Synthesis and characterization of transition metal complexes of some novel pyrazolo-chalcone derivatives

Some novel pyrazolo-chalcone molecules were synthesized by condensation of pyrzolo aldehyde with appropriate acetophenone. The synthesis of some metal complexes of transition metal was carried out with these pyrazoleo heterocyclic compounds. Each metal complex was synthesized by the reaction of new pyrazolochalcone derivatives with the metal salts such as Co(CH3COO)2·6H2O, Ni(CH3COO)2·6H2O, and Cu(CH3COO)2·2H2O. For the structure elucidation of ligand molecule various spectroscopic techniques such as 1H NMR, IR and mass has been used. The synthesized metal complexes were subjected to thermal study i.e., TGA and DTA in order to check structural conformation of synthesized metal complexes.