056
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-8 z 8

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