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Tytuł:
Synthesis, Structure and Energetic Properties of a Catenated N6, Polynitro Compound: 1,1’-Azobis(3,5-dinitropyrazole)
Autorzy:
Li, Y.-N.
Shu, Y.-J.
Wang, Y.-L.
Wang, B.-Z.
Zhang, S.-Y.
Bi, F.-Q.
Powiązania:
https://bibliotekanauki.pl/articles/358573.pdf
Data publikacji:
2017
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
Tematy:
energetic compound
1,1’-azobis(3,5-dinitropyrazole)
synthesis
energetic properties
Opis:
A nitrogen-rich, polynitro energetic compound with an N,N-azo linkage, 1,1’-azobis(3,5-dinitropyrazole) (ABDNP), has been synthesized by an oxidative coupling reaction of 1-amino-3,5-dinitropyrazole with different oxidizing agents. The target compound was characterized by IR spectroscopy, 1H and 13C nuclear magnetic resonance spectroscopy, elemental analysis, mass spectra, X-ray diffraction and differential scanning calorimetry (DSC). The DSC results show that 1,1’-azobis(3,5-dinitropyrazole) decomposes at a relatively high onset temperature (202.9 °C), which indicates that 1,1’-azobis(3,5-dinitropyrazole) has acceptable thermal stability. The energetic properties were obtained, with a measured density and heat of formation matched by theoretically computed values based on the B3LYP method.
Źródło:
Central European Journal of Energetic Materials; 2017, 14, 2; 321-335
1733-7178
Pojawia się w:
Central European Journal of Energetic Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
A new basal actinopterygian fish from the Anisian (Middle Triassic) of Luoping, Yunnan Province, Southwest China
Autorzy:
Wen, W.
Zhang, Q.-Y.
Hu, S.-X.
Zhou, C.-Y.
Xie, T.
Huang, J.-Y.
Chen, Z.Q.
Benton, M.J.
Powiązania:
https://bibliotekanauki.pl/articles/21811.pdf
Data publikacji:
2012
Wydawca:
Polska Akademia Nauk. Instytut Paleobiologii PAN
Tematy:
actinopterygian fish
fish
Anisian
Middle Triassic
Luoping
Yunnan Province
China
Actinopterygii
Halecomorphi
Triassic
Opis:
The new neopterygian fish taxon Luoxiongichthys hyperdorsalis gen. et sp. nov. is established on the basis of five specimens from the second member of the Guanling Formation (Anisian, Middle Triassic) from Daaozi Quarry, Luoping, Yunnan Province, Southwest China. The new taxon is characterized by the following characters: triangular body outline with a distinct apex located between skull and dorsal fin; free maxilla; slender preopercular almost vertical; three suborbitals; at least eight strong branchiostegals with tubercles and comb−like ornamentation on the anterior margin; clavicles present; two postcleithra; ganoid scales covered by tubercles and pectinate ornamentation on the posterior margin with peg−and−socket structure; hemiheterocercal tail slightly forked. Comparison with basal actinopterygians reveals that the new taxon has parasemionotid−like triangular symplectics, but a semionotid opercular system. Cladistic analysis suggests that this new genus is a holostean, and either a basal halecomorph or basal semionotiform.
Źródło:
Acta Palaeontologica Polonica; 2012, 57, 1
0567-7920
Pojawia się w:
Acta Palaeontologica Polonica
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Coelacanths from the Middle Triassic Luoping Biota, Yunnan, South China, with the earliest evidence of ovoviviparity
Autorzy:
Wen, W.
Zhang, Q.-Y.
Hu, S.-X.
Benton, M.J.
Zhou, C.-Y.
Tao, X.
Huang, J.-Y.
Chen, Z.-Q.
Powiązania:
https://bibliotekanauki.pl/articles/23008.pdf
Data publikacji:
2013
Wydawca:
Polska Akademia Nauk. Instytut Paleobiologii PAN
Tematy:
coelacanth
Middle Triassic
Triassic
Yunnan province
South China
China
evidence
ovoviviparity
Anisian
Actinistia
Coelacanthoidei
Latimerioidei
Opis:
The fossil record of coelacanths is patchy, with very few taxa known from the Triassic of Asia. We report here two new genera and species of coelacanths from the Luoping Biota, a recently found site of exceptional fossil preservation from Yunnan, South China. The first new taxon, Luopingcoelacanthus eurylacrimalis, is based on four specimens, which to− gether show most aspects of the anatomy. One specimen shows two small coelacanths inside the ventral portion of the ab− dominal cavity, and these are interpreted as intrauterine embryos, close to birth size, based on comparisons with previ− ously reported embryos of the fossil coelacanths Rhabdoderma and Undina, and the extant genus Latimeria. Our new find extends the evidence for ovoviviparity in coelacanths back from the Late Jurassic to the Middle Triassic. The second new taxon, Yunnancoelacanthus acrotuberculatus, is based on one specimen, and differs from Luopingcoelacanthus in the dentary, lachrymojugal, number of rays of the first dorsal fin, and especially in the ornament on dermal bones and scales. Acladistic analysis shows that the new taxa are closest relatives to the derived clade Latimerioidei. The relatively high di− versity of coelacanths in the Early Triassic, and adaptations of living Latimeria to low−oxygen conditions, suggests that the group may have included ‘disaster taxa’ that benefited from anoxic and dysoxic ocean conditions in the aftermath of the end−Permian mass extinction.
Źródło:
Acta Palaeontologica Polonica; 2013, 58, 1
0567-7920
Pojawia się w:
Acta Palaeontologica Polonica
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The cavitation nuclei transient characteristics of Lennard-Jones fluid in cavitation inception
Autorzy:
Fu, Q.
Zhang, B.
Zhao, Y.
Zhu, R.
Liu, G.
Li, M.
Powiązania:
https://bibliotekanauki.pl/articles/259255.pdf
Data publikacji:
2018
Wydawca:
Politechnika Gdańska. Wydział Inżynierii Mechanicznej i Okrętownictwa
Tematy:
cavitation nuclei
molecular dynamics simulation
Lennard-Jones fluid
cavitation inception
nucleation
Opis:
In the field of ocean engineering, cavitation is widespread, for the study of cavitation nuclei transient characteristics in cavitation inception, we applied theoretical analysis and molecular dynamics (MD) simulation to study Lennard-Jones (L-J) fluid with different initial cavitation nuclei under the NVT-constant ensemble in this manuscript. The results showed that in cavitation inception, due to the decrease of liquid local pressure, the liquid molecules would enter the cavitation nuclei, which contributed to the growth of cavitation nuclei. By using molecular potential energy, it was found that the molecular potential energy was higher in cavitation nuclei part, while the liquid molecular potential energy changes greatly at the beginning of the cavitation nuclei growth. The density of the liquid and the surface layer changes more obvious, but density of vapor in the bubble changes inconspicuously. With the growth of cavitation nuclei, the RDF peak intensity increased, the peak width narrowed and the first valley moved inner. When cavitation nuclei initial size reduced, the peak intensity reduced, the corresponding rbin increased. With the decrease of the initial cavitation nuclei, the system pressure and total energy achieved a balance longer, and correspondingly, they were smaller. In addition, at the beginning of the cavitation nuclei growth, the total energy and system pressure changed greatly.
Źródło:
Polish Maritime Research; 2018, S 2; 75-84
1233-2585
Pojawia się w:
Polish Maritime Research
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Analysis of future climate scenarios and their impact on agriculture in eastern Arkansas, United States
Analiza scenariuszy klimatycznych i ich wpływ na rolnictwo we wschodniej części Arkansas
Autorzy:
Magugu, J. W.
Feng, S.
Huang, Q.
Zhang, Y.
West, G. H.
Powiązania:
https://bibliotekanauki.pl/articles/292796.pdf
Data publikacji:
2018
Wydawca:
Instytut Technologiczno-Przyrodniczy
Tematy:
agriculture
climate change
climate scenarios
precipitation
temperature
opady
rolnictwo
scenariusze klimatyczne
temperatura
zmiany klimatu
Opis:
Impact of climate change on crop growth is dynamic and difficult to quantify due to heterogeneity of the associated effects and their interactions within the Earth system. The main objective of this study is to establish how future climate change might affect agriculture, through an assessment of temperature and precipitation driven parameters. These include percentage number of rainy days with extreme precipitation, percentage of extreme precipitation relative to wet days, first fall frost days, last spring frost days, growing degree days, growing season length and the total precipitation. Results show modest increase in total precipitation with a slight increase in extreme precipitation, representing up to 2.2% increase by 2060 under representative concentration pathway (RCP 8.5) scenario. There would be late first fall frost days, early last spring frost days and increased growing season length by up to 2 weeks in 2060. The growing degree days are projected to increase under all scenarios for all crops, with cotton showing the largest increase of up to 37% relative to the baseline period.
Wpływ zmian klimatu na wzrost upraw jest dynamiczny i trudny do ilościowej oceny z powodu różnorodności powiązanych efektów i ich interakcji w całym systemie Ziemi. Głównym celem badań prezentowanych w niniejszej pracy było ustalenie, jak zmiany klimatu w przyszłości mogą wpłynąć na rolnictwo, na podstawie oceny parametrów związanych z temperaturą i opadami. Analizowano następujące parametry: udział (w %) dni deszczowych z ekstremalnym opadem, udział ekstremalnych opadów w stosunku do opadów ogółem, pierwsze jesienne dni z mrozem, ostatnie wiosenne dni z mrozem, stopniodni w sezonie wegetacyjnym, długość sezonu wegetacyjnego, i sumę opadów. Wyniki wykazują umiarkowany wzrost całkowitych opadów i niewielki wzrost opadów ekstremalnych – do 2,2% do roku 2060 wg scenariusza Representative Concentration Pathway (RCP 8.5). W 2060 roku pierwsze jesienne dni z mrozem wystąpią później, ostatnie wiosenne dni z mrozem wystąpią wcześniej, a sezon wegetacyjny wydłuży się o ok. 2 tygodnie. Zgodnie ze wszystkimi scenariuszami przewiduje się, że liczba stopniodni w sezonie wegetacyjnym zwiększy się dla wszystkich upraw, a największy przyrost (maksymalnie o 37%) w stosunku do okresu bazowego prognozuje się dla upraw bawełny.
Źródło:
Journal of Water and Land Development; 2018, 37; 97-112
1429-7426
2083-4535
Pojawia się w:
Journal of Water and Land Development
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Genome-wide association study of terpenoids in resin reveals candidate genes for resin yield in Pinus massoniana
Autorzy:
Bai, Q.
Zhang, Q.
Cai, Y.
Lian, H.
Liu, W.
Luo, M.
Zeng, L.
He, B.
Powiązania:
https://bibliotekanauki.pl/articles/2078149.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Instytut Dendrologii PAN
Tematy:
Pinus massoniana
GC-MS
terpenoid
GWAS
candidate gene
Opis:
Masson pine (Pinus massoniana) is an important species for resin tapping in China. Molecular assisted selection (MAS) has been gradually introduced in to the selection and breeding of masson pine. Until now, the lack of connection between genome information and phenotypic data has hindered the breeding and selection of important chemical compounds of xylem resin. In this study, gas chromatography mass spectrometer (GC-MS) was employed for qualitative and quantitative analysis of chemical compounds of resin collected from 69 masson pine germplasm resources. Then, genome-wide association study (GWAS) was conducted for the terpenoids with higher heritability. A total of 15 primary compounds, including six diterpenes and nine monoterpenes/sesquiterpenes, were detected from xylem resin. By using five GWAS methods, 42 associated SNPs were identified from these masson pines. The P. taeda genome database was used for detecting candidate genes related to the associated SNPs. By using transcriptome data, several members of PKc_like super family, Cytochrome P450, AP2-ERF, F-box, and ABC transporter were found to be highly expressed in the masson pines with higher resin-yielding capacity. The terpenoids associated SNPs can be directly used for MAS. These candidate genes, especially the two F-box members, will contribute to the study of terpenoid biosynthesis mechanisms in the future.
Źródło:
Dendrobiology; 2020, 84; 109-121
1641-1307
Pojawia się w:
Dendrobiology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Common mycelium networks with Paraglomus occultum induce better plant growth and signal substance changes between trifoliate orange seedlings
Autorzy:
Zhang, Y.-C.
Xie, M.-M.
Feng, H.-D.
Zhou, M.
Zhang, Z.Z.
Liu, C.-Y.
Wu, Q.-S.
Powiązania:
https://bibliotekanauki.pl/articles/11877054.pdf
Data publikacji:
2018
Wydawca:
Uniwersytet Przyrodniczy w Lublinie. Wydawnictwo Uniwersytetu Przyrodniczego w Lublinie
Opis:
Mycorrhizal mycelium can simultaneously colonize two and more neighboring plants to form common mycelium network (CMNs), whereas the information regarding CMN effects on endogenous signal substances is limited. In this study, a rootbox was separated by 37- or 0.45-μm mesh to establish donor chamber (the presence of roots and hyphae) and receptor (hyphae presented or not, free of roots) chamber, where an arbuscular mycorrhizal (AM) fungus Paraglomus occultum was inoculated into trifoliate orange seedlings of donor chamber to illustrate the underground communications of signal substances by CMNs. Mycorrhizal colonization resulted in better plant growth performance and greater root morphology in donor and receptor plants. AM inoculation increased significantly the root nitric oxide (NO) and calmodulin (CaM) levels of donor plants, regardless of 37- and 0.45-μm mesh, and subsequent CMNs induced higher root NO and CaM levels in receptor plants. Mycorrhizal colonization did not produce significant changes in root zeatin riboside (ZR) levels of donor plants, but CMN hyphae modulated lower root ZR levels of receptor plants. Mycorrhizal inoculation and subsequent CMN hyphae induced lower root gibberellin levels of donor and receptor plants, and only CMN hyphae produced lower root methyl jasmonate concentrations of receptor plants. Our results first reveal the underground communication of CaM, NO, and ZR by CMNs with P. occultum between trifoliate orange seedlings.
Źródło:
Acta Scientiarum Polonorum. Hortorum Cultus; 2018, 17, 6; 95-104
1644-0692
Pojawia się w:
Acta Scientiarum Polonorum. Hortorum Cultus
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
A new troodontid theropod from the Late Cretaceous of central China, and the radiation of Asian troodontids
Autorzy:
Lu, J
Xu, L.
Liu, Y.
Zhang, X.
Jia, S.
Ji, Q.
Powiązania:
https://bibliotekanauki.pl/articles/20912.pdf
Data publikacji:
2010
Wydawca:
Polska Akademia Nauk. Instytut Paleobiologii PAN
Tematy:
new theropod
Late Cretaceous
Central China
Asian troodontid
troodontid
Theropoda
Troodontidae
Xixiasaurus
Cretaceous
Henan province
China
paleontology
Opis:
A new troodontid dinosaur, Xixiasaurus henanensis gen. et sp. nov., from the Upper Cretaceous Majiacun Formation of the Xixia Basin, Henan Province, is erected, based on a partial skull. It is characterized by bearing 22 maxillary teeth, a distinct opening on the lateral surface of the base of nasal process of the premaxilla, the rostral end of the upper jaw forming a tapered U−shape, and the mandibular symphyseal region slightly inflected medially. Xixiasaurus is most closely related to the Mongolian Byronosaurus among troodontids. Byronosaurus, Urbacodon, and Xixiasaurus may form a new clade, suggesting an endemic radiation of troodontids across Asia, including multiple taxa without dental serrations. The discovery of Xixiasaurus in the Xixia Basin may imply that the Xixiasaurus−bearing Majiacun Formation is Campanian in age.
Źródło:
Acta Palaeontologica Polonica; 2010, 55, 3; 381-388
0567-7920
Pojawia się w:
Acta Palaeontologica Polonica
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Molecular cloning, bioinformation analysis and expression of the strictosidine synthase in Dendrobium officinale
Autorzy:
Zhu, Y.-F.
Fan, H.-H.
Li, D.-H.
Jin, Q.
Zhang, C.-M.
Zhu, L.-Q.
Song, C.
Cai, Y.-P.
Lin, Y.
Powiązania:
https://bibliotekanauki.pl/articles/12715947.pdf
Data publikacji:
2020
Wydawca:
Uniwersytet Przyrodniczy w Lublinie. Wydawnictwo Uniwersytetu Przyrodniczego w Lublinie
Opis:
The enzyme strictosidine synthase (STR, EC: 4.3.3.2) plays a key role in the biosynthetic pathway of terpenoid indole alkaloid (TIA). It catalyzes the condensation of the tryptamine and secologanin to form 3α(S)-strictosidine, which is the common precursor of all TIAs. In this paper, a STR gene designated as DoSTR (GenBank: KX068707) was first cloned and characterized from Dendrobium officinale with rapid amplified cDNA ends method (RACE). DoSTR has a length of 1380bp with 1179bp open reading frame encoding 392 amino acids. BlastP analyses showed that its amino acid sequence was classified into Str_synth superfamily. qRT-PCR showed that DoSTR was expressed in all tissues tested, with a significantly higher level in flower and the lowest in stem. Four different treatments with MeJA, SA, ABA and AgNO₃, respectively, could induce the DoSTR expression to a different extent. And the effect of MeJA was the most obvious and transcript level of DoSTR induced by MeJA was 20.7 times greater than that of control at 48 hours after treatment. Furthermore, it was found that DoSTR was localized in vacuole through transient expression in tobacco. The characterization and expression of DoSTR can help in further studying the role of DoSTR in the biosynthesis of TIAs in D. officinale. This study may throw light on the alkaloid biosynthesis pathway of D. officinale.
Źródło:
Acta Scientiarum Polonorum. Hortorum Cultus; 2020, 19, 3; 111-124
1644-0692
Pojawia się w:
Acta Scientiarum Polonorum. Hortorum Cultus
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Morphology and developmental traits of the trilobite Changaspis elongata from the Cambrian Series 2 of Guizhou, South China
Autorzy:
Du, G.-Y.
Peng, J.
Wang, D.-Z.
Wang, Q.-J.
Wang, Y.-F.
Zhang, H.
Powiązania:
https://bibliotekanauki.pl/articles/22906.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Instytut Paleobiologii PAN
Opis:
The morphology and ontogeny of the trilobite Changaspis elongata based on 216 specimens collected from the Lazizhai section of the Balang Formation (Stage 4, Series 2 of the Cambrian) in Guizhou Province, South China are described. The relatively continuous ontogenetic series reveals morphological changes, and shows that the species has seventeen thoracic segments in the holaspid period, instead of the sixteen as previously suggested. The development of the pygidial segments shows that their number gradually decreases during ontogeny. A new dataset of well-preserved specimens offers a unique opportunity to investigate developmental traits after segment addition is completed. The ontogenetic size progressions for the lengths of cephalon and trunk show overall compliance with Dyar’s rule. As a result of different average growth rates for the lengths of cephalon, trunk and pygidium, the length of the thorax relative to the body shows a gradually increasing trend; however, the cephalon and pygidium follow the opposite trend. Morphometric analysis across fourteen post-embryonic stages reveals growth gradients with increasing values for each thoracic segment from anterior to posterior. The reconstruction of the development traits shows visualization of the changes in relative growth and segmentation for the different body parts. The new dataset and growth gradient of the trunk suggest that the thoracic segment growth dynamics of early Cambrian to Silurian trilobites follow the same general continuous, steady-state growth gradient decreasing from posterior to anterior.
Źródło:
Acta Palaeontologica Polonica; 2019, 64, 4
0567-7920
Pojawia się w:
Acta Palaeontologica Polonica
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effects of Polymeric Binders on the RDX-based Explosive Response Character under Slow Cook-off Conditions
Autorzy:
Yan, X.
Li, X. D.
Zhang, Y. R.
Liu, L.
Zhang, X. M.
Tan, Y. X.
Wang, H.
Wang, X. Q.
Powiązania:
https://bibliotekanauki.pl/articles/358419.pdf
Data publikacji:
2018
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
Tematy:
RDX-based explosive
slow cook-off experiment
binder content
binder type
Opis:
Due to safety requirements, insensitive behaviour under slow thermal heating (cook-off) conditions is a desirable behaviour for today’s munitions. In this paper a cook-off device is designed to test two groups of RDX-based PBX explosives. In the first group the binder type was varied and in the second group the binder content of the RDX-based explosive was changed. Eleven samples were examined in order to evaluate the influence of four different binders and seven different binder contents on the shell deformation and the degree of the involved reaction. The test results showed that the degree of the reaction can be improved by changing the binder content, but not by the binder type. This phenomenon was explained by the thermal-conduction theory.
Źródło:
Central European Journal of Energetic Materials; 2018, 15, 2; 339-350
1733-7178
Pojawia się w:
Central European Journal of Energetic Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Kinetics of photoelectrocatalytic degradation of diclofenac using N, S co-doped TiO2 nano-crystallite decorated TiO2 nanotube arrays photoelectrode
Autorzy:
Cui, Y.
Deng, X.
Ma, Q.
Zhang, H.
Cheng, X.
Li, X.
Xie, M.
Cheng, Q.
Li, B.
Powiązania:
https://bibliotekanauki.pl/articles/207955.pdf
Data publikacji:
2018
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
effluents
nanotubes
sodium sulfate
sulfur compounds
yarn
photoelectrocatalytic degradation
ścieki
nanorurki
siarczan sodu
związki siarki
przędza
Opis:
As a non-steroidal anti-inflammatory drug, diclofenac, was commonly used as analgesic, antiarthritic and antirheumatic, and has frequently been detected in municipal wastewater treatment plants (MWTPs) effluents and demonstrated to be potentially environmental risk on human beings. In the present study, N, S co-doped TiO2 nano-crystallites decorated TiO2 nano-tube arrays (N, S-TiO2 NCs/TiO2 NTAs) photoelectrode was used to degrade diclofenac containing wastewater. In addition, the effects of some critical parameters including initial pH, external positive potential, sodium sulfate concentration and initial diclofenac concentration on the photoelectrocatalytic (PEC) degradation of diclofenac containing wastewater and dynamic characteristics were investigated systematically. Results showed that N, S-TiO2 NCs/TiO2 NTAs photoelectrode exhibited high PEC efficiency for the degradation of diclofenac, in which the PEC processes fitted well with the Langmuir–Hinshelwood (L–H) model. Furthermore, external additional anions such as Cl–, ClO– and NO3 – played an important role in inhibiting the degradation of diclofenac. Also, the N, S-TiO2 NCs/TiO2 NTAs photoelectrode possessed good stability for consecutive applications for degradation of diclofenac, which could potentially be utilized in wastewater treatment.
Źródło:
Environment Protection Engineering; 2018, 44, 2; 117-130
0324-8828
Pojawia się w:
Environment Protection Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Selection of reference genes for quantitative real-time RT-PCR on gene expression in Golden Pompano (Trachinotus ovatus)
Autorzy:
Chen, X.J.
Sun, Y.
Zhang, X.Q.
Huang, S.
Cao, Z.J.
Qin, Q.W.
Hu, W.T.
Zhou, Y.C.
Powiązania:
https://bibliotekanauki.pl/articles/2087908.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Źródło:
Polish Journal of Veterinary Sciences; 2017, 3; 583-594
1505-1773
Pojawia się w:
Polish Journal of Veterinary Sciences
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Research on the Mechanism and Kinetics of Polymorphic Transitions of ε CL-20 in Composite Systems
Autorzy:
Guo, X.-Y.
Zhang, P.
Xu, J.-J.
Wang, Z.-H.
Jiao, Q.-J.
Powiązania:
https://bibliotekanauki.pl/articles/358032.pdf
Data publikacji:
2015
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
Tematy:
polymorphic transition
kinetics
activation energy
transition temperature
Opis:
In order to explore the polymorphic transition law for ε-CL-20 in composite systems, the polymorphic transition process of pure ε-CL-20 crystals stimulated by heat was investigated by the X-ray Diffraction (XRD) method, and the kinetic parameters of the polymorphic transition process were calculated (including the apparent activation energy Ea and the pre-exponential factor lnA). Meanwhile the effects of different additives on the polymorphic transition process and kinetics of ε-CL-20 were explored in detail. The experimental results showed that the ε-form tends to transform into the γ- form on heating and that the Ea and lnA for the transition process were 209.97 kJ/mol and 57.47, respectively. The first group of additives clearly promoted the polymorphic transition of ε-CL-20 and lowered the initial transition temperature and the activation energy. The second and third groups of additives inhibited the polymorphic transition of ε-CL-20 and raised the initial transition temperature and the activation energy.
Źródło:
Central European Journal of Energetic Materials; 2015, 12, 4; 689-702
1733-7178
Pojawia się w:
Central European Journal of Energetic Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
UV-Vis spectroscopic detection coupled with chemometrics for the measurement of mixed organic acids in water samples enriched by radial electric focusing solid phase extraction
Autorzy:
Guo, Y.
Liu, X.
Liu, J.
Bian, X.
Zhang, Q.
Pan, J.
Wan, D.
Powiązania:
https://bibliotekanauki.pl/articles/221808.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
chemometrics
UV-Vis spectrophotometer
radial electric focusing solid phase extraction
mixed organic acids
Opis:
Due to the difficulty of detecting traces of organic acid mixture in an aqueous sample and the complexity of resolving UV-Vis spectra effectively, a combinatory method based on a self-made radical electric focusing solid phase extraction (REFSPE) device, UV-Vis detection and partial least squares (PLS) calculation is proposed here. In this study, REFSPE was used to enhance the extraction process of analytes between the aqueous phase and the membrane phase to enrich the trace of mixed organic acid efficiently. Then, the analytes, which were eluted from the adsorption film by ethanol with the assistance of an ultrasonic cleaning machine, were detected with UV-Vis spectrophotometry. After that, the PLS method was introduced to solve the problem of overlapping peaks in UV-Vis spectra of mixed substances and to quantify each compound. The linearly dependent coefficients between the predicted value of the model and the actual concentration of the sample were all higher than 0.99. The limit values of detection for benzoic acid, phthalic acid and p-toluene sulfonic acid were found at 9.9 μg/L, 12.2 μg/L and 13.8 μg/L with the relative recovery values between 84.8% and 117.9%. The RSD (n = 20) values of each component are 1.17%, 1.11% and 0.86%, respectively. Therefore, the proposed combined method can determine traces of complex materials in an aqueous sample efficiently and has wonderful potential applications.
Źródło:
Metrology and Measurement Systems; 2018, 25, 2; 317-329
0860-8229
Pojawia się w:
Metrology and Measurement Systems
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 31-45 z 57

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